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Information card for entry 1568760
Preview
| Coordinates | 1568760.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C19 H22 O5 |
|---|---|
| Calculated formula | C19 H22 O5 |
| Title of publication | Total synthesis of (-)-scabrolide A and (-)-yonarolide. |
| Authors of publication | Hafeman, Nicholas J.; Loskot, Steven A.; Reimann, Christopher E.; Pritchett, Beau P.; Virgil, Scott C.; Stoltz, Brian M. |
| Journal of publication | Chemical science |
| Year of publication | 2023 |
| Journal volume | 14 |
| Journal issue | 18 |
| Pages of publication | 4745 - 4758 |
| a | 6.1878 ± 0.0004 Å |
| b | 14.9676 ± 0.0014 Å |
| c | 17.511 ± 0.002 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1621.8 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0369 |
| Residual factor for significantly intense reflections | 0.0353 |
| Weighted residual factors for significantly intense reflections | 0.0889 |
| Weighted residual factors for all reflections included in the refinement | 0.0906 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.048 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 284236 (current) | 2023-06-05 | cif/ Updating files of 1568754, 1568755, 1568756, 1568757, 1568758, 1568759, 1568760, 1568761, 1568762 Original log message: Adding full bibliography for 1568754--1568762.cif. |
1568760.cif |
| 282188 | 2023-04-02 | cif/ Adding structures of 1568754, 1568755, 1568756, 1568757, 1568758, 1568759, 1568760, 1568761, 1568762 via cif-deposit CGI script. |
1568760.cif |
All data in the COD and the database itself are dedicated to the
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.
Users of the data should acknowledge the original authors of the
structural data.