Crystallography Open Database

Information card for entry 1504801

Preview

Coordinates	1504801.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H22 Ag Cl3 N2
Calculated formula	C28 H22 Ag Cl3 N2
Title of publication	Synthesis of electronically diverse tetraarylimidazolylidene carbenes via catalytic aldimine coupling.
Authors of publication	Ogle, James W.; Zhang, Jubo; Reibenspies, Joseph H.; Abboud, Khalil A.; Miller, Stephen A.
Journal of publication	Organic letters
Year of publication	2008
Journal volume	10
Journal issue	17
Pages of publication	3677 - 3680
a	16.9545 ± 0.0011 Å
b	23.2586 ± 0.0015 Å
c	6.5773 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	2593.7 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	36
Hermann-Mauguin space group symbol	C m c 21
Hall space group symbol	C 2c -2
Residual factor for all reflections	0.0281
Residual factor for significantly intense reflections	0.0263
Weighted residual factors for significantly intense reflections	0.0623
Weighted residual factors for all reflections included in the refinement	0.063
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1504801.cif
91932	2013-12-28	cif/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the range 1 CIFs.	1504801.cif
42375	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 1504801 via cif-deposit CGI script.	1504801.cif