Crystallography Open Database

Information card for entry 1507938

Preview

Coordinates	1507938.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H72 Cl6 N2 Pd2
Calculated formula	C32 H72 Cl6 N2 Pd2
SMILES	[Pd]12(Cl)([Cl][Pd]1([Cl]2)(Cl)Cl)Cl.[N+](CCCC)(CCCC)(CCCC)CCCC.[N+](CCCC)(CCCC)(CCCC)CCCC
Title of publication	Core@shell bimetallic nanoparticle synthesis via anion coordination.
Authors of publication	Serpell, Christopher J.; Cookson, James; Ozkaya, Dogan; Beer, Paul D.
Journal of publication	Nature chemistry
Year of publication	2011
Journal volume	3
Journal issue	6
Pages of publication	478 - 483
a	10.9999 ± 0.0005 Å
b	11.9542 ± 0.0005 Å
c	17.7219 ± 0.0009 Å
α	91.4858 ± 0.0017°
β	103.352 ± 0.002°
γ	107.87 ± 0.002°
Cell volume	2146.14 ± 0.17 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1097
Residual factor for significantly intense reflections	0.0509
Weighted residual factors for all reflections	0.117
Weighted residual factors for significantly intense reflections	0.0821
Weighted residual factors for all reflections included in the refinement	0.1169
Goodness-of-fit parameter for all reflections included in the refinement	0.9755
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1507938.cif
120071	2014-07-11	Adding DOIs to range 1 structures.	1507938.cif
62484	2012-07-09	cif/ Adding structures of 1507938 via cif-deposit CGI script.	1507938.cif