Crystallography Open Database

Information card for entry 1507999

Preview

Coordinates	1507999.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H26 Cl4 F N2 O4 Pd2
Calculated formula	C30 H22 N2 O4 Pd2
Title of publication	Synthesis and structure of solution-stable one-dimensional palladium wires.
Authors of publication	Campbell, Michael G.; Powers, David C.; Raynaud, Jean; Graham, Michael J.; Xie, Ping; Lee, Eunsung; Ritter, Tobias
Journal of publication	Nature chemistry
Year of publication	2011
Journal volume	3
Journal issue	12
Pages of publication	949 - 953
a	11.3423 ± 0.0014 Å
b	16.545 ± 0.002 Å
c	17.388 ± 0.002 Å
α	90°
β	97.364 ± 0.002°
γ	90°
Cell volume	3236.1 ± 0.7 Å³
Cell temperature	130 ± 1 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0543
Residual factor for significantly intense reflections	0.0346
Weighted residual factors for significantly intense reflections	0.0838
Weighted residual factors for all reflections included in the refinement	0.0894
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1507999.cif
120071	2014-07-11	Adding DOIs to range 1 structures.	1507999.cif
62545	2012-07-09	cif/ Adding structures of 1507999 via cif-deposit CGI script.	1507999.cif