#------------------------------------------------------------------------------
#$Date: 2016-02-18 17:37:37 +0200 (Thu, 18 Feb 2016) $
#$Revision: 176729 $
#$URL: svn://www.crystallography.net/cod/cif/1/51/68/1516823.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1516823
loop_
_publ_author_name
'Peng Hu'
'Congming Zhang'
'Yuanyuan Gao'
'Yungai Li'
'Yue Ma'
'Licun Li'
'Daizheng Liao'
_publ_section_title
;
 Lanthanide-radical linear chain compounds based on
 2,4,4,5,5-pentamethylimidazoline-1-oxyl-3-oxide: Structure and magnetic
 properties
;
_journal_name_full
;
Inorganica Chimica Acta
;
_journal_page_first              136
_journal_page_last               140
_journal_volume                  398
_journal_year                    2013
_chemical_formula_sum            'C23 H18 Dy F18 N2 O8'
_chemical_formula_weight         954.89
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                90.00
_cell_angle_beta                 93.768(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.775(3)
_cell_length_b                   16.108(5)
_cell_length_c                   19.189(6)
_cell_measurement_temperature    113(2)
_cell_volume                     3323.3(17)
_computing_cell_refinement       CrystalClear
_computing_data_collection       CrystalClear
_computing_data_reduction        CrystalClear
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'CrystalStructure 3.8'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      113(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0514
_diffrn_reflns_av_sigmaI/netI    0.0484
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            24737
_diffrn_reflns_theta_full        25.01
_diffrn_reflns_theta_max         25.01
_diffrn_reflns_theta_min         1.65
_exptl_absorpt_coefficient_mu    2.395
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.617
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.909
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             1848
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.967
_refine_diff_density_min         -1.831
_refine_diff_density_rms         0.152
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.017
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     470
_refine_ls_number_reflns         5801
_refine_ls_number_restraints     36
_refine_ls_restrained_S_all      1.014
_refine_ls_R_factor_all          0.0622
_refine_ls_R_factor_gt           0.0532
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0600P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1204
_refine_ls_wR_factor_ref         0.1262
_reflns_number_gt                5167
_reflns_number_total             5800
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ICA-2013-398-136-140-2.cif
_cod_data_source_block           II
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to the built-in table from CIF Core dictionary
named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_sg_symbol_H-M      P21/n
_cod_database_code               1516823
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy Dy 0.21020(2) 0.462554(17) 0.235132(15) 0.02875(13) Uani 1 1 d . . .
O7 O 0.2107(4) 0.5743(3) 0.3139(2) 0.0370(10) Uani 1 1 d . . .
O5 O 0.0566(4) 0.5548(3) 0.1931(2) 0.0376(11) Uani 1 1 d . . .
O3 O 0.0415(4) 0.4193(3) 0.2979(2) 0.0341(10) Uani 1 1 d . . .
F6 F -0.1368(4) 0.4287(3) 0.3881(2) 0.0606(12) Uani 1 1 d . . .
F2 F 0.0308(3) 0.1901(2) 0.1309(2) 0.0461(10) Uani 1 1 d . . .
C17 C 0.1989(5) 0.7132(4) 0.2853(3) 0.0291(14) Uani 1 1 d . . .
F1 F -0.1501(3) 0.2415(3) 0.1062(2) 0.0561(11) Uani 1 1 d . . .
C9 C 0.1982(6) 0.5412(4) 0.0732(4) 0.0413(17) Uani 1 1 d . B .
F3 F 0.0064(4) 0.2878(2) 0.05490(19) 0.0505(10) Uani 1 1 d . . .
O4 O 0.0981(4) 0.3640(2) 0.1688(2) 0.0347(10) Uani 1 1 d . . .
N1 N 0.1707(4) 0.6469(3) 0.3229(3) 0.0309(12) Uani 1 1 d . A .
O6 O 0.2528(4) 0.5012(3) 0.1211(2) 0.0399(10) Uani 1 1 d . . .
N2 N 0.1460(4) 0.7807(3) 0.3117(3) 0.0317(12) Uani 1 1 d . . .
C2 C -0.0029(6) 0.3246(4) 0.1725(3) 0.0353(15) Uani 1 1 d . . .
F8 F -0.1259(4) 0.6768(3) 0.0765(2) 0.0826(16) Uani 1 1 d . . .
F9 F -0.0351(5) 0.7239(3) 0.1707(3) 0.0827(16) Uani 1 1 d . . .
F5 F -0.2431(4) 0.3373(3) 0.3322(3) 0.0835(16) Uani 1 1 d . . .
C3 C -0.0841(6) 0.3276(4) 0.2272(3) 0.0377(15) Uani 1 1 d . . .
H3 H 0.0000 0.2987 0.2235 0.046 Uiso 1 1 d . . .
C16 C 0.2717(5) 0.7133(4) 0.2224(3) 0.0355(15) Uani 1 1 d . . .
H16A H 0.3554 0.6920 0.2357 0.054 Uiso 1 1 d . . .
H16B H 0.2775 0.7700 0.2051 0.054 Uiso 1 1 d . . .
H16C H 0.2311 0.6777 0.1868 0.054 Uiso 1 1 d . . .
C7 C 0.0272(5) 0.5905(4) 0.1352(3) 0.0371(15) Uani 1 1 d . . .
C5 C -0.0501(5) 0.3734(4) 0.2870(3) 0.0328(14) Uani 1 1 d . . .
C1 C -0.0308(6) 0.2603(4) 0.1155(4) 0.0398(16) Uani 1 1 d . . .
F4 F -0.0785(5) 0.3016(3) 0.3901(3) 0.0859(16) Uani 1 1 d . . .
F7 F -0.1681(4) 0.6269(3) 0.1738(3) 0.0914(18) Uani 1 1 d . . .
C19 C 0.0959(6) 0.6678(4) 0.3836(4) 0.0442(17) Uani 1 1 d . . .
C8 C 0.0882(6) 0.5840(4) 0.0752(4) 0.0428(17) Uani 1 1 d . . .
H8 H 0.0547 0.6107 0.0338 0.054 Uiso 1 1 d . . .
C6 C -0.0792(7) 0.6550(5) 0.1386(4) 0.057(2) Uani 1 1 d . . .
C4 C -0.1291(7) 0.3606(4) 0.3502(4) 0.0485(18) Uani 1 1 d . . .
C18 C 0.0733(6) 0.7619(4) 0.3747(4) 0.0387(16) Uani 1 1 d . A .
C10 C 0.2613(8) 0.5438(5) 0.0054(5) 0.063(2) Uani 1 1 d . . .
O8 O 0.1514(4) 0.8544(2) 0.2872(2) 0.0386(11) Uani 1 1 d . . .
O2 O 0.4123(4) 0.5134(3) 0.2450(2) 0.0403(11) Uani 1 1 d . . .
O1 O 0.2943(4) 0.4160(2) 0.3431(2) 0.0378(11) Uani 1 1 d . . .
C11 C 0.3950(6) 0.4265(4) 0.3762(4) 0.0413(17) Uani 1 1 d . . .
C14 C 0.4971(6) 0.5085(4) 0.2912(4) 0.0446(18) Uani 1 1 d . . .
C22B C 0.0843(18) 0.8264(12) 0.4265(10) 0.0560(15) Uani 0.446(7) 1 d P A 2
H22A H 0.1624 0.8195 0.4551 0.084 Uiso 0.446(7) 1 calc PR A 2
H22B H 0.0142 0.8230 0.4564 0.084 Uiso 0.446(7) 1 calc PR A 2
H22C H 0.0838 0.8806 0.4034 0.084 Uiso 0.446(7) 1 calc PR A 2
C23B C 0.1205(16) 0.6201(11) 0.4431(9) 0.0560(15) Uani 0.446(7) 1 d P A 2
H23A H 0.1231 0.5613 0.4301 0.084 Uiso 0.446(7) 1 calc PR A 2
H23B H 0.0550 0.6289 0.4754 0.084 Uiso 0.446(7) 1 calc PR A 2
H23C H 0.2010 0.6365 0.4658 0.084 Uiso 0.446(7) 1 calc PR A 2
C21B C -0.0692(16) 0.7692(13) 0.3354(10) 0.0560(15) Uani 0.446(7) 1 d P A 2
H21A H -0.0750 0.8198 0.3070 0.084 Uiso 0.446(7) 1 calc PR A 2
H21B H -0.1307 0.7714 0.3707 0.084 Uiso 0.446(7) 1 calc PR A 2
H21C H -0.0854 0.7207 0.3053 0.084 Uiso 0.446(7) 1 calc PR A 2
C20B C -0.0430(16) 0.6289(11) 0.3528(10) 0.0560(15) Uani 0.446(7) 1 d P A 2
H20A H -0.0677 0.6548 0.3078 0.084 Uiso 0.446(7) 1 calc PR A 2
H20B H -0.1058 0.6407 0.3861 0.084 Uiso 0.446(7) 1 calc PR A 2
H20C H -0.0358 0.5687 0.3466 0.084 Uiso 0.446(7) 1 calc PR A 2
F13 F 0.3649(5) 0.3079(3) 0.4450(2) 0.0804(16) Uani 1 1 d . . .
F14 F 0.3304(6) 0.4260(4) 0.4901(3) 0.0996(19) Uani 1 1 d . . .
F15 F 0.5161(5) 0.3856(3) 0.4792(3) 0.108(2) Uani 1 1 d . . .
C13 C 0.4990(6) 0.4690(4) 0.3555(5) 0.050(2) Uani 1 1 d . . .
H13 H 0.5712 0.4725 0.3856 0.062 Uiso 1 1 d . . .
C15 C 0.6193(7) 0.5485(5) 0.2695(6) 0.065(3) Uani 1 1 d . . .
C12 C 0.4021(9) 0.3860(5) 0.4485(5) 0.067(2) Uani 1 1 d . . .
C22A C 0.1500(14) 0.8087(10) 0.4379(8) 0.0560(15) Uani 0.554(7) 1 d P A 1
H22D H 0.2384 0.7947 0.4371 0.084 Uiso 0.554(7) 1 calc PR A 1
H22E H 0.1191 0.7910 0.4824 0.084 Uiso 0.554(7) 1 calc PR A 1
H22F H 0.1392 0.8688 0.4326 0.084 Uiso 0.554(7) 1 calc PR A 1
C23A C 0.2050(13) 0.6621(9) 0.4490(7) 0.0560(15) Uani 0.554(7) 1 d P A 1
H23D H 0.2408 0.6061 0.4508 0.084 Uiso 0.554(7) 1 calc PR A 1
H23E H 0.1678 0.6740 0.4932 0.084 Uiso 0.554(7) 1 calc PR A 1
H23F H 0.2705 0.7027 0.4416 0.084 Uiso 0.554(7) 1 calc PR A 1
C21A C -0.0526(13) 0.7938(10) 0.3651(8) 0.0560(15) Uani 0.554(7) 1 d P A 1
H21D H -0.0505 0.8506 0.3470 0.084 Uiso 0.554(7) 1 calc PR A 1
H21E H -0.0911 0.7936 0.4100 0.084 Uiso 0.554(7) 1 calc PR A 1
H21F H -0.1011 0.7586 0.3318 0.084 Uiso 0.554(7) 1 calc PR A 1
C20A C -0.0002(13) 0.6084(9) 0.3968(8) 0.0560(15) Uani 0.554(7) 1 d P A 1
H20D H -0.0648 0.6100 0.3585 0.084 Uiso 0.554(7) 1 calc PR A 1
H20E H -0.0369 0.6224 0.4407 0.084 Uiso 0.554(7) 1 calc PR A 1
H20F H 0.0359 0.5526 0.4003 0.084 Uiso 0.554(7) 1 calc PR A 1
F10 F 0.5995(4) 0.6206(3) 0.2391(3) 0.0675(13) Uani 1 1 d . . .
F11 F 0.6763(5) 0.4996(4) 0.2277(4) 0.108(2) Uani 1 1 d . . .
F12 F 0.6986(5) 0.5638(4) 0.3245(4) 0.113(2) Uani 1 1 d . . .
F16A F 0.1840(12) 0.5575(8) -0.0518(6) 0.0854(19) Uani 0.512(6) 1 d PU B 1
F17B F 0.2560(12) 0.4630(7) -0.0239(6) 0.0854(19) Uani 0.512(6) 1 d PU B 2
F18B F 0.3827(11) 0.5507(8) 0.0151(6) 0.0854(19) Uani 0.512(6) 1 d PU B 2
F16B F 0.2289(13) 0.5974(9) -0.0409(7) 0.0854(19) Uani 0.488(6) 1 d PU B 2
F17A F 0.3394(13) 0.4846(9) -0.0064(6) 0.0854(19) Uani 0.488(6) 1 d PU B 1
F18A F 0.3341(10) 0.6149(8) 0.0084(5) 0.0854(19) Uani 0.488(6) 1 d PU B 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
O2 Dy O4 137.44(15) .
O2 Dy O5 116.38(15) .
O4 Dy O5 85.07(15) .
O2 Dy O1 74.53(16) .
O4 Dy O1 115.18(14) .
O5 Dy O1 137.68(16) .
O2 Dy O6 75.10(16) .
O4 Dy O6 78.29(15) .
O5 Dy O6 71.69(15) .
O1 Dy O6 145.61(15) .
O2 Dy O7 73.45(15) .
O4 Dy O7 148.73(14) .
O5 Dy O7 72.86(15) .
O1 Dy O7 71.96(14) .
O6 Dy O7 113.80(15) .
O2 Dy O3 144.59(15) .
O4 Dy O3 71.73(15) .
O5 Dy O3 79.12(15) .
O1 Dy O3 73.59(15) .
O6 Dy O3 139.53(14) .
O7 Dy O3 82.35(15) .
O2 Dy O8 70.95(14) 2_545
O4 Dy O8 72.97(14) 2_545
O5 Dy O8 148.72(16) 2_545
O1 Dy O8 73.10(15) 2_545
O6 Dy O8 82.05(15) 2_545
O7 Dy O8 135.25(14) 2_545
O3 Dy O8 113.23(14) 2_545
N1 O7 Dy 144.3(4) .
C7 O5 Dy 136.2(4) .
C5 O3 Dy 136.4(4) .
N1 C17 N2 109.1(6) .
N1 C17 C16 126.3(6) .
N2 C17 C16 124.5(6) .
O6 C9 C8 127.6(7) .
O6 C9 C10 115.8(6) .
C8 C9 C10 116.7(6) .
C2 O4 Dy 136.9(4) .
O7 N1 C17 125.1(5) .
O7 N1 C19 121.5(5) .
C17 N1 C19 113.1(5) .
C9 O6 Dy 135.7(4) .
O8 N2 C17 125.7(5) .
O8 N2 C18 121.2(5) .
C17 N2 C18 113.2(5) .
O4 C2 C3 127.1(6) .
O4 C2 C1 115.5(6) .
C3 C2 C1 117.0(6) .
C5 C3 C2 119.2(6) .
O5 C7 C8 126.5(6) .
O5 C7 C6 114.1(6) .
C8 C7 C6 119.0(6) .
O3 C5 C3 128.2(6) .
O3 C5 C4 115.0(6) .
C3 C5 C4 116.6(6) .
F1 C1 F3 107.7(5) .
F1 C1 F2 107.5(5) .
F3 C1 F2 107.5(5) .
F1 C1 C2 113.5(6) .
F3 C1 C2 110.2(6) .
F2 C1 C2 110.3(5) .
C23B C19 C20A 65.8(9) .
C23B C19 N1 115.6(9) .
C20A C19 N1 114.6(7) .
C23B C19 C18 130.9(9) .
C20A C19 C18 124.1(8) .
N1 C19 C18 103.0(5) .
C23B C19 C23A 42.4(8) .
C20A C19 C23A 108.0(9) .
N1 C19 C23A 100.6(6) .
C18 C19 C23A 103.6(7) .
C23B C19 C20B 101.5(10) .
C20A C19 C20B 35.8(8) .
N1 C19 C20B 98.8(8) .
C18 C19 C20B 101.3(8) .
C23A C19 C20B 143.8(9) .
C7 C8 C9 121.7(6) .
F7 C6 F8 108.4(6) .
F7 C6 F9 107.6(7) .
F8 C6 F9 107.4(7) .
F7 C6 C7 111.4(7) .
F8 C6 C7 112.4(7) .
F9 C6 C7 109.5(6) .
F5 C4 F4 107.0(6) .
F5 C4 F6 106.9(6) .
F4 C4 F6 108.6(6) .
F5 C4 C5 112.8(6) .
F4 C4 C5 109.0(6) .
F6 C4 C5 112.3(5) .
C22B C18 C21A 82.3(10) .
C22B C18 N2 112.6(9) .
C21A C18 N2 110.8(8) .
C22B C18 C19 129.0(10) .
C21A C18 C19 120.1(8) .
N2 C18 C19 101.4(5) .
C22B C18 C22A 29.0(8) .
C21A C18 C22A 111.1(8) .
N2 C18 C22A 103.9(7) .
C19 C18 C22A 107.9(8) .
C22B C18 C21B 107.0(10) .
C21A C18 C21B 24.9(7) .
N2 C18 C21B 97.6(8) .
C19 C18 C21B 104.7(8) .
C22A C18 C21B 136.0(9) .
F16B C10 F17A 121.8(10) .
F16B C10 F18B 105.4(10) .
F17A C10 F18B 55.8(8) .
F16B C10 F16A 36.4(7) .
F17A C10 F16A 110.5(11) .
F18B C10 F16A 131.0(9) .
F16B C10 F18A 66.2(9) .
F17A C10 F18A 103.9(10) .
F18B C10 F18A 50.8(7) .
F16A C10 F18A 102.5(9) .
F16B C10 F17B 110.1(11) .
F17A C10 F17B 43.0(7) .
F18B C10 F17B 98.5(9) .
F16A C10 F17B 79.7(9) .
F18A C10 F17B 141.5(9) .
F16B C10 C9 120.2(8) .
F17A C10 C9 117.7(7) .
F18B C10 C9 112.4(8) .
F16A C10 C9 114.6(8) .
F18A C10 C9 105.8(8) .
F17B C10 C9 108.0(7) .
N2 O8 Dy 143.0(3) 2
C14 O2 Dy 133.0(5) .
C11 O1 Dy 133.8(5) .
O1 C11 C13 128.2(7) .
O1 C11 C12 113.5(7) .
C13 C11 C12 118.4(6) .
O2 C14 C13 129.5(6) .
O2 C14 C15 112.5(7) .
C13 C14 C15 117.9(6) .
C14 C13 C11 121.0(6) .
F11 C15 F10 109.3(9) .
F11 C15 F12 107.1(7) .
F10 C15 F12 105.3(7) .
F11 C15 C14 110.9(6) .
F10 C15 C14 111.8(6) .
F12 C15 C14 112.1(8) .
F14 C12 F13 108.0(9) .
F14 C12 F15 107.2(8) .
F13 C12 F15 106.7(7) .
F14 C12 C11 110.1(7) .
F13 C12 C11 111.4(7) .
F15 C12 C11 113.2(8) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy O2 2.323(4) .
Dy O4 2.323(4) .
Dy O5 2.329(4) .
Dy O1 2.331(4) .
Dy O6 2.349(4) .
Dy O7 2.350(4) .
Dy O3 2.351(4) .
Dy O8 2.352(4) 2_545
O7 N1 1.261(6) .
O5 C7 1.272(7) .
O3 C5 1.240(7) .
F6 C4 1.322(8) .
F2 C1 1.335(7) .
C17 N1 1.334(7) .
C17 N2 1.342(7) .
C17 C16 1.483(9) .
F1 C1 1.322(7) .
C9 O6 1.238(7) .
C9 C8 1.373(9) .
C9 C10 1.508(11) .
F3 C1 1.331(8) .
O4 C2 1.265(7) .
N1 C19 1.498(8) .
N2 O8 1.279(6) .
N2 C18 1.514(8) .
C2 C3 1.412(9) .
C2 C1 1.522(9) .
F8 C6 1.312(8) .
F9 C6 1.340(9) .
F5 C4 1.309(8) .
C3 C5 1.393(9) .
C7 C8 1.368(9) .
C7 C6 1.551(10) .
C5 C4 1.540(8) .
F4 C4 1.315(8) .
F7 C6 1.290(9) .
C19 C23B 1.387(17) .
C19 C20A 1.444(14) .
C19 C18 1.543(9) .
C19 C23A 1.665(14) .
C19 C20B 1.693(18) .
C18 C22B 1.437(18) .
C18 C21A 1.451(15) .
C18 C22A 1.608(15) .
C18 C21B 1.670(19) .
C10 F16B 1.272(14) .
C10 F17A 1.301(14) .
C10 F18B 1.315(14) .
C10 F16A 1.352(15) .
C10 F18A 1.388(14) .
C10 F17B 1.417(14) .
O8 Dy 2.352(4) 2
O2 C14 1.233(8) .
O1 C11 1.232(7) .
C11 C13 1.392(10) .
C11 C12 1.530(11) .
C14 C13 1.388(11) .
C14 C15 1.547(10) .
F13 C12 1.320(9) .
F14 C12 1.316(10) .
F15 C12 1.326(9) .
C15 F11 1.306(10) .
C15 F10 1.312(9) .
C15 F12 1.337(10) .
