Crystallography Open Database

Information card for entry 1517764

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Coordinates	1517764.cif

Structure parameters

Formula	C52 H38 Cl4 N2 O4 P2 Pd
Calculated formula	C50 H38 N2 O4 P2 Pd
Title of publication	Monoanionic salicylaldimine ligands with (thio)phosphoryl pendant arms: Synthesis and complexing features
Authors of publication	Diana V. Aleksanyan; Valentina Yu. Aleksenko; Yulia V. Nelyubina; Andrei A. Vasil-ev; Rinat R. Aysin; Zinaida S. Klemenkova; Vladimir A. Kozlov; Pavel V. Petrovskii; Irina L. Odinets
Journal of publication	Inorganica Chimica Acta
Year of publication	2013
Journal volume	404
Pages of publication	167 - 174
a	8.3886 ± 0.0015 Å
b	11.599 ± 0.002 Å
c	14.078 ± 0.004 Å
α	105.217 ± 0.005°
β	105.536 ± 0.005°
γ	106.086 ± 0.004°
Cell volume	1181.2 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0559
Residual factor for significantly intense reflections	0.0427
Weighted residual factors for significantly intense reflections	0.0952
Weighted residual factors for all reflections included in the refinement	0.1022
Goodness-of-fit parameter for all reflections included in the refinement	1.002
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1517764.cif
123874	2014-09-16	cif/ Adding structures of 1517764 via cif-deposit CGI script.	1517764.cif