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Information card for entry 1517766
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Coordinates | 1517766.cif |
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Formula | C54 H54 N2 Ni O8 P2 |
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Calculated formula | C54 H52.8 N2 Ni O8 P2 |
Title of publication | Monoanionic salicylaldimine ligands with (thio)phosphoryl pendant arms: Synthesis and complexing features |
Authors of publication | Diana V. Aleksanyan; Valentina Yu. Aleksenko; Yulia V. Nelyubina; Andrei A. Vasil-ev; Rinat R. Aysin; Zinaida S. Klemenkova; Vladimir A. Kozlov; Pavel V. Petrovskii; Irina L. Odinets |
Journal of publication | Inorganica Chimica Acta |
Year of publication | 2013 |
Journal volume | 404 |
Pages of publication | 167 - 174 |
a | 9.4396 ± 0.0009 Å |
b | 11.8274 ± 0.0011 Å |
c | 12.3009 ± 0.0011 Å |
α | 61.711 ± 0.003° |
β | 76.08 ± 0.002° |
γ | 85.684 ± 0.002° |
Cell volume | 1172.6 ± 0.19 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.087 |
Residual factor for significantly intense reflections | 0.0485 |
Weighted residual factors for significantly intense reflections | 0.1018 |
Weighted residual factors for all reflections included in the refinement | 0.1181 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.002 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
176729 (current) | 2016-02-18 | cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1. |
1517766.cif |
123876 | 2014-09-16 | cif/ Adding structures of 1517766 via cif-deposit CGI script. |
1517766.cif |
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Users of the data should acknowledge the original authors of the
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