Crystallography Open Database

Information card for entry 1518477

Preview

Coordinates	1518477.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15 H22 F6 N O6 Pd Sb
Calculated formula	C15 H22 F6 N O6 Pd Sb
Title of publication	Bypassing the lack of reactivity of endo-substituted norbornenes with the catalytic rectification‒insertion mechanism
Authors of publication	Commarieu, Basile; Claverie, Jerome P.
Journal of publication	Chem. Sci.
Year of publication	2015
Journal volume	6
Journal issue	4
Pages of publication	2172
a	18.89 ± 0.005 Å
b	16.805 ± 0.004 Å
c	13.196 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	4189 ± 1.8 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	7
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0368
Residual factor for significantly intense reflections	0.0293
Weighted residual factors for significantly intense reflections	0.0711
Weighted residual factors for all reflections included in the refinement	0.0768
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1518477.cif
134905	2015-04-06	cif/ Updating files of 1518476, 1518477, 1518478, 1518479, 1518480 Original log message: Adding full bibliography for 1518476--1518480.cif.	1518477.cif
129056	2014-12-25	cif/ Adding structures of 1518476, 1518477, 1518478, 1518479, 1518480 via cif-deposit CGI script.	1518477.cif