Crystallography Open Database

Information card for entry 1520220

1520219 << 1520220 >> 1520221

Preview

Coordinates	1520220.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H19 N
Calculated formula	C24 H19 N
Title of publication	Synthesis of Multiple-Substituted Pyrroles via Gold(I)-Catalyzed Hydroamination/Cyclization Cascade.
Authors of publication	Li, Xiangdong; Chen, Ming; Xie, Xin; Sun, Ning; Li, Shi; Liu, Yuanhong
Journal of publication	Organic letters
Year of publication	2015
Journal volume	17
Journal issue	12
Pages of publication	2984 - 2987
a	42.784 ± 0.004 Å
b	6.0454 ± 0.0006 Å
c	31.552 ± 0.003 Å
α	90°
β	119.951 ± 0.002°
γ	90°
Cell volume	7071 ± 1.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	3
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0862
Residual factor for significantly intense reflections	0.0594
Weighted residual factors for significantly intense reflections	0.1526
Weighted residual factors for all reflections included in the refinement	0.1703
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
140265 (current)	2015-07-05	cif/ Updating files of 1520220, 1520221, 1520222 Original log message: Adding full bibliography for 1520220--1520222.cif.	1520220.cif
137799	2015-06-04	cif/ Adding structures of 1520220 via cif-deposit CGI script.	1520220.cif