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Information card for entry 1520304
Preview
| Coordinates | 1520304.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C66.33 H81.67 N2 O4 Yb |
|---|---|
| Calculated formula | C66.3333 H81.6667 N2 O4 Yb |
| Title of publication | Highly Enantioselective Epoxidation of α,β-Unsaturated Ketones Catalyzed by Rare-Earth Amides [(Me3Si)2N]3RE(μ-Cl)Li(THF)3 with Phenoxy-Functionalized Chiral Prolinols. |
| Authors of publication | Zeng, Chao; Yuan, Dan; Zhao, Bei; Yao, Yingming |
| Journal of publication | Organic letters |
| Year of publication | 2015 |
| Journal volume | 17 |
| Journal issue | 9 |
| Pages of publication | 2242 - 2245 |
| a | 15.592 ± 0.0006 Å |
| b | 20.5827 ± 0.0003 Å |
| c | 60.065 ± 0.0012 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 19276.4 ± 0.9 Å3 |
| Cell temperature | 295 ± 2 K |
| Ambient diffraction temperature | 295 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0944 |
| Residual factor for significantly intense reflections | 0.071 |
| Weighted residual factors for significantly intense reflections | 0.1658 |
| Weighted residual factors for all reflections included in the refinement | 0.1855 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.002 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 138031 (current) | 2015-06-05 | cif/ Adding structures of 1520304 via cif-deposit CGI script. |
1520304.cif |
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