Crystallography Open Database

Information card for entry 1520570

1520569 << 1520570 >> 1520571

Preview

Coordinates	1520570.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C11 H19 N O4
Title of publication	Electro-organic Synthesis 68. Diastereoselective Cathodic Reduction of Phenylglyoxylic Acid Attached to Chiral Auxiliaries
Authors of publication	Reufer, Christian; Zielinski, Claudia; Schafer, Hans Jurgen; Frolich, Roland
Journal of publication	Acta Chemica Scandinavica
Year of publication	1999
Journal volume	53
Pages of publication	1023 - 1037
a	7.269 ± 0.001 Å
b	10.484 ± 0.001 Å
c	8.094 ± 0.001 Å
α	90°
β	99.41 ± 0.01°
γ	90°
Cell volume	608.53 ± 0.13 Å³
Ambient diffraction temperature	198 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for significantly intense reflections	0.035
Weighted residual factors for significantly intense reflections	0.091
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	No
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	1520570.cif
175419	2016-02-02	cif/ Replacing parameters of a dummy hydrogen atom with question mark in order for the structure to be identified as having no coordinates.	1520570.cif
139328	2015-06-18	cif/ Adding structures of 1520570 via cif-deposit CGI script.	1520570.cif