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Information card for entry 1520632
Preview
| Coordinates | 1520632.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C16 H44.4 N6 O13.2 Re3 Rh |
|---|---|
| Calculated formula | C16 N6 O13.2 Re3 Rh |
| Title of publication | Mononuclear Rhodium(III) Complexes with N,N',N"-Trimethyl-1,1,1- tris(aminomethyl)ethane (Me3-tame). Preparations, Characterization and Configurational Isomerization. Crystal Structure of meso-[Rh(Me3-tame)2](ReO4)3.1.2H2O. |
| Authors of publication | Andersen, Peter; Galsbol, Frode; Jensen, Anette Frost; Matsui, Hayato; Monsted, Lene; Simonsen, Kim |
| Journal of publication | Acta Chemica Scandinavica |
| Year of publication | 1999 |
| Journal volume | 53 |
| Pages of publication | 1093 - 1102 |
| a | 10.184 ± 0.002 Å |
| b | 17.559 ± 0.004 Å |
| c | 9.161 ± 0.004 Å |
| α | 90.68 ± 0.03° |
| β | 112.57 ± 0.03° |
| γ | 87.78 ± 0.02° |
| Cell volume | 1511.6 ± 0.9 Å3 |
| Ambient diffraction temperature | 122 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for significantly intense reflections | 0.0386 |
| Weighted residual factors for significantly intense reflections | 0.0982 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.2 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 139504 (current) | 2015-06-23 | cif/ Adding structures of 1520632 via cif-deposit CGI script. |
1520632.cif |
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