Crystallography Open Database

Information card for entry 1520689

1520688 << 1520689 >> 1520690

Preview

Coordinates	1520689.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H23 N O4
Calculated formula	C19 N O4
Title of publication	Reactions of Myrtenylzinc Bromide with Carbonyl Compounds. Regio- and Diastereo-selectivity
Authors of publication	Aukrust, Inger Reidun; Nilsen, Nils Olav; Romming, Christian; Skattebol, Lars
Journal of publication	Acta Chemica Scandinavica
Year of publication	1998
Journal volume	52
Pages of publication	385 - 390
a	7.002 ± 0.001 Å
b	6.637 ± 0.002 Å
c	19.154 ± 0.002 Å
α	90°
β	95.42 ± 0.02°
γ	90°
Cell volume	886.2 ± 0.3 Å³
Ambient diffraction temperature	138 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for significantly intense reflections	0.0649
Weighted residual factors for significantly intense reflections	0.1441
Goodness-of-fit parameter for all reflections included in the refinement	0.938
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.7093 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	1520689.cif
139752	2015-06-29	cif/ Adding structures of 1520689 via cif-deposit CGI script.	1520689.cif