#------------------------------------------------------------------------------ #$Date: 2016-04-06 15:35:39 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181862 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/52/92/1529230.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1529230 _cell_angle_alpha 90.000 _cell_angle_beta 110.003 _cell_angle_gamma 90.000 _cell_length_a 14.1033 _cell_length_b 10.0988 _cell_length_c 15.4061 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.6096 _cod_data_source_file EuHTBA3H2O3.fcf _cod_data_source_block z #BEGIN Tags that were not found in dictionaries: _shelx_title ' m in P2/n at room T Bruker X8 Apex' _shelx_refln_list_code 4 _shelx_f_calc_maximum 408.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 39901.29 38550.02 861.84 o 4 0 0 45249.27 43490.93 1129.20 o 6 0 0 33118.32 32250.40 850.56 o 8 0 0 8007.73 7956.02 437.23 o 10 0 0 8386.13 7720.97 271.63 o 12 0 0 7034.21 6754.94 275.39 o 14 0 0 7684.32 7621.41 459.91 o 16 0 0 8772.45 8308.36 515.50 o 18 0 0 7733.82 7460.75 496.17 o 20 0 0 8622.46 8196.05 555.28 o 0 1 0 8790.33 8910.33 288.45 o 1 1 0 18090.78 18868.38 320.65 o 2 1 0 718.93 605.82 16.93 o 3 1 0 33693.58 32836.27 522.34 o 4 1 0 728.56 814.00 29.84 o 5 1 0 15458.43 14900.88 285.55 o 6 1 0 180.33 171.25 17.90 o 7 1 0 55260.23 55317.98 1020.73 o 8 1 0 1683.24 1536.41 50.51 o 9 1 0 17808.13 16716.61 330.74 o 10 1 0 510.11 564.54 42.48 o 11 1 0 25433.18 23017.34 777.90 o 12 1 0 163.86 176.18 39.42 o 13 1 0 13715.79 14146.30 526.39 o 14 1 0 15.97 51.31 45.83 o 15 1 0 4399.16 4456.47 230.90 o 16 1 0 18.74 69.14 53.83 o 17 1 0 3913.34 4010.48 230.77 o 18 1 0 4.57 60.79 66.18 o 19 1 0 1190.39 838.24 127.94 o 20 1 0 5.31 5.70 112.31 o 21 1 0 1554.46 1604.06 377.31 o 0 2 0 11797.79 11815.34 273.65 o 1 2 0 1546.71 1864.15 44.40 o 2 2 0 255.00 188.45 13.21 o 3 2 0 656.28 918.69 28.19 o 4 2 0 17572.70 18074.28 361.88 o 5 2 0 505.01 420.37 24.72 o 6 2 0 1260.23 1258.42 42.25 o 7 2 0 913.25 746.58 37.06 o 8 2 0 3643.83 3818.39 121.32 o 9 2 0 165.61 157.30 21.86 o 10 2 0 8893.31 8174.36 292.33 o 11 2 0 451.38 452.41 43.18 o 12 2 0 2312.12 2245.37 93.62 o 13 2 0 252.30 147.16 97.91 o 14 2 0 4335.87 4101.60 213.70 o 15 2 0 510.59 449.54 84.83 o 16 2 0 2468.02 2420.68 189.70 o 17 2 0 50.22 -15.20 52.80 o 18 2 0 221.35 245.13 87.31 o 19 2 0 394.07 244.83 86.56 o 20 2 0 623.73 859.79 210.86 o 21 2 0 188.75 85.73 75.58 o 0 3 0 17598.90 17571.96 406.43 o 1 3 0 1320.56 1476.61 36.64 o 2 3 0 1221.65 1114.16 33.94 o 3 3 0 568.36 730.85 49.96 o 4 3 0 649.92 955.99 34.88 o 5 3 0 8767.55 8450.18 173.80 o 6 3 0 2393.59 2330.24 70.01 o 7 3 0 609.12 501.62 36.98 o 8 3 0 297.83 335.17 31.22 o 9 3 0 1715.31 1723.34 64.66 o 10 3 0 557.02 576.35 42.36 o 11 3 0 9450.88 9255.03 251.33 o 12 3 0 51.40 65.67 32.78 o 13 3 0 368.32 447.35 81.68 o 14 3 0 95.04 143.57 56.78 o 15 3 0 1374.37 1517.47 144.34 o 16 3 0 75.03 -0.33 58.01 o 17 3 0 666.08 659.68 107.22 o 18 3 0 50.11 60.12 63.90 o 19 3 0 50.93 112.27 70.15 o 20 3 0 2.43 -62.30 62.30 o 21 3 0 16.95 80.04 109.85 o 0 4 0 18404.38 17845.56 482.88 o 1 4 0 3745.12 3924.21 98.75 o 2 4 0 4741.22 4234.97 117.93 o 3 4 0 2137.20 2102.26 63.70 o 4 4 0 17620.36 17515.32 371.07 o 5 4 0 904.56 1128.76 46.59 o 6 4 0 16840.71 17611.42 377.29 o 7 4 0 331.13 322.32 30.54 o 8 4 0 12627.69 13137.98 294.21 o 9 4 0 1773.46 1606.91 65.29 o 10 4 0 10911.39 10370.03 250.77 o 11 4 0 86.71 82.04 34.98 o 12 4 0 8160.68 8016.40 322.35 o 13 4 0 650.27 635.88 89.51 o 14 4 0 5626.70 5715.24 271.54 o 15 4 0 89.16 34.10 50.42 o 16 4 0 3155.42 2964.36 437.64 o 17 4 0 453.09 408.19 94.68 o 18 4 0 3481.23 3607.35 229.35 o 19 4 0 150.46 66.55 76.60 o 20 4 0 1948.83 1888.93 272.87 o 21 4 0 5.41 6.65 65.12 o 0 5 0 396.79 427.07 79.96 o 1 5 0 36255.21 35075.47 720.47 o 2 5 0 9.58 25.24 17.99 o 3 5 0 38385.02 39059.28 801.34 o 4 5 0 10906.00 11609.46 258.61 o 5 5 0 31371.36 31024.31 645.13 o 6 5 0 2979.16 2972.71 89.34 o 7 5 0 13903.51 13359.12 308.46 o 8 5 0 3280.62 3299.82 100.43 o 9 5 0 7168.49 7244.55 182.80 o 10 5 0 2215.61 2254.07 93.29 o 11 5 0 12047.84 11635.05 509.03 o 12 5 0 2290.03 2079.20 117.58 o 13 5 0 2592.60 2549.88 162.26 o 14 5 0 1506.23 1471.47 144.07 o 15 5 0 5887.30 6155.61 298.96 o 16 5 0 1766.75 1867.42 173.06 o 17 5 0 4062.74 3874.11 235.63 o 18 5 0 51.03 76.49 71.09 o 19 5 0 3440.93 3698.39 296.31 o 20 5 0 170.85 46.11 84.85 o 0 6 0 20219.54 20148.51 683.07 o 1 6 0 8816.30 9299.09 242.41 o 2 6 0 16130.62 16163.18 481.15 o 3 6 0 6574.14 6504.82 181.28 o 4 6 0 12248.38 11918.39 296.03 o 5 6 0 692.68 872.80 51.22 o 6 6 0 6609.24 6588.72 166.97 o 7 6 0 2588.02 2630.81 89.71 o 8 6 0 12710.18 12118.33 361.20 o 9 6 0 396.97 429.76 46.96 o 10 6 0 12967.73 12143.03 378.21 o 11 6 0 51.38 20.53 32.49 o 12 6 0 5745.50 5648.10 215.95 o 13 6 0 1151.19 1160.84 163.22 o 14 6 0 3584.97 3500.86 208.17 o 15 6 0 292.14 248.70 74.04 o 16 6 0 2485.76 2583.19 210.65 o 17 6 0 225.13 142.42 73.97 o 18 6 0 2906.40 2816.51 234.38 o 19 6 0 1144.83 1497.18 174.67 o 20 6 0 1048.64 965.42 191.72 o 0 7 0 18849.21 19842.02 683.13 o 1 7 0 587.30 608.75 50.63 o 2 7 0 193.60 325.26 49.74 o 3 7 0 1338.96 1515.28 79.50 o 4 7 0 682.51 798.69 58.26 o 5 7 0 134.23 99.34 30.16 o 6 7 0 5.51 19.86 24.23 o 7 7 0 2867.33 3091.09 115.42 o 8 7 0 172.79 191.51 35.05 o 9 7 0 3136.76 2965.96 137.18 o 10 7 0 1395.78 1227.40 98.75 o 11 7 0 1773.49 1535.21 112.61 o 12 7 0 5.60 22.42 47.43 o 13 7 0 1081.26 1082.51 125.21 o 14 7 0 481.44 414.19 135.48 o 15 7 0 1196.72 1171.33 138.19 o 16 7 0 467.35 377.21 223.09 o 17 7 0 321.57 313.45 96.29 o 18 7 0 125.62 130.02 77.47 o 19 7 0 269.23 222.69 95.33 o 0 8 0 2765.85 2951.27 159.13 o 1 8 0 1643.25 1645.67 82.78 o 2 8 0 908.14 944.41 64.58 o 3 8 0 195.74 199.87 56.80 o 4 8 0 9.46 -10.37 24.82 o 5 8 0 3032.49 2865.12 110.99 o 6 8 0 1493.94 1647.41 92.31 o 7 8 0 1961.49 1843.03 96.09 o 8 8 0 468.34 514.40 69.44 o 9 8 0 211.89 213.78 49.64 o 10 8 0 1547.21 1551.96 116.80 o 11 8 0 135.25 98.95 44.94 o 12 8 0 656.13 649.05 103.13 o 13 8 0 895.35 853.19 117.56 o 14 8 0 576.85 719.45 113.52 o 15 8 0 1.50 -53.57 53.57 o 16 8 0 368.61 381.74 99.39 o 17 8 0 29.36 149.23 94.72 o 18 8 0 46.52 55.46 74.95 o 19 8 0 255.14 335.35 98.42 o 0 9 0 2169.88 2062.91 142.03 o 1 9 0 9628.92 9786.55 314.19 o 2 9 0 2134.65 2223.39 102.35 o 3 9 0 5467.79 5640.65 200.87 o 4 9 0 613.21 638.18 60.11 o 5 9 0 5305.71 5389.05 177.02 o 6 9 0 1853.86 1805.71 103.05 o 7 9 0 1847.89 1824.33 121.85 o 8 9 0 2829.22 2869.78 144.40 o 9 9 0 5335.82 4865.50 201.72 o 10 9 0 1007.34 893.84 94.19 o 11 9 0 4934.99 5186.02 266.49 o 12 9 0 1737.01 1665.24 159.93 o 13 9 0 1921.18 1821.43 170.45 o 14 9 0 383.60 394.73 98.37 o 15 9 0 3713.67 3760.64 303.90 o 16 9 0 626.26 645.44 120.03 o 17 9 0 2366.73 2483.84 227.32 o 18 9 0 73.34 123.24 77.96 o 0 10 0 2852.52 3259.86 182.54 o 1 10 0 2361.64 2500.48 110.45 o 2 10 0 10619.69 10737.10 301.95 o 3 10 0 511.41 616.55 65.14 o 4 10 0 7860.83 8104.31 243.68 o 5 10 0 3903.94 3965.87 149.15 o 6 10 0 9379.74 9248.74 317.09 o 7 10 0 1144.44 1519.26 158.88 o 8 10 0 7737.04 7897.98 288.24 o 9 10 0 4261.91 4327.37 193.65 o 10 10 0 6648.25 6663.75 261.60 o 11 10 0 3183.22 3451.44 217.61 o 12 10 0 5402.09 5566.08 373.39 o 13 10 0 970.28 968.00 143.97 o 14 10 0 3221.82 3547.85 248.49 o 15 10 0 1842.27 1560.94 348.69 o 16 10 0 991.40 1237.44 165.85 o 17 10 0 377.84 346.63 102.73 o 0 11 0 1045.91 890.28 150.70 o 1 11 0 9891.46 9661.51 284.31 o 2 11 0 6445.02 6279.97 207.31 o 3 11 0 5215.20 4963.28 177.99 o 4 11 0 3641.77 3751.76 173.55 o 5 11 0 4932.89 5034.76 210.74 o 6 11 0 1384.85 1405.43 119.98 o 7 11 0 2956.12 3050.60 159.74 o 8 11 0 768.62 899.03 100.27 o 9 11 0 1373.75 1213.60 114.20 o 10 11 0 268.78 193.92 81.03 o 11 11 0 1899.76 2039.11 188.64 o 12 11 0 400.87 333.41 90.26 o 13 11 0 1439.92 1511.12 284.30 o 14 11 0 703.64 571.04 116.83 o 15 11 0 1607.57 1401.14 173.93 o 16 11 0 311.37 37.92 134.36 o 0 12 0 572.34 569.86 115.08 o 1 12 0 82.21 128.58 51.67 o 2 12 0 1516.14 1448.55 122.78 o 3 12 0 470.03 684.67 88.30 o 4 12 0 368.41 398.01 70.84 o 5 12 0 659.31 647.83 88.33 o 6 12 0 40.53 114.28 51.35 o 7 12 0 351.76 372.34 74.84 o 8 12 0 976.17 1000.66 107.47 o 9 12 0 211.38 137.67 73.27 o 10 12 0 609.13 640.60 117.84 o 11 12 0 369.90 219.80 81.63 o 12 12 0 553.65 856.90 157.71 o 13 12 0 158.14 117.73 81.13 o 14 12 0 137.53 145.45 98.86 o 0 13 0 665.08 598.36 151.96 o 1 13 0 873.19 1147.92 146.94 o 2 13 0 1019.56 908.16 127.95 o 3 13 0 784.55 907.39 141.23 o 4 13 0 369.01 358.23 77.05 o 5 13 0 225.89 180.12 64.52 o 6 13 0 560.10 712.55 96.44 o 7 13 0 10.51 87.32 58.26 o 8 13 0 50.98 85.91 59.31 o 9 13 0 26.95 85.25 74.41 o 10 13 0 93.89 9.96 91.34 o 11 13 0 46.89 66.07 111.49 o 12 13 0 80.91 64.83 77.92 o 13 13 0 28.42 80.97 79.79 o 0 14 0 1174.19 1310.88 223.63 o 1 14 0 576.87 507.60 110.92 o 2 14 0 353.64 206.66 79.40 o 3 14 0 907.09 905.28 132.32 o 4 14 0 1256.48 1304.82 230.32 o 5 14 0 1713.10 1756.33 377.33 o 6 14 0 2026.33 2243.49 172.39 o 7 14 0 1750.41 1692.29 173.01 o 8 14 0 1258.99 1198.47 162.91 o 9 14 0 1989.23 1946.12 202.24 o 10 14 0 1777.32 1644.51 187.72 o 11 14 0 1026.86 1166.68 275.25 o 0 15 0 2347.27 2600.09 336.73 o 1 15 0 2957.11 2815.08 252.61 o 2 15 0 3486.42 3520.21 271.34 o 3 15 0 1015.44 838.93 152.62 o 4 15 0 1954.19 1866.58 200.23 o 5 15 0 1045.05 1065.23 398.35 o 6 15 0 1914.50 1701.10 217.58 o 7 15 0 2901.55 3486.00 401.82 o 8 15 0 992.49 772.70 200.31 o 9 15 0 1566.82 1310.30 238.62 o 0 16 0 2906.05 3582.24 414.25 o 1 16 0 2548.34 2586.71 243.78 o 2 16 0 1564.10 2155.42 420.51 o 3 16 0 1144.01 916.36 195.73 o 4 16 0 1849.88 1241.31 167.26 o 5 16 0 1511.16 1411.60 263.70 o -21 0 1 339.98 230.05 127.76 o -19 0 1 48.79 30.64 90.90 o -17 0 1 247.54 297.14 102.40 o -15 0 1 57.05 132.50 77.28 o -13 0 1 112.04 153.68 69.90 o -11 0 1 1140.63 1067.83 67.84 o -9 0 1 3792.02 3751.75 130.36 o -7 0 1 927.27 1254.85 57.19 o -5 0 1 4286.53 4877.14 174.81 o -3 0 1 17944.02 17394.43 452.26 o 1 0 1 1348.18 1135.47 34.79 o 3 0 1 2836.62 2349.13 69.67 o 5 0 1 5860.44 4960.54 153.92 o 7 0 1 3830.80 3903.75 155.41 o 9 0 1 3042.85 2785.87 153.22 o 11 0 1 70.16 54.40 37.71 o 13 0 1 1220.04 1177.45 167.01 o 15 0 1 807.22 791.14 154.04 o 17 0 1 999.64 1388.11 218.59 o 19 0 1 108.82 -5.16 91.02 o 21 0 1 694.74 459.63 152.21 o -21 1 1 786.13 1097.47 151.02 o -20 1 1 6.44 4.34 65.54 o -19 1 1 431.62 527.73 100.45 o -18 1 1 0.82 3.52 54.12 o -17 1 1 1351.11 1309.95 137.80 o -16 1 1 173.84 177.24 77.52 o -15 1 1 1712.96 1319.21 213.19 o -14 1 1 2.78 32.35 40.84 o -13 1 1 1091.19 1372.27 118.96 o -12 1 1 48.88 75.67 41.16 o -11 1 1 13679.58 12662.24 286.20 o -10 1 1 380.61 442.48 31.17 o -9 1 1 21180.23 20387.02 461.37 o -8 1 1 82.13 177.21 18.55 o -7 1 1 15986.88 14536.16 281.29 o -6 1 1 3713.47 4060.55 97.68 o -5 1 1 28621.67 27369.02 555.89 o -4 1 1 586.48 581.06 24.38 o -3 1 1 16641.08 16967.87 272.42 o -2 1 1 9918.17 9052.53 156.63 o -1 1 1 13824.57 14469.90 246.83 o 0 1 1 719.99 793.75 17.53 o 1 1 1 35645.40 35457.65 561.32 o 2 1 1 1268.74 1131.62 31.41 o 3 1 1 779.39 644.75 23.61 o 4 1 1 3681.56 4249.13 143.92 o 5 1 1 2607.16 2359.34 67.24 o 6 1 1 35.77 78.49 16.35 o 7 1 1 5982.22 5985.82 133.58 o 8 1 1 518.54 487.48 33.11 o 9 1 1 5838.56 5727.91 250.64 o 10 1 1 2107.04 2030.96 79.51 o 11 1 1 5708.84 5699.66 172.46 o 12 1 1 952.62 933.80 66.83 o 13 1 1 8103.16 8065.45 340.33 o 14 1 1 578.62 653.69 98.36 o 15 1 1 5779.47 5821.68 283.80 o 16 1 1 100.06 -21.20 52.29 o 17 1 1 2540.35 2477.65 203.21 o 18 1 1 45.68 105.32 66.25 o 19 1 1 1158.67 1014.65 156.23 o 20 1 1 100.83 28.88 69.32 o 21 1 1 910.40 1022.26 150.31 o -21 2 1 96.73 -27.23 64.22 o -20 2 1 5049.45 5463.46 507.25 o -19 2 1 141.80 184.20 74.14 o -18 2 1 6373.84 6419.49 314.21 o -17 2 1 67.75 135.10 63.98 o -16 2 1 8699.84 8809.38 376.02 o -15 2 1 40.28 -23.69 42.53 o -14 2 1 16016.50 15357.12 567.35 o -13 2 1 372.16 406.70 69.41 o -12 2 1 6371.11 6156.92 179.87 o -11 2 1 8498.26 7803.84 227.61 o -10 2 1 14510.58 14014.85 282.95 o -9 2 1 1093.86 1072.37 53.07 o -8 2 1 13346.99 12610.70 259.19 o -7 2 1 3.62 -10.61 10.61 o -6 2 1 19798.32 19598.89 450.36 o -5 2 1 1895.73 2347.41 63.60 o -4 2 1 32500.47 33173.42 670.56 o -3 2 1 471.50 488.28 21.24 o -2 2 1 26453.91 27235.54 435.28 o -1 2 1 236.63 210.66 13.02 o 0 2 1 46132.80 44577.69 753.72 o 1 2 1 2938.59 2784.17 54.07 o 2 2 1 78787.76 76968.71 1213.80 o 3 2 1 136.17 87.69 13.64 o 4 2 1 36826.95 36822.30 683.57 o 5 2 1 311.09 278.96 22.92 o 6 2 1 59822.64 57745.84 1342.52 o 7 2 1 2435.10 2367.28 71.31 o 8 2 1 12631.43 12471.78 423.85 o 9 2 1 1300.39 1487.65 65.21 o 10 2 1 9561.97 9261.68 276.86 o 11 2 1 55.96 9.35 23.85 o 12 2 1 12525.35 11624.58 376.40 o 13 2 1 62.58 17.18 44.56 o 14 2 1 4156.03 3605.40 202.89 o 15 2 1 560.81 758.67 138.14 o 16 2 1 4342.88 4245.59 269.32 o 17 2 1 0.65 80.78 65.11 o 18 2 1 4913.00 4990.04 277.74 o 19 2 1 258.84 261.36 89.56 o 20 2 1 2352.25 2298.36 301.01 o 21 2 1 3.80 -23.85 78.86 o -21 3 1 3466.27 3567.39 262.88 o -20 3 1 174.29 305.69 90.13 o -19 3 1 3911.94 3738.06 554.80 o -18 3 1 425.88 510.68 96.19 o -17 3 1 5802.82 5590.79 281.51 o -16 3 1 208.67 192.94 216.00 o -15 3 1 11497.72 11089.30 443.21 o -14 3 1 131.97 90.89 52.44 o -13 3 1 9479.47 10284.76 402.30 o -12 3 1 115.18 84.60 32.23 o -11 3 1 16113.86 15094.11 494.50 o -10 3 1 3049.92 2908.95 81.29 o -9 3 1 7516.36 7055.36 184.73 o -8 3 1 227.71 213.47 22.72 o -7 3 1 23995.73 23296.88 443.97 o -6 3 1 40.28 -0.90 11.55 o -5 3 1 40400.13 40736.71 754.79 o -4 3 1 5337.44 5387.70 147.10 o -3 3 1 35175.80 35033.61 648.87 o -2 3 1 150.34 140.84 15.47 o -1 3 1 17183.76 16432.09 288.68 o 0 3 1 1141.43 1147.82 31.15 o 1 3 1 23912.45 22762.05 395.10 o 2 3 1 10086.98 10229.82 186.67 o 3 3 1 54216.18 55032.92 1012.50 o 4 3 1 406.05 388.87 32.38 o 5 3 1 47663.84 48453.57 984.60 o 6 3 1 6.18 11.61 15.11 o 7 3 1 23946.08 23787.96 583.80 o 8 3 1 404.33 310.17 45.88 o 9 3 1 17890.39 17349.54 463.89 o 10 3 1 3052.63 2843.56 94.22 o 11 3 1 10862.24 10450.59 282.04 o 12 3 1 1099.74 1100.95 90.86 o 13 3 1 8087.72 7385.34 322.07 o 14 3 1 100.50 31.99 50.95 o 15 3 1 6148.59 6488.73 308.56 o 16 3 1 434.63 326.34 83.93 o 17 3 1 4122.79 3983.19 241.90 o 18 3 1 9.92 -22.11 58.04 o 19 3 1 3198.33 3706.55 274.68 o 20 3 1 10.22 25.09 75.02 o 21 3 1 1754.64 2027.66 212.13 o -21 4 1 485.37 554.49 111.63 o -20 4 1 457.72 436.18 135.92 o -19 4 1 239.87 154.73 72.55 o -18 4 1 1352.15 1737.22 172.51 o -17 4 1 929.68 859.76 118.56 o -16 4 1 744.99 680.63 102.72 o -15 4 1 2040.38 1969.67 257.79 o -14 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