data_1529491 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_length_a 9.85508(31) _cell_length_b 9.85508(31) _cell_length_c 7.30235(24) _cod_data_source_file La6Sr4SiO46F2_Ce_Tb.fcf _cod_data_source_block a _shelx_f_squared_multiplier 1 loop_ _symmetry_equiv_pos_as_xyz '-x, -y, -z' '-x, -y, z+1/2' '-x+y, -x, -z+1/2' '-x+y, -x, z' '-y, x-y, -z+1/2' '-y, x-y, z' 'y, -x+y, -z' 'y, -x+y, z+1/2' 'x-y, x, -z' 'x-y, x, z+1/2' 'x, y, -z+1/2' 'x, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc 0 1 0 0.08 0.08 180.00000 0 1 1 0.03 0.03 180.00000 1 1 0 2.35 2.25 0.00000 0 2 0 9.28 9.17 180.00000 1 1 1 8.43 8.22 180.00000 0 2 1 0.12 0.12 0.00000 0 0 2 4.89 4.81 180.00000 0 1 2 17.88 19.87 180.00000 2 1 0 15.07 15.42 180.00000 1 2 0 6.43 6.58 180.00000 2 1 1 42.14 41.56 180.00000 1 2 1 20.80 20.51 180.00000 1 1 2 44.61 42.62 0.00000 0 3 0 30.05 29.65 0.00000 0 2 2 2.22 2.48 180.00000 0 3 1 0.03 0.02 180.00000 2 2 0 1.49 1.72 0.00000 2 1 2 0.09 0.07 180.00000 1 2 2 0.01 0.01 180.00000 3 1 0 2.58 2.45 180.00000 1 3 0 4.52 4.30 0.00000 0 1 3 0.03 0.03 180.00000 2 2 1 1.61 1.64 180.00000 3 1 1 0.44 0.42 180.00000 1 3 1 0.39 0.37 0.00000 0 3 2 8.84 8.17 0.00000 1 1 3 16.60 15.09 0.00000 0 4 0 6.22 6.16 0.00000 0 2 3 2.06 2.01 180.00000 0 4 1 0.25 0.26 180.00000 2 2 2 45.87 43.70 0.00000 3 1 2 8.63 8.77 180.00000 1 3 2 25.01 25.40 180.00000 3 2 0 4.33 4.08 180.00000 2 3 0 6.70 6.32 180.00000 2 1 3 31.45 32.13 0.00000 1 2 3 17.62 18.00 0.00000 3 2 1 17.30 17.51 0.00000 2 3 1 11.25 11.39 0.00000 1 4 0 30.93 29.57 0.00000 4 1 0 14.13 13.51 0.00000 0 3 3 0.02 0.02 0.00000 0 4 2 51.00 52.37 180.00000 0 0 4 25.16 24.18 0.00000 1 4 1 0.00 0.00 0.00000 4 1 1 1.19 1.18 0.00000 0 1 4 0.11 0.09 180.00000 2 2 3 0.26 0.28 0.00000 3 2 2 2.21 2.54 180.00000 2 3 2 0.93 1.07 180.00000 1 1 4 4.47 4.60 0.00000 0 5 0 0.62 0.59 0.00000 3 1 3 0.37 0.31 180.00000 1 3 3 0.46 0.38 180.00000 0 2 4 8.99 7.94 180.00000 0 5 1 0.03 0.03 0.00000 1 4 2 0.02 0.02 180.00000 4 1 2 6.32 6.21 0.00000 3 3 0 1.17 1.10 0.00000 4 2 0 5.55 5.57 180.00000 2 4 0 7.62 7.65 180.00000 0 4 3 0.13 0.13 0.00000 3 3 1 17.26 16.43 0.00000 2 1 4 16.11 14.58 180.00000 1 2 4 12.62 11.41 180.00000 4 2 1 2.34 2.34 0.00000 2 4 1 1.97 1.96 180.00000 0 5 2 27.70 28.08 180.00000 0 3 4 25.12 25.90 0.00000 5 1 0 6.74 6.96 180.00000 1 5 0 1.77 1.82 180.00000 3 2 3 17.07 18.09 180.00000 2 3 3 4.54 4.81 180.00000 5 1 1 11.90 12.43 180.00000 1 5 1 3.87 4.04 180.00000 3 3 2 28.74 30.45 0.00000 4 1 3 0.90 0.88 180.00000 1 4 3 0.02 0.02 180.00000 4 2 2 0.66 0.62 0.00000 2 4 2 0.04 0.04 180.00000 2 2 4 2.14 2.39 0.00000 3 1 4 1.42 1.39 180.00000 1 3 4 0.58 0.57 0.00000 0 1 5 0.01 0.01 0.00000 0 6 0 1.59 1.52 0.00000 1 5 2 2.07 1.95 180.00000 5 1 2 0.17 0.16 0.00000 4 3 0 0.22 0.22 180.00000 3 4 0 0.65 0.67 180.00000 1 1 5 4.00 4.07 180.00000 0 5 3 1.29 1.32 180.00000 0 6 1 1.34 1.38 0.00000 0 4 4 6.52 7.35 0.00000 0 2 5 0.02 0.02 0.00000 4 3 1 4.70 4.21 0.00000 3 4 1 0.84 0.75 180.00000 2 5 0 0.94 0.86 0.00000 5 2 0 8.47 7.72 0.00000 3 3 3 10.76 9.97 180.00000 4 2 3 1.69 1.73 180.00000 2 4 3 3.11 3.19 0.00000 5 2 1 4.81 4.83 180.00000 2 5 1 11.04 11.11 180.00000 3 2 4 4.96 4.73 180.00000 2 3 4 6.19 5.90 180.00000 2 1 5 19.55 19.09 180.00000 1 2 5 8.92 8.71 180.00000 0 6 2 21.73 21.20 0.00000 4 3 2 5.02 5.48 180.00000 3 4 2 5.45 5.95 180.00000 4 1 4 16.44 17.35 0.00000 1 4 4 38.33 40.47 0.00000 6 1 0 7.84 7.97 180.00000 1 6 0 4.58 4.66 180.00000 0 3 5 0.03 0.03 0.00000 1 5 3 3.27 3.11 0.00000 5 1 3 10.40 9.89 0.00000 1 6 1 5.67 5.64 180.00000 6 1 1 12.81 12.73 180.00000 2 5 2 33.28 32.56 0.00000 5 2 2 9.77 9.56 0.00000 2 2 5 1.00 0.89 180.00000 0 5 4 1.87 1.75 0.00000 3 1 5 0.03 0.03 180.00000 1 3 5 0.12 0.11 0.00000 4 4 0 23.28 23.89 0.00000 0 6 3 0.89 0.89 180.00000 6 1 2 0.19 0.18 0.00000 1 6 2 0.26 0.26 0.00000 3 3 4 1.61 1.59 0.00000 5 3 0 0.97 0.96 0.00000 3 5 0 0.59 0.58 180.00000 0 7 0 0.88 0.88 180.00000 0 0 6 2.14 2.08 180.00000 4 3 3 4.60 4.41 180.00000 3 4 3 0.39 0.38 0.00000 4 4 1 0.63 0.60 180.00000 4 2 4 12.82 12.01 180.00000 2 4 4 9.26 8.67 180.00000 0 4 5 0.14 0.13 180.00000 0 1 6 8.90 8.29 180.00000 5 3 1 0.49 0.46 180.00000 3 5 1 1.36 1.27 180.00000 0 7 1 1.54 1.44 0.00000 2 5 3 9.73 9.23 0.00000 5 2 3 4.36 4.13 0.00000 6 2 0 2.55 2.23 180.00000 2 6 0 3.89 3.41 180.00000 1 1 6 24.13 21.54 0.00000 5 1 4 10.75 10.24 180.00000 1 5 4 3.16 3.01 180.00000 3 2 5 8.67 8.31 0.00000 2 3 5 6.80 6.52 0.00000 0 2 6 0.26 0.25 180.00000 6 2 1 0.10 0.09 180.00000 2 6 1 2.99 2.84 180.00000 4 4 2 1.26 1.20 180.00000 5 3 2 18.44 19.80 180.00000 3 5 2 3.88 4.17 180.00000 0 7 2 3.30 3.54 180.00000 4 1 5 0.46 0.49 0.00000 1 4 5 0.00 0.00 0.00000 6 1 3 7.99 8.41 0.00000 1 6 3 3.94 4.14 0.00000 2 1 6 0.21 0.22 0.00000 1 2 6 0.30 0.32 180.00000 1 7 0 14.75 16.64 0.00000 7 1 0 2.18 2.45 0.00000 2 6 2 0.00 0.01 180.00000 6 2 2 1.07 1.15 180.00000 0 6 4 2.25 2.27 0.00000 0 3 6 1.76 1.72 0.00000 1 7 1 0.20 0.20 180.00000 7 1 1 0.92 0.90 180.00000 3 4 4 0.67 0.67 180.00000 4 3 4 0.51 0.51 180.00000 0 5 5 0.01 0.01 0.00000 4 4 3 0.04 0.05 0.00000 2 5 4 0.39 0.39 0.00000 5 2 4 7.87 7.92 0.00000 4 5 0 0.08 0.07 180.00000 5 4 0 1.00 0.97 0.00000 3 3 5 9.32 8.93 0.00000 2 2 6 18.74 17.95 0.00000 5 3 3 0.99 0.94 0.00000 3 5 3 0.60 0.57 0.00000 0 7 3 0.50 0.48 180.00000 2 4 5 1.30 1.26 180.00000 4 2 5 1.84 1.79 0.00000 3 1 6 2.39 2.32 180.00000 1 3 6 13.05 12.66 180.00000 5 4 1 0.23 0.22 180.00000 4 5 1 2.81 2.62 0.00000 1 7 2 0.12 0.11 180.00000 7 1 2 12.27 11.35 0.00000 6 3 0 3.04 2.95 0.00000 3 6 0 0.24 0.23 0.00000 0 8 0 2.15 2.08 0.00000 6 2 3 0.20 0.19 0.00000 2 6 3 3.14 3.01 0.00000 3 6 1 4.70 4.55 0.00000 6 3 1 3.76 3.64 0.00000 6 1 4 9.90 9.54 180.00000 1 6 4 9.08 8.75 180.00000 5 1 5 7.92 7.54 180.00000 1 5 5 2.32 2.21 180.00000 0 4 6 24.22 23.08 180.00000 0 8 1 0.03 0.02 180.00000 4 5 2 5.07 4.78 180.00000 5 4 2 15.32 14.44 180.00000 2 7 0 1.24 1.10 180.00000 7 2 0 5.04 4.48 180.00000 0 1 7 0.03 0.03 0.00000 3 2 6 0.50 0.51 180.00000 2 3 6 0.29 0.30 180.00000 2 7 1 1.47 1.45 0.00000 7 2 1 9.90 9.75 0.00000 6 3 2 7.17 7.01 0.00000 3 6 2 18.83 18.40 0.00000 1 7 3 0.03 0.03 0.00000 7 1 3 0.50 0.50 0.00000 0 8 2 20.68 21.14 180.00000 4 4 4 36.27 36.29 0.00000 1 1 7 3.09 3.07 0.00000 0 6 5 0.78 0.75 0.00000 4 1 6 3.72 3.60 0.00000 1 4 6 0.03 0.03 0.00000 5 3 4 1.64 1.68 0.00000 3 5 4 0.63 0.64 180.00000 0 7 4 0.89 0.91 180.00000 0 2 7 0.25 0.25 180.00000 3 4 5 0.28 0.29 180.00000 4 3 5 1.79 1.83 0.00000 7 2 2 0.28 0.29 0.00000 2 7 2 1.50 1.58 180.00000