data_1529493 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_length_a 9.79306(41) _cell_length_b 9.79306(41) _cell_length_c 9.33885(46) _cod_data_source_file K0p17Mg2Al4p17Si4p83O18_Eu.fcf _cod_data_source_block a _shelx_f_squared_multiplier 1 loop_ _symmetry_equiv_pos_as_xyz '-x, -x+y, -z+1/2' '-x, -x+y, z+1/2' '-x, -y, -z' '-x, -y, z' '-x+y, -x, -z' '-x+y, -x, z' '-x+y, y, -z+1/2' '-x+y, y, z+1/2' '-y, -x, -z+1/2' '-y, -x, z+1/2' '-y, x-y, -z' '-y, x-y, z' 'y, -x+y, -z' 'y, -x+y, z' 'y, x, -z+1/2' 'y, x, z+1/2' 'x-y, -y, -z+1/2' 'x-y, -y, z+1/2' 'x-y, x, -z' 'x-y, x, z' 'x, y, -z' 'x, y, z' 'x, x-y, -z+1/2' 'x, x-y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc 0 1 0 44.51 44.30 180.00000 1 1 0 30.52 29.68 180.00000 0 0 2 11.63 11.63 0.00000 0 2 0 1.37 1.37 0.00000 0 1 2 76.09 75.04 0.00000 1 1 2 126.05 126.95 180.00000 2 1 0 2.69 2.48 0.00000 0 2 2 180.21 178.87 180.00000 2 1 1 253.47 250.29 180.00000 0 3 0 3.61 3.68 0.00000 2 1 2 87.96 87.21 0.00000 2 2 0 29.54 31.62 0.00000 0 3 2 10.80 11.96 0.00000 3 1 0 1.54 1.29 0.00000 0 0 4 53.28 52.57 0.00000 3 1 1 13.11 12.48 0.00000 0 1 4 0.86 0.83 0.00000 2 1 3 19.55 19.24 0.00000 2 2 2 28.19 28.61 180.00000 0 4 0 2.13 2.03 180.00000 1 1 4 31.72 32.79 180.00000 3 1 2 64.70 66.85 0.00000 0 2 4 14.77 14.72 180.00000 3 2 0 35.59 33.26 180.00000 0 4 2 37.13 37.63 180.00000 3 2 1 17.85 17.86 0.00000 2 1 4 18.83 18.64 180.00000 3 1 3 103.73 100.40 180.00000 4 1 0 49.36 51.40 0.00000 4 1 1 51.24 52.62 0.00000 0 3 4 60.16 58.64 0.00000 3 2 2 0.15 0.15 180.00000 4 1 2 22.26 22.68 180.00000 0 5 0 97.99 95.76 180.00000 2 2 4 246.57 243.10 0.00000 3 1 4 19.97 20.25 180.00000 3 2 3 26.63 27.74 0.00000 3 3 0 30.87 31.92 180.00000 2 1 5 21.84 21.71 180.00000 4 2 0 60.42 59.52 0.00000 0 5 2 0.43 0.42 180.00000 4 1 3 119.67 118.00 0.00000 4 2 1 0.02 0.02 180.00000 0 4 4 10.13 11.09 0.00000 0 0 6 35.21 34.78 0.00000 3 3 2 38.39 38.35 180.00000 0 1 6 6.27 6.20 0.00000 5 1 0 2.64 2.61 180.00000 4 2 2 3.26 3.21 0.00000 5 1 1 1.54 1.47 0.00000 3 2 4 112.47 111.86 180.00000 1 1 6 45.79 47.54 180.00000 3 1 5 15.10 14.94 180.00000 0 2 6 46.48 45.63 180.00000 4 1 4 18.49 17.98 180.00000 5 1 2 112.53 105.31 0.00000 4 2 3 22.82 19.28 0.00000 0 6 0 32.53 29.83 0.00000 2 1 6 77.09 79.81 0.00000 4 3 0 6.57 6.86 180.00000 4 3 1 0.71 0.75 0.00000 0 5 4 17.49 18.56 180.00000 5 1 3 3.07 3.16 180.00000 0 3 6 0.16 0.16 0.00000 5 2 0 54.99 54.00 0.00000 0 6 2 221.84 221.45 180.00000 3 2 5 13.65 13.53 0.00000 5 2 1 102.69 104.48 180.00000 3 3 4 2.05 2.10 180.00000 4 3 2 0.20 0.20 180.00000 4 2 4 140.58 136.19 0.00000 4 1 5 56.21 55.13 0.00000 2 2 6 58.01 56.99 180.00000 5 2 2 59.31 62.70 0.00000 3 1 6 53.34 55.03 0.00000 6 1 0 13.09 13.38 180.00000 6 1 1 0.55 0.56 180.00000 5 1 4 7.34 7.31 0.00000 4 3 3 103.37 103.44 180.00000 0 4 6 46.96 47.11 180.00000 6 1 2 6.82 6.99 0.00000 5 2 3 44.40 45.45 180.00000 2 1 7 120.33 120.99 180.00000 4 4 0 1.47 1.49 0.00000 4 2 5 4.36 4.31 0.00000 3 2 6 0.82 0.81 0.00000 5 3 0 13.38 13.10 180.00000 0 7 0 19.96 19.56 180.00000 0 6 4 7.48 7.27 180.00000 5 3 1 0.30 0.29 0.00000 4 3 4 96.99 99.37 180.00000 6 1 3 25.09 25.37 180.00000 4 1 6 2.54 2.49 0.00000 4 4 2 92.50 92.07 180.00000 5 1 5 0.01 0.01 180.00000 6 2 0 20.59 20.48 0.00000 5 2 4 106.98 106.47 0.00000 5 3 2 10.12 10.00 0.00000 0 7 2 0.59 0.58 0.00000 0 0 8 84.21 81.02 0.00000 6 2 1 6.14 5.90 180.00000 3 1 7 1.59 1.57 0.00000 0 1 8 7.70 7.59 180.00000 0 5 6 10.64 10.71 180.00000 6 2 2 37.58 37.33 180.00000 1 1 8 11.60 11.60 180.00000 6 1 4 22.36 22.57 180.00000 5 3 3 5.54 5.57 0.00000 3 3 6 42.82 42.60 180.00000 0 2 8 0.03 0.03 0.00000 7 1 0 1.75 1.71 180.00000 4 3 5 16.22 15.96 180.00000 4 2 6 0.42 0.42 0.00000 7 1 1 37.92 37.37 0.00000 3 2 7 4.84 5.08 0.00000 6 2 3 12.35 12.94 0.00000 5 2 5 48.54 50.66 180.00000 2 1 8 0.00 0.00 180.00000 7 1 2 0.03 0.03 180.00000 5 1 6 37.36 37.57 0.00000 5 4 0 0.29 0.29 180.00000 4 4 4 17.38 17.38 0.00000 4 1 7 18.05 18.08 0.00000 0 3 8 5.88 5.98 0.00000 5 4 1 38.83 39.48 0.00000 5 3 4 11.59 11.80 180.00000 0 7 4 10.41 10.61 180.00000 6 3 0 0.01 0.01 0.00000 6 1 5 6.02 6.20 180.00000 6 3 1 27.26 27.95 0.00000 0 8 0 52.52 53.34 0.00000 5 4 2 31.99 31.73 0.00000 7 1 3 43.41 42.65 0.00000 2 2 8 39.63 38.02 0.00000 6 2 4 0.11 0.11 0.00000 0 6 6 58.67 57.32 180.00000 3 1 8 0.96 0.94 180.00000 6 3 2 1.36 1.33 180.00000 4 3 6 5.29 5.28 0.00000 7 2 0 7.22 7.26 180.00000 0 8 2 0.65 0.65 0.00000 7 2 1 7.58 7.72 0.00000 4 2 7 0.02 0.02 180.00000 5 4 3 44.28 45.22 0.00000 5 2 6 30.19 30.24 0.00000 0 4 8 0.00 0.00 180.00000 5 3 5 1.61 1.55 0.00000 7 1 4 13.95 13.55 0.00000 7 2 2 0.63 0.61 0.00000 6 3 3 3.69 3.57 0.00000 5 1 7 2.17 2.14 0.00000 3 2 8 31.82 31.23 180.00000 6 2 5 0.22 0.22 0.00000 6 1 6 3.54 3.56 0.00000 8 1 0 4.87 4.90 180.00000 4 1 8 6.38 6.39 0.00000 2 1 9 7.37 7.38 180.00000 8 1 1 2.58 2.58 0.00000 5 4 4 0.47 0.48 180.00000 7 2 3 17.57 17.87 180.00000 5 5 0 13.63 14.03 0.00000 6 4 0 0.80 0.82 0.00000 6 3 4 1.58 1.63 0.00000 8 1 2 9.54 9.78 0.00000 6 4 1 1.24 1.26 0.00000 0 8 4 15.97 16.16 0.00000 4 3 7 3.69 3.71 0.00000 7 1 5 29.84 29.79 0.00000 4 4 6 72.34 71.89 180.00000 0 5 8 38.04 37.59 180.00000 5 5 2 1.67 1.64 180.00000 5 3 6 3.29 3.28 0.00000 0 7 6 0.10 0.10 180.00000 7 3 0 0.02 0.02 180.00000 6 4 2 8.40 8.39 180.00000 5 2 7 53.05 52.78 180.00000 3 3 8 12.75 12.56 180.00000 3 1 9 14.62 14.40 180.00000 7 3 1 63.19 62.22 180.00000 7 2 4 30.65 30.09 180.00000 8 1 3 26.72 26.19 0.00000 4 2 8 57.19 55.47 0.00000 0 9 0 0.81 0.79 0.00000 5 4 5 32.56 32.02 0.00000 6 2 6 8.74 8.61 180.00000 7 3 2 13.55 13.32 0.00000 0 0 10 0.02 0.02 180.00000 6 1 7 0.01 0.01 0.00000 6 4 3 3.44 3.47 0.00000 0 1 10 13.20 13.27 0.00000 6 3 5 9.31 9.33 0.00000 5 1 8 0.00 0.00 180.00000 8 2 0 12.30 12.26 0.00000 0 9 2 1.06 1.06 180.00000 8 2 1 18.27 18.54 180.00000 1 1 10 14.75 15.02 180.00000 3 2 9 5.30 5.37 0.00000 8 1 4 4.46 4.50 180.00000 7 3 3 14.80 14.90 180.00000 0 2 10 31.36 31.55 180.00000 7 1 6 5.18 5.19 180.00000 8 2 2 49.32 49.58 180.00000 7 2 5 0.50 0.51 180.00000 4 1 9 25.26 25.19 0.00000 5 5 4 5.29 5.25 180.00000 0 6 8 5.99 5.95 0.00000 6 4 4 23.79 23.54 0.00000 5 3 7 0.01 0.01 0.00000 2 1 10 13.33 13.13 0.00000 4 3 8 13.55 13.32 180.00000 5 4 6 20.28 20.50 0.00000 6 5 0 21.42 21.69 180.00000 9 1 0 19.87 20.13 180.00000