#------------------------------------------------------------------------------ #$Date: 2016-04-06 15:35:39 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181862 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/52/94/1529494.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1529494 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_length_a 9.79423(48) _cell_length_b 9.79423(48) _cell_length_c 9.34129(51) _cod_data_source_file K0p26Mg2Al4p26Si4p74O18_Eu.fcf _cod_data_source_block a #BEGIN Tags that were not found in dictionaries: _shelx_f_squared_multiplier 1 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz '-x, -x+y, -z+1/2' '-x, -x+y, z+1/2' '-x, -y, -z' '-x, -y, z' '-x+y, -x, -z' '-x+y, -x, z' '-x+y, y, -z+1/2' '-x+y, y, z+1/2' '-y, -x, -z+1/2' '-y, -x, z+1/2' '-y, x-y, -z' '-y, x-y, z' 'y, -x+y, -z' 'y, -x+y, z' 'y, x, -z+1/2' 'y, x, z+1/2' 'x-y, -y, -z+1/2' 'x-y, -y, z+1/2' 'x-y, x, -z' 'x-y, x, z' 'x, y, -z' 'x, y, z' 'x, x-y, -z+1/2' 'x, x-y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc 0 1 0 32.26 32.19 180.00000 1 1 0 21.89 20.89 180.00000 0 0 2 8.83 8.79 0.00000 0 2 0 1.78 1.83 0.00000 0 1 2 59.43 58.83 0.00000 1 1 2 99.87 101.59 180.00000 2 1 0 2.17 2.25 0.00000 0 2 2 142.58 143.32 180.00000 2 1 1 197.57 196.76 180.00000 0 3 0 3.39 3.39 0.00000 2 1 2 69.93 68.29 0.00000 2 2 0 25.90 27.19 0.00000 0 3 2 7.73 8.79 0.00000 3 1 0 2.16 1.70 0.00000 0 0 4 41.99 40.96 0.00000 3 1 1 11.25 10.78 0.00000 0 1 4 0.43 0.40 0.00000 2 1 3 16.26 15.37 0.00000 2 2 2 23.67 24.26 180.00000 0 4 0 1.33 1.33 180.00000 1 1 4 25.73 27.11 180.00000 3 1 2 51.18 52.52 0.00000 0 2 4 13.02 13.39 180.00000 3 2 0 27.02 25.01 180.00000 0 4 2 29.95 29.71 180.00000 3 2 1 14.78 14.81 0.00000 2 1 4 16.12 16.83 180.00000 3 1 3 84.64 80.04 180.00000 4 1 0 43.29 44.26 0.00000 4 1 1 39.75 40.59 0.00000 0 3 4 49.38 45.90 0.00000 3 2 2 0.06 0.06 180.00000 4 1 2 18.17 19.09 180.00000 0 5 0 76.17 75.12 180.00000 2 2 4 201.78 194.74 0.00000 3 1 4 19.15 19.49 180.00000 3 2 3 21.48 22.43 0.00000 3 3 0 22.62 23.46 180.00000 2 1 5 17.22 17.27 180.00000 4 2 0 46.52 47.25 0.00000 0 5 2 0.25 0.25 180.00000 4 1 3 101.57 100.07 0.00000 4 2 1 0.01 0.01 180.00000 0 4 4 7.84 8.85 0.00000 0 0 6 27.72 27.71 0.00000 3 3 2 32.05 31.95 180.00000 0 1 6 5.56 5.56 0.00000 5 1 0 2.07 2.01 180.00000 4 2 2 2.40 2.34 0.00000 5 1 1 1.37 1.37 0.00000 3 2 4 92.71 93.39 180.00000 1 1 6 36.88 38.10 180.00000 3 1 5 11.24 11.10 180.00000 0 2 6 35.94 35.15 180.00000 4 1 4 14.63 14.12 180.00000 5 1 2 93.66 84.40 0.00000 4 2 3 18.36 14.42 0.00000 0 6 0 29.78 26.28 0.00000 2 1 6 64.26 66.40 0.00000 4 3 0 4.89 5.09 180.00000 4 3 1 0.59 0.63 0.00000 0 5 4 15.05 16.14 180.00000 5 1 3 3.13 3.28 180.00000 0 3 6 0.06 0.06 0.00000 5 2 0 45.60 45.55 0.00000 0 6 2 185.56 185.06 180.00000 3 2 5 11.30 11.15 0.00000 5 2 1 86.18 86.89 180.00000 3 3 4 1.68 1.69 180.00000 4 3 2 0.12 0.12 180.00000 4 2 4 112.19 109.09 0.00000 4 1 5 46.87 45.17 0.00000 2 2 6 50.73 48.86 180.00000 5 2 2 44.59 46.64 0.00000 3 1 6 47.34 48.65 0.00000 6 1 0 10.49 10.77 180.00000 6 1 1 0.47 0.48 180.00000 5 1 4 4.21 4.21 0.00000 4 3 3 85.58 85.15 180.00000 0 4 6 38.35 37.77 180.00000 6 1 2 6.29 6.31 0.00000 5 2 3 34.90 34.81 180.00000 2 1 7 98.09 97.49 180.00000 4 4 0 1.68 1.69 0.00000 4 2 5 3.28 3.23 0.00000 3 2 6 1.20 1.18 0.00000 5 3 0 11.74 11.47 180.00000 0 7 0 17.07 16.67 180.00000 0 6 4 5.25 5.10 180.00000 5 3 1 0.22 0.23 0.00000 4 3 4 83.39 86.91 180.00000 6 1 3 20.04 20.49 180.00000 4 1 6 1.94 1.94 0.00000 4 4 2 76.89 78.35 180.00000 5 1 5 0.01 0.01 180.00000 6 2 0 18.35 18.85 0.00000 5 2 4 83.56 85.81 0.00000 5 3 2 9.40 9.59 0.00000 0 7 2 0.72 0.73 0.00000 0 0 8 68.49 67.57 0.00000 6 2 1 4.55 4.48 180.00000 3 1 7 1.88 1.87 0.00000 0 1 8 6.64 6.51 180.00000 0 5 6 7.91 7.85 180.00000 6 2 2 30.72 30.07 180.00000 1 1 8 8.52 8.32 180.00000 6 1 4 20.39 20.36 180.00000 5 3 3 4.59 4.63 0.00000 3 3 6 35.51 35.42 180.00000 0 2 8 0.07 0.07 0.00000 7 1 0 1.05 1.02 180.00000 4 3 5 13.32 12.98 180.00000 4 2 6 0.19 0.19 0.00000 7 1 1 30.67 29.82 0.00000 3 2 7 4.14 4.33 0.00000 6 2 3 10.04 10.52 0.00000 5 2 5 39.38 41.10 180.00000 2 1 8 0.04 0.04 180.00000 7 1 2 0.09 0.09 180.00000 5 1 6 31.82 32.19 0.00000 5 4 0 0.24 0.24 180.00000 4 4 4 16.45 16.60 0.00000 4 1 7 13.50 13.63 0.00000 0 3 8 5.30 5.41 0.00000 5 4 1 30.03 30.68 0.00000 5 3 4 9.60 9.79 180.00000 0 7 4 8.63 8.80 180.00000 6 3 0 0.09 0.09 0.00000 6 1 5 4.81 5.01 180.00000 6 3 1 23.10 24.01 0.00000 0 8 0 44.43 45.73 0.00000 5 4 2 26.19 26.27 0.00000 7 1 3 35.22 34.92 0.00000 2 2 8 35.85 34.51 0.00000 6 2 4 0.10 0.09 0.00000 0 6 6 50.96 49.48 180.00000 3 1 8 0.93 0.90 180.00000 6 3 2 1.39 1.39 180.00000 4 3 6 5.66 5.67 0.00000 7 2 0 6.25 6.24 180.00000 0 8 2 0.25 0.25 0.00000 7 2 1 6.36 6.50 0.00000 4 2 7 0.02 0.02 180.00000 5 4 3 36.82 37.63 0.00000 5 2 6 22.58 22.71 0.00000 0 4 8 0.00 0.00 0.00000 5 3 5 1.35 1.27 0.00000 7 1 4 13.06 12.39 0.00000 7 2 2 0.94 0.89 0.00000 6 3 3 2.46 2.32 0.00000 5 1 7 1.97 1.95 0.00000 3 2 8 26.68 26.46 180.00000 6 2 5 0.19 0.20 0.00000 6 1 6 3.76 3.84 0.00000 8 1 0 4.89 4.99 180.00000 4 1 8 6.45 6.46 0.00000 2 1 9 5.33 5.34 180.00000 8 1 1 2.00 2.00 0.00000 5 4 4 1.11 1.12 180.00000 7 2 3 14.09 14.34 180.00000 5 5 0 11.51 11.88 0.00000 6 4 0 0.60 0.62 0.00000 6 3 4 1.76 1.81 0.00000 8 1 2 8.51 8.74 0.00000 6 4 1 0.80 0.82 0.00000 0 8 4 10.84 11.07 0.00000 4 3 7 3.31 3.36 0.00000 7 1 5 24.01 24.19 0.00000 4 4 6 63.54 63.75 180.00000 0 5 8 31.99 31.93 180.00000 5 5 2 1.91 1.88 180.00000 5 3 6 3.32 3.31 0.00000 0 7 6 0.04 0.04 180.00000 7 3 0 0.04 0.05 180.00000 6 4 2 7.40 7.45 180.00000 5 2 7 44.98 45.21 180.00000 3 3 8 9.23 9.21 180.00000 3 1 9 11.25 11.22 180.00000 7 3 1 51.26 51.13 180.00000 7 2 4 26.36 26.16 180.00000 8 1 3 20.94 20.61 0.00000 4 2 8 46.79 45.12 0.00000 0 9 0 0.75 0.72 0.00000 5 4 5 26.86 25.84 0.00000 6 2 6 6.37 6.14 180.00000 7 3 2 12.07 11.68 0.00000 0 0 10 0.12 0.12 180.00000 6 1 7 0.01 0.01 0.00000 6 4 3 2.82 2.83 0.00000 0 1 10 12.00 12.07 0.00000 6 3 5 7.56 7.59 0.00000 5 1 8 0.06 0.06 180.00000 8 2 0 12.67 12.61 0.00000 0 9 2 1.17 1.16 180.00000 8 2 1 15.03 15.26 180.00000 1 1 10 13.12 13.46 180.00000 3 2 9 4.49 4.59 0.00000 8 1 4 4.48 4.57 180.00000 7 3 3 10.29 10.47 180.00000 0 2 10 26.83 27.31 180.00000 7 1 6 5.08 5.16 180.00000 8 2 2 46.86 47.54 180.00000 7 2 5 0.34 0.34 180.00000 4 1 9 21.44 21.40 0.00000 5 5 4 4.15 4.11 180.00000 0 6 8 6.75 6.66 0.00000 6 4 4 20.20 19.83 0.00000 5 3 7 0.01 0.01 0.00000 2 1 10 11.84 11.59 0.00000 4 3 8 12.08 11.82 180.00000 5 4 6 18.52 18.73 0.00000 6 5 0 18.00 18.35 180.00000 9 1 0 16.48 16.80 180.00000