data_1529495 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_length_a 9.79964(49) _cell_length_b 9.79964(49) _cell_length_c 9.36376(55) _cod_data_source_file K0p5Mg2Al4p5Si4p5O18_Eu.fcf _cod_data_source_block a _shelx_f_squared_multiplier 1 loop_ _symmetry_equiv_pos_as_xyz '-x, -x+y, -z+1/2' '-x, -x+y, z+1/2' '-x, -y, -z' '-x, -y, z' '-x+y, -x, -z' '-x+y, -x, z' '-x+y, y, -z+1/2' '-x+y, y, z+1/2' '-y, -x, -z+1/2' '-y, -x, z+1/2' '-y, x-y, -z' '-y, x-y, z' 'y, -x+y, -z' 'y, -x+y, z' 'y, x, -z+1/2' 'y, x, z+1/2' 'x-y, -y, -z+1/2' 'x-y, -y, z+1/2' 'x-y, x, -z' 'x-y, x, z' 'x, y, -z' 'x, y, z' 'x, x-y, -z+1/2' 'x, x-y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc 0 1 0 21.57 21.39 180.00000 1 1 0 14.15 13.42 180.00000 0 0 2 5.76 6.10 0.00000 0 2 0 2.46 2.62 0.00000 0 1 2 51.90 50.88 0.00000 1 1 2 94.26 95.51 180.00000 2 1 0 4.01 4.25 0.00000 0 2 2 138.22 137.88 180.00000 2 1 1 175.63 174.72 180.00000 0 3 0 3.85 3.72 0.00000 2 1 2 55.14 52.55 0.00000 2 2 0 30.01 30.84 0.00000 0 3 2 3.87 4.63 0.00000 3 1 0 3.38 2.70 0.00000 0 0 4 40.07 37.05 0.00000 3 1 1 8.32 7.63 0.00000 0 1 4 0.06 0.05 0.00000 2 1 3 13.49 13.17 0.00000 2 2 2 20.38 20.71 180.00000 0 4 0 0.49 0.48 180.00000 1 1 4 24.84 25.57 180.00000 3 1 2 41.30 42.22 0.00000 0 2 4 13.22 13.78 180.00000 3 2 0 19.24 17.37 180.00000 0 4 2 27.33 27.45 180.00000 3 2 1 13.02 12.62 0.00000 2 1 4 17.75 18.36 180.00000 3 1 3 75.69 73.54 180.00000 4 1 0 45.01 45.90 0.00000 4 1 1 41.35 42.29 0.00000 0 3 4 36.48 33.26 0.00000 3 2 2 0.10 0.10 180.00000 4 1 2 18.77 20.05 180.00000 0 5 0 60.62 59.14 180.00000 2 2 4 173.24 169.70 0.00000 3 1 4 18.80 19.19 180.00000 3 2 3 19.27 19.72 0.00000 3 3 0 17.87 18.12 180.00000 2 1 5 19.09 20.27 180.00000 4 2 0 44.95 45.03 0.00000 0 5 2 0.07 0.07 180.00000 4 1 3 91.54 90.66 0.00000 4 2 1 0.02 0.02 0.00000 0 4 4 5.04 5.72 0.00000 0 0 6 25.47 26.60 0.00000 3 3 2 31.06 30.45 180.00000 0 1 6 6.51 6.64 0.00000 5 1 0 1.34 1.33 180.00000 4 2 2 1.30 1.28 0.00000 5 1 1 2.35 2.37 0.00000 3 2 4 84.72 85.10 180.00000 1 1 6 29.87 30.22 180.00000 3 1 5 9.51 9.07 180.00000 0 2 6 28.85 27.39 180.00000 4 1 4 11.06 10.73 180.00000 5 1 2 79.01 71.57 0.00000 4 2 3 17.87 13.96 0.00000 0 6 0 29.71 25.13 0.00000 2 1 6 64.26 67.51 0.00000 4 3 0 3.83 4.05 180.00000 4 3 1 0.11 0.11 0.00000 0 5 4 13.97 15.30 180.00000 5 1 3 0.99 1.07 180.00000 0 3 6 0.02 0.02 0.00000 5 2 0 42.16 42.89 0.00000 0 6 2 166.11 169.66 180.00000 3 2 5 8.95 9.09 0.00000 5 2 1 74.04 76.82 180.00000 3 3 4 1.79 1.89 180.00000 4 3 2 0.18 0.19 180.00000 4 2 4 87.51 84.91 0.00000 4 1 5 42.48 40.90 0.00000 2 2 6 41.21 39.65 180.00000 5 2 2 33.48 34.73 0.00000 3 1 6 45.71 47.96 0.00000 6 1 0 9.08 9.48 180.00000 6 1 1 0.70 0.72 180.00000 5 1 4 2.36 2.33 0.00000 4 3 3 78.33 76.56 180.00000 0 4 6 30.65 30.13 180.00000 6 1 2 4.35 4.30 0.00000 5 2 3 34.16 33.58 180.00000 2 1 7 86.21 83.34 180.00000 4 4 0 2.07 2.09 0.00000 4 2 5 2.90 2.81 0.00000 3 2 6 2.33 2.26 0.00000 5 3 0 8.18 7.69 180.00000 0 7 0 13.25 12.44 180.00000 0 6 4 3.86 3.62 180.00000 5 3 1 0.09 0.09 0.00000 4 3 4 72.43 76.01 180.00000 6 1 3 17.86 18.57 180.00000 4 1 6 2.47 2.53 0.00000 4 4 2 70.36 72.41 180.00000 5 1 5 0.23 0.24 0.00000 6 2 0 15.63 16.16 0.00000 5 2 4 70.22 71.68 0.00000 5 3 2 9.00 9.03 0.00000 0 7 2 0.80 0.80 0.00000 0 0 8 56.68 55.26 0.00000 6 2 1 5.16 4.94 180.00000 3 1 7 0.66 0.65 0.00000 0 1 8 5.35 5.28 180.00000 0 5 6 5.13 5.00 180.00000 6 2 2 27.35 26.81 180.00000 1 1 8 6.65 6.57 180.00000 6 1 4 21.10 21.44 180.00000 5 3 3 3.27 3.34 0.00000 3 3 6 30.70 31.16 180.00000 0 2 8 0.00 0.00 180.00000 7 1 0 0.30 0.30 180.00000 4 3 5 10.90 10.41 180.00000 4 2 6 0.56 0.53 0.00000 7 1 1 23.85 22.79 0.00000 3 2 7 3.30 3.43 0.00000 6 2 3 6.73 7.03 0.00000 5 2 5 36.93 38.43 180.00000 2 1 8 0.17 0.17 180.00000 7 1 2 0.30 0.31 180.00000 5 1 6 29.96 30.60 0.00000 5 4 0 0.28 0.29 180.00000 4 4 4 13.26 13.50 0.00000 4 1 7 14.32 14.56 0.00000 0 3 8 4.86 4.91 0.00000 5 4 1 29.41 30.03 0.00000 5 3 4 9.42 9.78 180.00000 0 7 4 8.28 8.60 180.00000 6 3 0 0.85 0.87 0.00000 6 1 5 4.02 4.18 180.00000 6 3 1 21.17 21.91 0.00000 0 8 0 39.75 40.61 0.00000 5 4 2 21.73 21.68 0.00000 7 1 3 26.77 26.44 0.00000 2 2 8 35.98 34.94 0.00000 6 2 4 0.04 0.03 0.00000 0 6 6 43.16 41.60 180.00000 3 1 8 1.56 1.50 180.00000 6 3 2 0.77 0.78 180.00000 4 3 6 6.32 6.41 0.00000 7 2 0 5.46 5.47 180.00000 0 8 2 0.67 0.68 0.00000 7 2 1 5.47 5.55 0.00000 4 2 7 0.01 0.01 0.00000 5 4 3 33.42 34.05 0.00000 5 2 6 18.02 18.31 0.00000 0 4 8 0.00 0.00 0.00000 5 3 5 0.74 0.72 0.00000 7 1 4 10.89 10.13 0.00000 7 2 2 0.61 0.56 0.00000 6 3 3 3.72 3.41 0.00000 5 1 7 2.56 2.50 0.00000 3 2 8 24.89 24.81 180.00000 6 2 5 0.00 0.00 180.00000 6 1 6 3.50 3.55 0.00000 8 1 0 4.18 4.15 180.00000 4 1 8 5.14 5.06 0.00000 2 1 9 4.23 4.16 180.00000 8 1 1 2.48 2.45 0.00000 5 4 4 1.47 1.48 180.00000 7 2 3 10.92 11.09 180.00000 5 5 0 8.85 9.09 0.00000 6 4 0 0.95 0.98 0.00000 6 3 4 3.09 3.17 0.00000 8 1 2 6.75 6.92 0.00000 6 4 1 1.31 1.34 0.00000 0 8 4 12.31 12.56 0.00000 4 3 7 1.53 1.56 0.00000 7 1 5 17.94 18.11 0.00000 4 4 6 55.32 55.75 180.00000 0 5 8 24.57 24.77 180.00000 5 5 2 3.49 3.54 180.00000 5 3 6 4.41 4.51 0.00000 0 7 6 0.03 0.03 0.00000 7 3 0 0.00 0.00 180.00000 6 4 2 5.28 5.24 180.00000 5 2 7 38.54 38.32 180.00000 3 3 8 6.71 6.55 180.00000 3 1 9 12.92 12.64 180.00000 7 3 1 43.78 42.50 180.00000 7 2 4 25.63 25.08 180.00000 8 1 3 19.61 19.26 0.00000 4 2 8 38.43 37.64 0.00000 0 9 0 0.95 0.92 0.00000 5 4 5 24.63 23.97 0.00000 6 2 6 4.70 4.58 180.00000 7 3 2 12.41 12.07 0.00000 0 0 10 0.13 0.12 180.00000 6 1 7 0.02 0.02 180.00000 6 4 3 3.04 3.06 0.00000 0 1 10 9.85 9.85 0.00000 6 3 5 8.29 8.36 0.00000 5 1 8 0.05 0.05 180.00000 8 2 0 10.82 10.86 0.00000 0 9 2 1.49 1.50 180.00000 8 2 1 10.56 10.68 180.00000 1 1 10 12.93 13.06 180.00000 3 2 9 3.72 3.75 0.00000 8 1 4 5.45 5.53 180.00000 7 3 3 10.01 10.15 180.00000 0 2 10 22.79 23.16 180.00000 7 1 6 4.66 4.73 180.00000 8 2 2 46.27 47.53 180.00000 7 2 5 0.06 0.06 180.00000 4 1 9 19.83 20.06 0.00000 5 5 4 3.68 3.60 180.00000 0 6 8 4.99 4.87 0.00000 6 4 4 15.74 15.34 0.00000 5 3 7 0.00 0.00 180.00000 2 1 10 10.47 10.20 0.00000 4 3 8 12.76 12.48 180.00000 5 4 6 16.67 16.93 0.00000 6 5 0 16.42 16.50 180.00000 9 1 0 14.95 15.03 180.00000