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Information card for entry 1532486
Preview
| Coordinates | 1532486.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C112 H158 N2 O2 Si2 Sn2 |
|---|---|
| Calculated formula | C112 H158 N2 O2 Si2 Sn2 |
| Title of publication | Two-coordinate group 14 element(ii) hydrides as reagents for the facile, and sometimes reversible, hydrogermylation/hydrostannylation of unactivated alkenes and alkynes |
| Authors of publication | Hadlington, Terrance J.; Hermann, Markus; Frenking, Gernot; Jones, Cameron |
| Journal of publication | Chem. Sci. |
| Year of publication | 2015 |
| Journal volume | 6 |
| Journal issue | 12 |
| Pages of publication | 7249 |
| a | 15.4827 ± 0.0008 Å |
| b | 16.4448 ± 0.0009 Å |
| c | 23.7823 ± 0.0011 Å |
| α | 72.311 ± 0.004° |
| β | 88.259 ± 0.004° |
| γ | 62.908 ± 0.005° |
| Cell volume | 5094.1 ± 0.5 Å3 |
| Cell temperature | 123 ± 2 K |
| Ambient diffraction temperature | 123 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0726 |
| Residual factor for significantly intense reflections | 0.0495 |
| Weighted residual factors for significantly intense reflections | 0.1182 |
| Weighted residual factors for all reflections included in the refinement | 0.1342 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.052 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176428 (current) | 2016-02-13 | Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively. |
1532486.cif |
| 170966 | 2015-12-09 | cif/ Updating files of 1532469, 1532470, 1532471, 1532472, 1532473, 1532474, 1532475, 1532476, 1532477, 1532478, 1532479, 1532480, 1532481, 1532482, 1532483, 1532484, 1532485, 1532486 Original log message: Adding full bibliography for 1532469--1532486.cif. |
1532486.cif |
| 158237 | 2015-09-23 | cif/ Adding structures of 1532469, 1532470, 1532471, 1532472, 1532473, 1532474, 1532475, 1532476, 1532477, 1532478, 1532479, 1532480, 1532481, 1532482, 1532483, 1532484, 1532485, 1532486 via cif-deposit CGI script. |
1532486.cif |
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Users of the data should acknowledge the original authors of the
structural data.