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Information card for entry 1542387
Preview
| Coordinates | 1542387.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C10 H16 N4 O5 |
|---|---|
| Calculated formula | C10 H13 N4 O5 |
| SMILES | O=C1N(C)C(=O)C(=NNC(C)(CO)CO)C(=O)N1C |
| Title of publication | Fe-Catalyzed Olefin Hydroamination with Diazo Compounds for Hydrazone Synthesis. |
| Authors of publication | Zheng, Jing; Qi, Jifeng; Cui, Sunliang |
| Journal of publication | Organic letters |
| Year of publication | 2016 |
| Journal volume | 18 |
| Journal issue | 1 |
| Pages of publication | 128 - 131 |
| a | 14.614 ± 0.003 Å |
| b | 12.706 ± 0.003 Å |
| c | 13.842 ± 0.003 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2570.3 ± 1 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 60 |
| Hermann-Mauguin space group symbol | P b c n |
| Hall space group symbol | -P 2n 2ab |
| Residual factor for all reflections | 0.0953 |
| Residual factor for significantly intense reflections | 0.078 |
| Weighted residual factors for significantly intense reflections | 0.2131 |
| Weighted residual factors for all reflections included in the refinement | 0.2419 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 175747 (current) | 2016-02-04 | cif/ Adding structures of 1542387 via cif-deposit CGI script. |
1542387.cif |
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