#------------------------------------------------------------------------------ #$Date: 2016-04-06 14:21:12 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181861 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/24/1542453.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1542453 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.7430 _cell_length_b 37.3075 _cell_length_c 6.1420 _exptl_crystal_F_000 1696.00 _reflns_d_resolution_high 0.8296 _cod_data_source_file su4007Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' UMD581A_a_a.res in Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 403.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 -7 1158.13 1071.57 88.19 o 3 1 -7 855.43 967.42 104.11 o 5 1 -7 3234.59 2928.06 275.19 o 1 3 -7 2926.80 2692.87 109.24 o 3 3 -7 1692.72 1681.06 103.70 o 5 3 -7 2090.02 2313.43 133.55 o 1 5 -7 1582.27 1616.76 88.80 o 3 5 -7 507.44 574.52 92.83 o 5 5 -7 1003.69 828.10 87.46 o 1 7 -7 2118.44 2194.99 99.86 o 3 7 -7 4820.39 4575.42 157.16 o 5 7 -7 457.40 240.13 68.55 o 1 9 -7 592.40 462.37 80.54 o 3 9 -7 55.97 83.86 83.69 o 5 9 -7 55.28 188.42 106.10 o 1 11 -7 2740.29 2807.24 208.03 o 3 11 -7 2781.79 3078.01 138.81 o 1 13 -7 1138.88 1292.03 100.08 o 3 13 -7 396.89 67.78 105.48 o 2 0 -6 2434.78 2600.19 216.72 o 6 0 -6 3712.52 3801.29 161.01 o 10 0 -6 6365.03 6229.45 334.26 o 0 2 -6 7894.72 7665.22 329.00 o 2 2 -6 390.19 453.74 58.78 o 4 2 -6 755.89 712.87 62.68 o 6 2 -6 357.75 349.79 56.19 o 8 2 -6 948.48 1038.34 80.84 o 10 2 -6 1094.68 1029.22 111.53 o 12 2 -6 16.28 49.69 141.18 o 2 4 -6 1939.50 2057.55 100.99 o 4 4 -6 4701.16 4769.58 116.51 o 6 4 -6 10791.98 11112.04 190.37 o 8 4 -6 3269.30 3157.89 140.07 o 10 4 -6 2389.94 2653.95 190.10 o 12 4 -6 86.32 -56.21 129.28 o 0 6 -6 5018.65 5092.98 172.64 o 2 6 -6 398.56 325.81 55.96 o 4 6 -6 3301.42 3276.52 107.91 o 6 6 -6 217.50 114.88 63.75 o 8 6 -6 1670.43 1426.10 103.23 o 10 6 -6 431.23 339.68 110.93 o 12 6 -6 141.59 351.30 198.74 o 2 8 -6 8395.96 8542.70 171.47 o 4 8 -6 1913.93 1767.91 79.70 o 6 8 -6 5320.12 5605.53 140.64 o 8 8 -6 678.61 783.01 143.56 o 10 8 -6 2183.93 3057.62 336.32 o 0 10 -6 9223.81 9146.26 238.66 o 2 10 -6 1513.93 1551.39 93.19 o 4 10 -6 4939.62 4861.14 131.20 o 6 10 -6 411.21 415.88 52.18 o 8 10 -6 487.94 408.05 112.37 o 10 10 -6 832.43 805.89 178.89 o 2 12 -6 5359.74 5493.09 125.55 o 4 12 -6 1713.67 1561.17 91.97 o 6 12 -6 4432.15 4354.87 163.97 o 8 12 -6 769.20 656.67 84.53 o 10 12 -6 1103.05 1158.56 129.56 o 0 14 -6 6188.35 6256.47 204.78 o 2 14 -6 303.48 286.95 65.14 o 4 14 -6 4566.78 4716.14 121.81 o 6 14 -6 866.81 780.76 82.76 o 8 14 -6 3366.67 3433.00 150.27 o 10 14 -6 819.02 912.10 129.61 o 2 16 -6 2300.79 2331.72 100.59 o 4 16 -6 198.06 108.90 55.32 o 6 16 -6 3246.95 3340.05 148.16 o 8 16 -6 1332.76 1299.19 119.91 o 0 18 -6 4520.01 4959.49 245.94 o 2 18 -6 11.48 46.67 55.12 o 4 18 -6 5615.85 5774.96 157.16 o 6 18 -6 463.95 377.41 90.18 o 8 18 -6 2834.66 2880.41 141.76 o 2 20 -6 896.95 986.51 91.34 o 4 20 -6 31.35 88.04 55.77 o 6 20 -6 2580.36 2492.45 139.69 o 8 20 -6 782.45 512.07 135.21 o 0 22 -6 2991.34 3047.89 373.94 o 2 22 -6 287.04 127.04 90.34 o 4 22 -6 7477.31 7858.58 176.34 o 6 22 -6 509.20 416.88 152.61 o 2 24 -6 525.76 406.99 83.36 o 4 24 -6 1027.28 1075.95 91.90 o 0 26 -6 2525.88 2267.41 205.83 o 1 1 -5 3680.02 3687.61 78.67 o 3 1 -5 11479.97 11637.83 157.38 o 5 1 -5 2106.00 2017.90 67.47 o 7 1 -5 1032.41 932.41 53.40 o 9 1 -5 2783.34 2694.44 64.60 o 11 1 -5 2250.71 2050.59 74.74 o 13 1 -5 3151.24 2982.44 177.68 o 15 1 -5 914.28 843.05 141.12 o 1 3 -5 3526.44 3443.90 77.87 o 3 3 -5 2263.72 2157.94 65.95 o 5 3 -5 4057.90 4101.13 85.80 o 7 3 -5 3849.09 3526.01 133.28 o 9 3 -5 5763.68 5483.65 131.15 o 11 3 -5 740.54 906.29 74.95 o 13 3 -5 4459.02 4260.46 252.54 o 15 3 -5 2057.62 2189.62 170.32 o 1 5 -5 15812.45 16258.69 273.93 o 3 5 -5 4089.95 4101.93 90.56 o 5 5 -5 4713.18 4615.48 91.37 o 7 5 -5 512.85 499.78 35.49 o 9 5 -5 1471.16 1317.01 95.53 o 11 5 -5 323.63 192.28 80.16 o 13 5 -5 91.50 119.99 127.33 o 15 5 -5 291.13 490.74 148.23 o 1 7 -5 4912.15 4820.33 92.02 o 3 7 -5 5896.66 6122.32 105.05 o 5 7 -5 2865.17 2635.07 69.20 o 7 7 -5 2492.56 2427.43 109.40 o 9 7 -5 11173.24 10516.81 252.57 o 11 7 -5 2908.60 2918.85 130.44 o 13 7 -5 1464.08 1647.82 117.51 o 15 7 -5 428.25 242.05 117.90 o 1 9 -5 1845.49 1950.87 65.51 o 3 9 -5 9888.91 9659.14 152.75 o 5 9 -5 922.75 852.13 45.97 o 7 9 -5 67.73 37.12 57.31 o 9 9 -5 801.67 731.37 70.01 o 11 9 -5 48.14 83.31 62.13 o 13 9 -5 1319.96 1456.67 204.16 o 15 9 -5 355.21 812.45 442.77 o 1 11 -5 5436.24 5492.16 99.92 o 3 11 -5 8115.48 8172.29 148.28 o 5 11 -5 658.27 652.54 41.89 o 7 11 -5 2239.00 2326.04 126.26 o 9 11 -5 597.42 657.40 76.55 o 11 11 -5 4834.53 4697.97 141.16 o 13 11 -5 2020.03 1973.12 156.09 o 1 13 -5 2173.45 2182.10 91.11 o 3 13 -5 1736.38 1676.79 77.93 o 5 13 -5 558.71 554.11 39.66 o 7 13 -5 2005.66 1974.81 103.45 o 9 13 -5 407.44 335.80 72.01 o 11 13 -5 2034.86 2142.23 123.69 o 13 13 -5 1615.74 1522.95 123.25 o 1 15 -5 2174.85 2138.48 78.74 o 3 15 -5 5595.29 5756.05 125.62 o 5 15 -5 1732.13 1757.68 66.43 o 7 15 -5 6319.79 6016.98 181.62 o 9 15 -5 823.24 770.91 102.86 o 11 15 -5 3332.49 3115.34 139.61 o 13 15 -5 1543.19 1661.59 131.98 o 1 17 -5 75.81 108.27 47.01 o 3 17 -5 1113.73 1097.67 110.20 o 5 17 -5 103.03 102.01 37.66 o 7 17 -5 812.88 792.76 84.20 o 9 17 -5 376.64 278.32 84.77 o 11 17 -5 939.39 831.67 94.72 o 13 17 -5 1273.72 1168.31 122.67 o 1 19 -5 6629.04 7098.69 143.65 o 3 19 -5 357.97 372.72 80.22 o 5 19 -5 1898.35 1934.24 75.79 o 7 19 -5 1035.65 1022.50 85.90 o 9 19 -5 3254.74 3320.99 136.41 o 11 19 -5 1385.31 1379.30 107.77 o 1 21 -5 1516.94 1547.74 82.97 o 3 21 -5 1211.14 1356.16 80.45 o 5 21 -5 434.90 337.56 44.56 o 7 21 -5 2148.93 2251.67 116.94 o 9 21 -5 33.06 24.17 82.11 o 11 21 -5 1778.87 1939.77 119.40 o 1 23 -5 71.01 77.06 62.16 o 3 23 -5 270.37 327.94 57.41 o 5 23 -5 5413.59 5518.25 149.31 o 7 23 -5 980.00 905.03 95.29 o 9 23 -5 1979.10 1882.47 113.99 o 11 23 -5 2520.71 2365.69 141.87 o 1 25 -5 1649.50 1936.73 110.05 o 3 25 -5 2505.23 2203.58 94.72 o 5 25 -5 4330.25 4441.94 130.14 o 7 25 -5 2681.40 2622.33 132.96 o 9 25 -5 2004.59 2065.91 129.45 o 1 27 -5 2766.00 2654.23 115.76 o 3 27 -5 1653.88 1737.49 106.49 o 5 27 -5 1069.97 1093.54 84.64 o 7 27 -5 1501.69 1457.49 113.73 o 9 27 -5 1725.20 1690.88 139.96 o 1 29 -5 5016.99 4685.26 134.29 o 3 29 -5 590.35 679.00 97.52 o 5 29 -5 3796.14 3565.47 166.70 o 7 29 -5 436.72 198.70 118.02 o 1 31 -5 3158.38 3329.55 141.93 o 3 31 -5 355.24 420.57 79.90 o 5 31 -5 1011.98 1323.06 135.26 o 1 33 -5 5213.29 5229.71 224.78 o 0 0 -4 18079.75 19065.62 438.82 o 4 0 -4 19164.21 19547.32 326.89 o 8 0 -4 12012.61 12885.33 226.72 o 12 0 -4 16075.91 15158.28 324.62 o 16 0 -4 8463.31 8040.69 231.91 o 2 2 -4 1402.79 1319.54 51.59 o 4 2 -4 1189.51 1342.61 48.48 o 6 2 -4 1214.60 1273.85 44.16 o 8 2 -4 2763.13 2966.79 57.60 o 10 2 -4 429.82 418.04 41.70 o 12 2 -4 1351.89 1303.98 68.20 o 14 2 -4 1710.48 1647.79 108.46 o 16 2 -4 969.82 1113.42 88.45 o 0 4 -4 14298.88 13596.45 235.64 o 2 4 -4 1775.95 1890.55 54.58 o 4 4 -4 11244.09 11289.64 168.03 o 6 4 -4 373.31 312.43 28.13 o 8 4 -4 16163.67 16410.45 262.44 o 10 4 -4 4232.49 4196.00 191.13 o 12 4 -4 11138.10 10755.25 282.23 o 14 4 -4 699.15 607.83 59.63 o 16 4 -4 4540.93 4451.54 161.13 o 2 6 -4 1917.47 1926.29 54.39 o 4 6 -4 842.93 813.65 39.73 o 6 6 -4 870.63 842.16 30.67 o 8 6 -4 695.37 782.32 51.27 o 10 6 -4 1165.35 1166.53 67.44 o 12 6 -4 961.04 1042.50 74.13 o 14 6 -4 248.95 326.83 80.34 o 16 6 -4 3438.85 3201.82 236.59 o 0 8 -4 29515.17 30368.21 581.73 o 2 8 -4 2530.40 2696.16 60.86 o 4 8 -4 12811.53 12266.54 182.01 o 6 8 -4 8658.86 8693.08 396.44 o 8 8 -4 6548.74 6468.07 145.59 o 10 8 -4 342.98 462.44 50.74 o 12 8 -4 4216.06 4129.42 118.87 o 14 8 -4 668.48 725.44 104.94 o 16 8 -4 5204.67 5089.58 259.25 o 2 10 -4 6242.17 6323.76 98.07 o 4 10 -4 506.76 522.52 38.93 o 6 10 -4 9063.02 9376.14 158.78 o 8 10 -4 134.50 217.86 47.52 o 10 10 -4 999.79 990.92 64.65 o 12 10 -4 702.94 734.99 66.49 o 14 10 -4 212.89 223.22 68.62 o 16 10 -4 2681.40 2498.41 174.81 o 0 12 -4 4699.30 4394.50 161.97 o 2 12 -4 995.29 1029.05 45.30 o 4 12 -4 11685.26 11495.46 220.38 o 6 12 -4 1221.41 1201.21 63.49 o 8 12 -4 12495.38 12107.12 219.54 o 10 12 -4 293.78 329.08 57.11 o 12 12 -4 1928.27 1964.19 108.67 o 14 12 -4 2253.03 2353.97 129.07 o 16 12 -4 4203.12 4293.11 186.93 o 2 14 -4 6509.76 6603.68 147.71 o 4 14 -4 4076.53 3906.69 88.04 o 6 14 -4 5066.72 4786.08 118.00 o 8 14 -4 1185.74 1138.79 75.56 o 10 14 -4 1054.82 1052.04 73.01 o 12 14 -4 298.39 251.36 67.65 o 14 14 -4 827.20 811.74 97.53 o 16 14 -4 865.69 831.21 118.16 o 0 16 -4 5613.19 5415.92 133.41 o 2 16 -4 275.70 259.21 34.28 o 4 16 -4 6611.75 6398.75 105.87 o 6 16 -4 16297.53 16249.94 223.82 o 8 16 -4 1553.04 1560.61 90.98 o 10 16 -4 2604.76 2656.82 107.83 o 12 16 -4 1947.53 1996.85 117.21 o 14 16 -4 1535.56 1616.18 103.73 o 16 16 -4 1020.02 831.55 115.95 o 2 18 -4 8470.04 8627.53 130.08 o 4 18 -4 693.52 685.62 48.76 o 6 18 -4 3751.18 3711.68 77.65 o 8 18 -4 2248.64 2191.86 113.14 o 10 18 -4 810.10 776.91 85.74 o 12 18 -4 4432.35 4303.26 147.42 o 14 18 -4 1441.74 1792.19 110.27 o 0 20 -4 5265.33 4891.69 142.68 o 2 20 -4 484.19 524.71 43.18 o 4 20 -4 1715.26 1722.62 74.33 o 6 20 -4 385.21 391.44 37.06 o 8 20 -4 616.52 651.76 106.06 o 10 20 -4 4072.82 4011.29 152.47 o 12 20 -4 1604.09 1661.65 102.55 o 14 20 -4 2301.53 2366.58 127.95 o 2 22 -4 11013.08 11406.98 218.31 o 4 22 -4 553.60 613.38 49.82 o 6 22 -4 5491.93 5507.61 140.78 o 8 22 -4 4674.49 4626.78 97.47 o 10 22 -4 5745.70 5786.39 161.81 o 12 22 -4 1502.57 1419.56 102.63 o 14 22 -4 2378.08 2497.22 132.83 o 0 24 -4 1681.88 1612.21 117.32 o 2 24 -4 7862.06 7605.94 139.00 o 4 24 -4 552.45 516.68 76.15 o 6 24 -4 4675.01 4627.10 112.60 o 8 24 -4 454.97 464.50 60.46 o 10 24 -4 663.18 588.85 90.25 o 12 24 -4 547.36 698.45 97.87 o 2 26 -4 6000.76 6453.67 164.88 o 4 26 -4 1961.88 1876.91 88.97 o 6 26 -4 8064.15 8371.24 189.06 o 8 26 -4 136.19 183.83 46.81 o 10 26 -4 6436.14 6327.00 189.12 o 12 26 -4 123.71 35.67 98.80 o 0 28 -4 43.28 64.85 72.68 o 2 28 -4 399.50 380.94 63.07 o 4 28 -4 1605.51 1511.17 80.66 o 6 28 -4 235.40 251.18 93.97 o 8 28 -4 19.05 -27.84 50.01 o 10 28 -4 1539.52 1799.87 118.02 o 12 28 -4 1308.20 1326.91 147.71 o 2 30 -4 11807.13 11905.41 205.96 o 4 30 -4 449.70 411.24 61.73 o 6 30 -4 4047.87 4032.89 162.74 o 8 30 -4 50.38 44.27 70.88 o 10 30 -4 2395.36 2781.16 171.33 o 0 32 -4 641.95 521.19 98.09 o 2 32 -4 21.24 6.59 65.34 o 4 32 -4 462.86 353.33 78.01 o 6 32 -4 362.80 316.88 78.81 o 8 32 -4 345.92 252.29 70.51 o 2 34 -4 4382.85 4246.55 133.05 o 4 34 -4 196.00 167.31 75.87 o 6 34 -4 7786.28 8339.10 189.99 o 0 36 -4 34.39 -108.73 108.73 o 2 36 -4 102.23 -3.19 85.33 o 4 36 -4 1048.53 1084.34 102.75 o 1 1 -3 8335.03 8502.74 150.40 o 3 1 -3 6461.38 7048.82 152.05 o 5 1 -3 5578.30 5256.19 97.32 o 7 1 -3 1777.46 1804.94 47.11 o 9 1 -3 3090.26 3139.94 58.43 o 11 1 -3 2804.12 3025.13 72.76 o 13 1 -3 4544.80 4294.49 100.12 o 15 1 -3 418.81 452.13 47.28 o 17 1 -3 2274.50 2375.13 104.10 o 19 1 -3 275.44 322.10 122.49 o 1 3 -3 11806.08 12112.36 144.22 o 3 3 -3 8574.41 8462.62 138.41 o 5 3 -3 8156.39 8105.12 226.20 o 7 3 -3 7146.78 6918.46 112.40 o 9 3 -3 4592.40 4622.91 76.01 o 11 3 -3 2272.13 2364.64 88.18 o 13 3 -3 2822.10 2648.65 64.87 o 15 3 -3 801.26 813.62 49.76 o 17 3 -3 3554.22 3494.70 121.72 o 19 3 -3 1942.54 2030.37 288.58 o 1 5 -3 792.06 937.01 39.32 o 3 5 -3 242.10 305.74 24.64 o 5 5 -3 10810.07 11581.72 152.98 o 7 5 -3 7008.17 6675.58 116.76 o 9 5 -3 995.67 1055.85 52.34 o 11 5 -3 2172.52 2105.40 109.33 o 13 5 -3 1224.33 1195.36 53.70 o 15 5 -3 2.62 11.76 35.41 o 17 5 -3 2133.77 2230.00 100.74 o 19 5 -3 1018.72 1253.94 95.43 o 1 7 -3 15717.90 16386.56 191.32 o 3 7 -3 16850.03 16942.09 202.61 o 5 7 -3 23863.97 24843.55 326.86 o 7 7 -3 4612.19 4563.93 112.66 o 9 7 -3 6964.99 7392.84 134.71 o 11 7 -3 2270.48 2288.11 78.98 o 13 7 -3 2785.82 2579.69 59.77 o 15 7 -3 4008.88 3859.43 86.42 o 17 7 -3 767.85 795.02 68.71 o 19 7 -3 2290.24 2465.49 234.74 o 1 9 -3 2254.95 2228.00 49.33 o 3 9 -3 929.29 1039.01 35.42 o 5 9 -3 1256.92 1189.24 51.84 o 7 9 -3 2632.15 2554.04 72.76 o 9 9 -3 3990.27 3891.33 94.85 o 11 9 -3 5848.15 6048.64 128.09 o 13 9 -3 3608.77 3453.66 115.29 o 15 9 -3 685.63 688.60 42.83 o 17 9 -3 812.67 933.70 77.42 o 19 9 -3 1227.14 1346.24 133.48 o 1 11 -3 20548.40 21825.96 248.22 o 3 11 -3 6746.02 6344.94 100.05 o 5 11 -3 19764.08 20130.93 230.53 o 7 11 -3 192.43 165.18 34.51 o 9 11 -3 6575.12 6655.95 139.74 o 11 11 -3 162.22 140.38 46.50 o 13 11 -3 8972.70 8988.51 176.07 o 15 11 -3 5216.10 4997.38 119.28 o 17 11 -3 2563.48 2564.02 130.80 o 1 13 -3 3675.60 3876.53 68.61 o 3 13 -3 486.46 517.73 32.91 o 5 13 -3 1008.26 820.11 32.36 o 7 13 -3 785.05 808.49 52.60 o 9 13 -3 4885.28 4888.90 110.67 o 11 13 -3 3572.02 3593.44 105.54 o 13 13 -3 3459.42 3445.60 112.04 o 15 13 -3 1436.77 1521.11 157.85 o 17 13 -3 1863.13 1949.46 130.64 o 1 15 -3 6173.89 6210.07 94.21 o 3 15 -3 5034.49 4754.14 79.71 o 5 15 -3 9742.03 9384.25 127.22 o 7 15 -3 10510.71 10258.73 136.33 o 9 15 -3 13575.90 13679.94 218.44 o 11 15 -3 18771.33 18962.71 289.60 o 13 15 -3 2264.76 2590.40 146.59 o 15 15 -3 902.75 975.09 90.29 o 17 15 -3 3251.08 2897.89 137.54 o 1 17 -3 101.13 70.92 25.81 o 3 17 -3 4153.64 4468.31 79.95 o 5 17 -3 315.01 326.77 31.52 o 7 17 -3 445.02 520.44 34.31 o 9 17 -3 14311.53 14071.74 201.40 o 11 17 -3 955.21 1041.71 72.71 o 13 17 -3 2486.05 2658.41 128.03 o 15 17 -3 1856.68 1686.49 103.43 o 17 17 -3 1269.84 1319.87 110.73 o 1 19 -3 2339.23 2202.47 60.30 o 3 19 -3 10542.46 10242.33 141.98 o 5 19 -3 11345.48 11030.32 284.68 o 7 19 -3 15267.71 15431.60 199.18 o 9 19 -3 4989.93 4789.36 88.03 o 11 19 -3 10981.17 10662.21 160.82 o 13 19 -3 4082.24 4438.39 156.45 o 15 19 -3 5537.79 5812.61 200.34 o 17 19 -3 983.37 1207.83 189.60 o 1 21 -3 430.50 493.98 37.29 o 3 21 -3 1857.98 1951.84 72.25 o 5 21 -3 4002.28 3947.73 82.72 o 7 21 -3 9754.43 9601.02 177.60 o 9 21 -3 1604.63 1569.32 57.13 o 11 21 -3 4825.92 4747.09 100.02 o 13 21 -3 2857.55 2785.92 93.39 o 15 21 -3 3124.14 3210.10 151.86 o 1 23 -3 4026.60 3703.96 83.82 o 3 23 -3 4709.21 4480.09 95.09 o 5 23 -3 863.55 867.22 51.32 o 7 23 -3 4186.17 4357.52 121.90 o 9 23 -3 10020.08 9892.64 159.69 o 11 23 -3 7202.89 6890.92 129.54 o 13 23 -3 3428.07 3110.07 105.74 o 15 23 -3 3289.53 3279.11 165.48 o 1 25 -3 2361.08 2263.83 74.76 o 3 25 -3 2424.85 2366.22 75.66 o 5 25 -3 1224.21 1179.91 66.04 o 7 25 -3 1255.95 1212.87 70.63 o 9 25 -3 2048.49 2067.92 79.54 o 11 25 -3 5287.38 5154.57 127.98 o 13 25 -3 913.53 706.66 90.88 o 15 25 -3 6334.42 5833.01 203.30 o 1 27 -3 1918.91 1725.30 71.84 o 3 27 -3 8218.80 8232.43 137.50 o 5 27 -3 1523.54 1386.01 75.22 o 7 27 -3 3546.16 3400.52 118.94 o 9 27 -3 727.91 874.25 79.68 o 11 27 -3 376.51 505.52 64.58 o 13 27 -3 1365.89 1231.10 90.89 o 1 29 -3 2025.35 1997.98 82.32 o 3 29 -3 3360.83 3275.83 102.63 o 5 29 -3 2332.44 2368.67 100.41 o 7 29 -3 3965.15 3963.64 191.51 o 9 29 -3 130.96 205.01 61.58 o 11 29 -3 3894.07 3909.99 135.44 o 13 29 -3 20.53 -76.15 76.15 o 1 31 -3 1196.70 1079.13 107.21 o 3 31 -3 4245.71 4056.15 116.62 o 5 31 -3 808.90 864.42 86.94 o 7 31 -3 3555.50 3378.44 118.13 o 9 31 -3 1490.04 1462.44 104.63 o 11 31 -3 494.62 714.45 81.26 o 1 33 -3 446.54 625.29 90.48 o 3 33 -3 2769.27 2882.76 114.99 o 5 33 -3 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100.18 o 1 1 1 13628.99 13335.66 168.58 o 3 1 1 55918.80 53416.55 578.44 o 5 1 1 46221.34 45699.30 454.30 o 7 1 1 18611.26 18736.07 185.62 o 9 1 1 2337.19 2391.18 45.65 o 11 1 1 1739.23 1717.21 55.81 o 13 1 1 3303.91 3192.89 79.18 o 15 1 1 3963.49 3973.41 76.67 o 17 1 1 7467.22 7329.08 125.86 o 19 1 1 1057.11 1022.78 59.51 o 21 1 1 3474.65 3363.38 149.70 o 1 3 1 44996.11 42630.57 512.44 o 3 3 1 65258.49 61186.92 908.95 o 5 3 1 96588.30 90748.96 841.09 o 7 3 1 2801.00 2539.07 42.91 o 9 3 1 5179.58 5151.07 72.49 o 11 3 1 7242.04 7359.51 99.17 o 13 3 1 269.30 229.53 30.61 o 15 3 1 2855.99 2693.06 70.59 o 17 3 1 5089.13 5192.34 105.30 o 19 3 1 3402.31 3433.51 94.31 o 21 3 1 2104.97 2069.29 117.32 o 1 5 1 29255.32 28266.51 295.67 o 3 5 1 15472.20 15233.25 194.69 o 5 5 1 15762.05 15493.20 196.62 o 7 5 1 358.56 410.36 21.22 o 9 5 1 10432.71 10712.05 119.96 o 11 5 1 6310.54 6587.48 86.61 o 13 5 1 7051.88 7012.65 109.45 o 15 5 1 2312.78 2393.47 67.52 o 17 5 1 7816.26 7883.48 132.94 o 19 5 1 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o 0 2 2 4792.21 4569.39 86.95 o 2 2 2 21202.57 21252.71 463.06 o 4 2 2 8442.70 9125.45 129.42 o 6 2 2 3343.16 3493.25 67.63 o 8 2 2 4057.01 4377.22 56.20 o 10 2 2 300.25 318.38 19.96 o 12 2 2 65.82 51.99 22.70 o 14 2 2 2360.55 2263.21 67.44 o 16 2 2 723.30 780.36 50.05 o 18 2 2 3471.16 3472.79 89.23 o 20 2 2 241.59 181.30 58.17 o 2 4 2 14209.87 14007.70 169.42 o 4 4 2 2250.72 2275.15 53.74 o 6 4 2 10528.85 9964.07 145.78 o 8 4 2 8986.85 10282.50 117.57 o 10 4 2 18731.78 18686.20 192.55 o 12 4 2 965.10 1009.21 51.55 o 14 4 2 900.21 991.01 43.60 o 16 4 2 1206.99 1299.36 64.28 o 18 4 2 1209.99 1225.26 73.70 o 20 4 2 995.65 986.53 66.99 o 0 6 2 11756.78 11935.49 194.53 o 2 6 2 22921.69 24030.74 264.46 o 4 6 2 4847.36 4896.38 83.24 o 6 6 2 12435.91 13468.30 187.81 o 8 6 2 9857.02 9837.70 125.20 o 10 6 2 7078.73 6952.71 91.41 o 12 6 2 2188.54 2308.44 53.10 o 14 6 2 8229.17 8371.39 117.11 o 16 6 2 940.18 935.82 52.35 o 18 6 2 2034.80 2095.50 81.89 o 20 6 2 1698.51 1573.79 84.72 o 2 8 2 23176.46 22949.42 270.85 o 4 8 2 107.16 121.38 24.38 o 6 8 2 1181.84 1568.00 45.80 o 8 8 2 1324.85 1403.61 47.51 o 10 8 2 5588.23 5213.20 73.84 o 12 8 2 3550.70 3531.09 63.60 o 14 8 2 16403.61 16436.63 193.33 o 16 8 2 2322.50 2194.97 75.50 o 18 8 2 4410.38 4540.52 106.65 o 20 8 2 291.31 334.10 67.76 o 0 10 2 32825.59 35316.96 652.49 o 2 10 2 276.70 288.27 19.44 o 4 10 2 12421.78 12772.02 151.47 o 6 10 2 4167.79 4427.78 84.45 o 8 10 2 12727.30 12658.81 185.55 o 10 10 2 7622.10 7398.16 96.95 o 12 10 2 13271.76 13348.60 166.67 o 14 10 2 5749.96 5481.67 92.57 o 16 10 2 5850.02 5914.95 104.74 o 18 10 2 296.03 390.83 52.20 o 20 10 2 748.49 876.10 123.69 o 2 12 2 41678.96 43816.50 470.74 o 4 12 2 873.30 998.30 27.74 o 6 12 2 11199.28 10689.29 111.71 o 8 12 2 6373.51 6563.16 81.98 o 10 12 2 9134.62 8883.46 113.18 o 12 12 2 2960.31 3044.04 63.35 o 14 12 2 9984.48 10066.58 136.04 o 16 12 2 296.46 254.54 40.94 o 18 12 2 774.98 840.91 58.07 o 0 14 2 25919.33 28310.08 393.84 o 2 14 2 2405.56 2621.17 45.02 o 4 14 2 13293.24 13852.12 147.84 o 6 14 2 588.38 661.18 23.93 o 8 14 2 19221.95 18844.85 200.98 o 10 14 2 1779.31 1808.20 44.61 o 12 14 2 14166.56 14209.92 164.98 o 14 14 2 483.35 516.92 41.17 o 16 14 2 1391.53 1538.40 61.85 o 18 14 2 949.07 862.52 59.37 o 2 16 2 12590.89 12348.62 135.91 o 4 16 2 5352.83 5657.97 72.22 o 6 16 2 10209.86 10142.17 112.57 o 8 16 2 12121.95 12276.43 141.10 o 10 16 2 9757.35 9595.57 129.68 o 12 16 2 9362.17 9186.43 132.10 o 14 16 2 2468.32 2504.61 72.54 o 16 16 2 1251.64 1224.42 60.10 o 18 16 2 1543.42 1563.42 76.43 o 0 18 2 17832.84 17549.40 259.67 o 2 18 2 7677.29 8354.81 102.32 o 4 18 2 8576.89 8436.04 98.89 o 6 18 2 905.50 976.95 33.53 o 8 18 2 11991.13 11965.43 142.32 o 10 18 2 176.11 158.75 26.75 o 12 18 2 8880.38 9035.19 140.53 o 14 18 2 2326.25 2350.62 72.92 o 16 18 2 1968.92 1999.57 73.50 o 18 18 2 496.64 565.15 57.50 o 2 20 2 9945.99 10745.70 119.68 o 4 20 2 1005.64 1143.50 37.75 o 6 20 2 4776.58 4754.16 70.76 o 8 20 2 4135.10 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106.88 o 2 28 2 4043.40 4049.62 72.65 o 4 28 2 1593.74 1641.28 56.47 o 6 28 2 92.99 114.79 38.09 o 8 28 2 428.00 442.22 46.54 o 10 28 2 1006.83 1095.82 61.07 o 12 28 2 4360.81 4517.51 108.94 o 14 28 2 2031.17 1900.96 79.98 o 0 30 2 15473.61 15041.67 235.32 o 2 30 2 1806.18 1674.06 59.60 o 4 30 2 2346.47 2384.67 70.81 o 6 30 2 634.38 643.88 46.98 o 8 30 2 501.83 699.32 54.28 o 10 30 2 5.93 -32.61 48.34 o 12 30 2 4146.41 4164.56 127.86 o 14 30 2 127.23 154.43 60.46 o 2 32 2 2855.18 2607.55 75.44 o 4 32 2 1312.05 1311.16 59.77 o 6 32 2 641.35 617.26 51.09 o 8 32 2 3725.32 3607.08 97.06 o 10 32 2 165.29 103.78 53.79 o 12 32 2 1875.55 2165.94 89.51 o 0 34 2 3755.51 3753.68 133.75 o 2 34 2 177.05 170.01 46.00 o 4 34 2 769.74 857.94 62.16 o 6 34 2 568.21 536.38 60.18 o 8 34 2 4515.25 4651.20 112.59 o 10 34 2 173.10 33.73 56.35 o 12 34 2 3252.20 3291.13 108.26 o 2 36 2 1817.67 1726.07 65.75 o 4 36 2 3539.32 3415.00 102.14 o 6 36 2 425.85 457.65 68.69 o 8 36 2 990.61 1149.87 68.43 o 10 36 2 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5221.33 150.35 o 13 25 3 916.60 875.94 82.98 o 15 25 3 6269.01 6264.63 168.88 o 1 27 3 1935.92 1726.54 58.24 o 3 27 3 8227.97 7935.28 143.76 o 5 27 3 1504.95 1379.25 52.87 o 7 27 3 3407.21 3378.99 75.98 o 9 27 3 739.25 688.45 44.83 o 11 27 3 427.35 440.66 78.71 o 13 27 3 1366.74 1412.72 100.28 o 1 29 3 2058.33 1942.16 66.57 o 3 29 3 3395.14 3319.69 84.11 o 5 29 3 2277.56 2348.08 70.07 o 7 29 3 4015.91 3931.15 91.33 o 9 29 3 128.75 221.88 43.98 o 11 29 3 3836.42 3758.04 90.43 o 13 29 3 29.11 -22.82 78.71 o 1 31 3 1259.56 1188.71 56.87 o 3 31 3 4249.22 4045.51 89.71 o 5 31 3 777.06 907.86 51.93 o 7 31 3 3582.78 3620.95 95.35 o 9 31 3 1490.90 1508.04 67.36 o 11 31 3 509.15 661.28 56.71 o 1 33 3 465.78 494.39 52.30 o 3 33 3 2674.71 2605.90 83.48 o 5 33 3 1436.76 1443.32 62.74 o 7 33 3 3978.50 3773.44 103.69 o 9 33 3 920.77 1079.22 66.00 o 11 33 3 1427.63 1530.97 115.53 o 1 35 3 190.86 265.58 50.59 o 3 35 3 682.05 797.22 59.47 o 5 35 3 858.39 854.26 58.72 o 7 35 3 1691.92 1576.56 74.15 o 9 35 3 463.34 524.69 66.53 o 1 37 3 163.13 210.94 56.31 o 3 37 3 2917.25 2944.59 96.13 o 5 37 3 1304.27 1599.13 129.56 o 7 37 3 2627.52 2719.93 121.97 o 1 39 3 1013.01 1199.29 71.28 o 3 39 3 580.01 675.68 91.34 o 5 39 3 781.17 812.57 80.11 o 1 41 3 3177.06 3448.93 135.08 o 0 0 4 17865.03 18155.53 432.96 o 4 0 4 19237.29 20278.24 381.52 o 8 0 4 12116.18 12259.76 359.96 o 12 0 4 15994.01 14884.58 324.32 o 16 0 4 8424.42 8341.45 246.28 o 2 2 4 1382.48 1433.81 43.44 o 4 2 4 1155.64 1280.04 41.71 o 6 2 4 1202.88 1231.76 37.58 o 8 2 4 2852.17 2836.34 71.82 o 10 2 4 426.93 364.17 38.62 o 12 2 4 1315.51 1329.56 88.13 o 14 2 4 1716.29 1593.92 81.96 o 16 2 4 967.67 1048.10 76.05 o 0 4 4 14108.57 13176.73 340.13 o 2 4 4 1770.52 1780.00 47.68 o 4 4 4 11239.18 11227.11 142.03 o 6 4 4 371.10 316.05 34.98 o 8 4 4 16147.17 15476.78 230.41 o 10 4 4 4235.08 4076.90 94.97 o 12 4 4 11006.98 10556.24 145.90 o 14 4 4 711.14 609.27 45.54 o 16 4 4 4512.01 4573.43 165.81 o 2 6 4 2005.14 2122.16 52.06 o 4 6 4 815.07 850.76 33.54 o 6 6 4 814.76 886.93 49.60 o 8 6 4 676.95 718.92 47.68 o 10 6 4 1137.85 1146.39 56.04 o 12 6 4 961.88 1003.04 45.50 o 14 6 4 263.86 325.90 38.33 o 16 6 4 3460.54 3339.01 124.90 o 0 8 4 28721.11 28780.72 730.21 o 2 8 4 2522.77 2838.65 58.99 o 4 8 4 12864.75 12127.16 190.50 o 6 8 4 8611.57 8760.00 161.10 o 8 8 4 6479.49 6158.74 122.92 o 10 8 4 332.90 317.64 40.56 o 12 8 4 4169.38 4154.61 83.34 o 14 8 4 638.25 646.30 63.50 o 16 8 4 5290.86 5084.77 232.51 o 2 10 4 6438.74 6452.67 97.59 o 4 10 4 489.67 431.82 26.18 o 6 10 4 9278.56 9082.77 274.60 o 8 10 4 153.18 94.41 42.34 o 10 10 4 928.95 795.54 51.88 o 12 10 4 697.36 736.31 54.78 o 14 10 4 242.55 327.86 54.92 o 16 10 4 2728.87 2801.02 135.03 o 0 12 4 4646.14 4355.44 115.45 o 2 12 4 1003.49 1065.24 44.07 o 4 12 4 11461.95 11204.83 145.62 o 6 12 4 1249.47 1177.37 72.02 o 8 12 4 12563.56 12609.96 202.40 o 10 12 4 286.45 335.18 48.40 o 12 12 4 1948.75 1855.91 82.00 o 14 12 4 2192.76 2186.15 89.22 o 16 12 4 4387.10 4310.58 128.42 o 2 14 4 6465.88 6680.51 103.38 o 4 14 4 4041.69 4197.33 74.19 o 6 14 4 5195.12 5050.67 115.79 o 8 14 4 1221.16 1110.68 67.31 o 10 14 4 1156.54 1237.66 66.70 o 12 14 4 289.91 234.61 54.76 o 14 14 4 748.81 793.31 68.61 o 16 14 4 874.29 873.93 89.08 o 0 16 4 5596.71 5213.56 129.88 o 2 16 4 280.00 236.68 32.40 o 4 16 4 6824.53 6540.11 135.90 o 6 16 4 16432.69 16526.88 251.40 o 8 16 4 1518.93 1437.47 54.41 o 10 16 4 2674.56 2728.54 84.83 o 12 16 4 1963.92 1939.47 86.42 o 14 16 4 1525.09 1537.56 81.29 o 16 16 4 1034.80 999.44 86.56 o 2 18 4 8339.37 8524.60 128.43 o 4 18 4 698.80 769.83 39.83 o 6 18 4 3904.08 3988.66 121.24 o 8 18 4 2237.64 2211.65 65.76 o 10 18 4 733.59 798.68 48.54 o 12 18 4 4422.90 4156.79 119.26 o 14 18 4 1440.76 1668.86 87.88 o 0 20 4 5353.96 5008.62 118.73 o 2 20 4 493.49 515.08 35.28 o 4 20 4 1820.03 1733.17 52.02 o 6 20 4 380.40 422.01 45.95 o 8 20 4 657.30 751.73 46.20 o 10 20 4 4124.03 4073.05 94.91 o 12 20 4 1544.09 1494.79 81.24 o 14 20 4 2229.14 2218.72 104.63 o 2 22 4 11266.95 11721.91 146.05 o 4 22 4 554.87 599.76 37.79 o 6 22 4 5619.80 5726.48 105.32 o 8 22 4 4699.03 4665.06 101.56 o 10 22 4 5612.22 5793.75 132.02 o 12 22 4 1480.33 1283.00 83.08 o 14 22 4 2378.21 2576.89 134.57 o 0 24 4 1737.24 1781.27 102.17 o 2 24 4 7824.44 7384.82 128.30 o 4 24 4 571.27 467.07 39.84 o 6 24 4 4617.56 4484.32 77.71 o 8 24 4 474.32 461.26 56.75 o 10 24 4 626.51 599.07 75.03 o 12 24 4 526.67 605.31 81.06 o 2 26 4 6092.93 6407.66 113.49 o 4 26 4 1963.65 1928.10 70.29 o 6 26 4 8003.84 8347.70 121.09 o 8 26 4 137.61 132.98 58.01 o 10 26 4 6366.11 6607.69 152.11 o 12 26 4 125.49 141.75 80.40 o 0 28 4 42.36 -32.61 67.32 o 2 28 4 391.83 438.52 46.90 o 4 28 4 1609.00 1665.11 67.80 o 6 28 4 218.57 308.16 47.66 o 8 28 4 18.68 64.94 58.06 o 10 28 4 1549.88 2007.36 103.15 o 12 28 4 1312.76 1215.49 132.46 o 2 30 4 11457.72 11714.68 156.27 o 4 30 4 450.19 401.98 56.02 o 6 30 4 4096.99 4018.65 102.76 o 8 30 4 52.00 25.82 45.05 o 10 30 4 2332.03 2756.00 203.28 o 0 32 4 622.70 555.44 79.42 o 2 32 4 22.86 83.06 48.12 o 4 32 4 474.86 487.59 53.02 o 6 32 4 379.47 315.67 53.80 o 8 32 4 352.23 370.23 65.20 o 2 34 4 4259.70 4347.03 109.34 o 4 34 4 198.24 202.06 56.64 o 6 34 4 7835.77 8324.17 141.76 o 0 36 4 45.91 8.64 130.24 o 2 36 4 99.69 139.32 80.31 o 4 36 4 1081.42 1040.79 75.66 o 1 1 5 3653.48 3542.79 76.01 o 3 1 5 11391.15 11521.36 163.43 o 5 1 5 2113.85 2087.21 57.82 o 7 1 5 979.10 930.29 57.14 o 9 1 5 2855.65 2507.35 143.65 o 11 1 5 2246.32 2200.83 135.78 o 13 1 5 3235.52 3014.43 106.97 o 15 1 5 923.02 939.51 77.81 o 1 3 5 3634.50 3599.71 82.96 o 3 3 5 2287.64 2155.12 61.86 o 5 3 5 4048.14 4161.19 76.22 o 7 3 5 3782.40 3461.42 90.55 o 9 3 5 5741.29 5490.78 110.46 o 11 3 5 746.65 671.49 100.69 o 13 3 5 4505.17 4020.40 117.15 o 15 3 5 2094.07 2252.52 105.83 o 1 5 5 15873.53 16104.03 217.40 o 3 5 5 4023.46 3984.83 93.79 o 5 5 5 4749.12 4622.42 79.29 o 7 5 5 513.36 412.36 47.42 o 9 5 5 1484.60 1460.01 85.52 o 11 5 5 363.02 350.98 49.40 o 13 5 5 109.58 87.47 82.86 o 15 5 5 283.47 341.56 95.42 o 1 7 5 5112.60 5141.34 96.34 o 3 7 5 6101.93 6147.00 117.71 o 5 7 5 2801.29 2624.50 88.23 o 7 7 5 2468.59 2292.21 85.13 o 9 7 5 11155.36 10591.48 183.48 o 11 7 5 2919.73 2981.57 89.56 o 13 7 5 1406.62 1595.18 59.11 o 15 7 5 393.89 315.26 65.04 o 1 9 5 1836.43 2007.24 74.60 o 3 9 5 9970.65 9723.08 137.46 o 5 9 5 940.11 866.25 57.37 o 7 9 5 78.03 120.45 48.58 o 9 9 5 782.38 794.14 64.27 o 11 9 5 60.62 128.08 55.69 o 13 9 5 1339.93 1301.50 58.50 o 15 9 5 367.03 566.48 64.56 o 1 11 5 5364.38 5360.85 154.64 o 3 11 5 7890.09 7879.89 120.74 o 5 11 5 714.26 769.41 58.91 o 7 11 5 2268.23 2335.95 97.10 o 9 11 5 592.57 682.37 63.75 o 11 11 5 4840.30 4932.42 124.51 o 13 11 5 1953.43 1926.22 106.80 o 1 13 5 2188.47 2255.52 69.18 o 3 13 5 1754.08 1762.08 60.46 o 5 13 5 569.12 627.59 60.16 o 7 13 5 2052.71 1942.56 94.15 o 9 13 5 390.27 324.09 61.76 o 11 13 5 2057.35 2111.13 112.37 o 13 13 5 1649.98 1630.99 87.45 o 1 15 5 2116.45 2140.59 77.37 o 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4751.48 142.44 o 2 6 6 391.95 371.25 44.70 o 4 6 6 3259.44 3221.54 81.58 o 6 6 6 234.06 189.87 55.64 o 8 6 6 1688.73 1463.77 85.46 o 10 6 6 429.45 461.04 51.24 o 12 6 6 139.22 230.32 123.68 o 2 8 6 8320.55 8172.50 134.96 o 4 8 6 1904.81 1994.52 65.76 o 6 8 6 5375.64 5783.98 141.59 o 8 8 6 667.56 686.98 71.93 o 10 8 6 2233.23 2468.48 128.42 o 0 10 6 9274.59 8816.15 307.40 o 2 10 6 1513.27 1586.81 69.20 o 4 10 6 4929.59 4966.63 95.58 o 6 10 6 413.36 443.85 66.22 o 8 10 6 492.95 605.68 90.28 o 10 10 6 839.89 781.84 76.19 o 2 12 6 5310.09 5512.28 109.82 o 4 12 6 1697.76 1617.69 55.36 o 6 12 6 4445.77 4648.45 140.25 o 8 12 6 770.19 755.85 76.33 o 10 12 6 1108.16 1083.89 88.73 o 0 14 6 6139.21 6231.96 168.21 o 2 14 6 299.82 257.20 51.70 o 4 14 6 4537.84 4584.98 136.32 o 6 14 6 852.60 756.99 77.99 o 8 14 6 3242.12 3363.79 138.95 o 10 14 6 826.94 990.44 93.82 o 2 16 6 2282.51 2495.21 89.34 o 4 16 6 192.06 155.92 71.36 o 6 16 6 3265.74 3573.79 156.82 o 8 16 6 1370.66 1303.48 99.61 o 0 18 6 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