#------------------------------------------------------------------------------ #$Date: 2016-04-06 14:21:12 +0300 (Wed, 06 Apr 2016) $ #$Revision: 181861 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/24/1542483.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1542483 _cell_angle_alpha 90.000 _cell_angle_beta 112.276 _cell_angle_gamma 90.000 _cell_length_a 12.1802 _cell_length_b 7.3646 _cell_length_c 13.9001 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.7699 _cod_data_source_file hb4004Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 212.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 206.30 187.62 21.22 o 3 0 0 11.69 23.43 4.15 o 5 0 0 123.02 121.79 5.59 o 6 0 0 3.76 1.48 2.29 o 7 0 0 434.78 457.59 16.36 o 8 0 0 17.28 19.66 2.89 o 9 0 0 56.40 54.57 8.16 o 10 0 0 385.85 358.15 19.66 o 11 0 0 423.87 385.17 21.94 o 12 0 0 16.10 9.86 6.52 o 13 0 0 375.35 398.98 41.13 o 14 0 0 488.61 490.93 36.08 o 1 1 0 486.24 364.12 46.16 o 2 1 0 162.12 137.69 4.84 o 3 1 0 1345.04 1242.68 21.48 o 4 1 0 2534.17 2283.76 45.14 o 5 1 0 65.44 91.23 4.33 o 6 1 0 323.72 287.49 8.79 o 7 1 0 255.70 208.51 9.16 o 8 1 0 30.33 29.12 3.39 o 9 1 0 345.30 328.16 10.13 o 10 1 0 1964.26 2025.60 46.14 o 11 1 0 60.36 49.23 4.09 o 12 1 0 0.70 3.90 2.90 o 13 1 0 4.92 1.21 4.67 o 14 1 0 109.39 97.97 10.13 o 0 2 0 8269.64 8031.60 212.94 o 1 2 0 170.09 201.74 5.69 o 2 2 0 273.74 261.59 7.35 o 3 2 0 75.59 85.84 3.56 o 4 2 0 134.38 147.88 4.70 o 5 2 0 182.28 213.74 5.33 o 6 2 0 1.34 8.16 2.32 o 7 2 0 260.49 259.91 7.67 o 8 2 0 143.14 147.56 7.22 o 9 2 0 0.02 3.28 2.88 o 10 2 0 29.58 42.76 3.88 o 11 2 0 0.18 -3.11 3.20 o 12 2 0 41.87 25.04 9.45 o 13 2 0 30.76 41.21 9.66 o 14 2 0 19.50 16.91 10.37 o 1 3 0 1978.75 2081.83 32.38 o 2 3 0 11.28 4.83 2.77 o 3 3 0 1407.72 1276.84 24.74 o 4 3 0 1177.25 1097.96 27.86 o 5 3 0 128.00 140.03 5.28 o 6 3 0 95.56 77.97 3.86 o 7 3 0 769.82 718.15 16.59 o 8 3 0 13.48 16.27 3.47 o 9 3 0 931.98 961.80 29.00 o 10 3 0 2211.89 2294.37 69.72 o 11 3 0 208.01 190.30 11.91 o 12 3 0 7.64 7.37 7.71 o 13 3 0 135.95 131.00 19.99 o 0 4 0 22997.44 23790.70 550.13 o 1 4 0 1666.07 1678.11 33.84 o 2 4 0 421.20 453.21 14.86 o 3 4 0 896.31 799.83 23.32 o 4 4 0 3013.84 3152.92 70.92 o 5 4 0 117.82 119.99 7.07 o 6 4 0 0.08 -1.87 2.37 o 7 4 0 20.26 20.83 3.76 o 8 4 0 37.28 45.66 4.71 o 9 4 0 52.96 55.81 5.83 o 10 4 0 86.76 93.71 7.10 o 11 4 0 466.44 472.12 29.09 o 12 4 0 145.29 163.28 19.16 o 13 4 0 168.96 247.26 30.56 o 1 5 0 1263.64 1356.35 30.89 o 2 5 0 4.17 9.63 4.19 o 3 5 0 346.66 342.40 12.07 o 4 5 0 457.29 435.97 14.60 o 5 5 0 1.63 0.25 3.31 o 6 5 0 217.66 212.51 9.37 o 7 5 0 13.01 8.26 3.07 o 8 5 0 10.55 15.68 3.99 o 9 5 0 22.11 23.57 4.63 o 10 5 0 215.88 229.26 11.09 o 11 5 0 0.15 -12.69 12.99 o 12 5 0 0.46 11.54 18.05 o 0 6 0 1008.66 1133.43 50.27 o 1 6 0 1177.49 1139.36 32.02 o 2 6 0 9.36 21.61 5.09 o 3 6 0 1653.75 1668.96 51.37 o 4 6 0 1.09 11.93 4.12 o 5 6 0 18.87 7.25 5.43 o 6 6 0 42.50 40.49 5.46 o 7 6 0 330.82 304.64 14.82 o 8 6 0 102.00 99.33 9.23 o 9 6 0 4.18 11.94 8.28 o 10 6 0 23.55 17.63 26.04 o 11 6 0 70.96 62.03 16.81 o 1 7 0 26.58 15.44 5.56 o 2 7 0 169.65 165.31 10.61 o 3 7 0 490.81 507.68 25.48 o 4 7 0 411.95 414.94 28.95 o 5 7 0 4.02 6.77 5.33 o 6 7 0 16.73 31.82 8.96 o 7 7 0 452.30 452.62 22.21 o 8 7 0 79.42 61.88 11.44 o 9 7 0 248.42 239.13 29.00 o 0 8 0 986.75 1028.46 71.31 o 1 8 0 106.16 97.86 17.73 o 2 8 0 64.55 37.91 14.04 o 3 8 0 2.53 12.55 8.11 o 4 8 0 173.56 147.22 16.29 o 5 8 0 1.80 -0.69 11.17 o 6 8 0 19.52 26.72 12.04 o 7 8 0 14.84 2.98 9.25 o 1 9 0 75.80 58.26 17.37 o 2 9 0 230.44 229.67 45.85 o 3 9 0 30.82 25.74 20.23 o 4 9 0 0.83 -6.73 11.40 o -14 1 1 0.02 -3.63 11.82 o -13 1 1 66.01 64.88 8.97 o -12 1 1 233.83 230.66 12.01 o -11 1 1 6.70 4.49 2.14 o -10 1 1 300.75 322.49 8.97 o -9 1 1 2616.99 2691.69 66.91 o -8 1 1 556.12 560.58 15.23 o -7 1 1 237.86 216.10 7.77 o -6 1 1 6.13 0.66 2.00 o -5 1 1 1214.55 1087.99 17.39 o -4 1 1 1238.41 1164.10 22.24 o -3 1 1 10969.83 9844.41 161.33 o -2 1 1 133.17 130.92 4.75 o -1 1 1 6440.26 3014.32 291.37 o 0 1 1 5501.58 5217.46 129.71 o 1 1 1 100.93 80.71 4.08 o 2 1 1 0.41 3.66 1.84 o 3 1 1 33.60 37.80 2.53 o 4 1 1 4235.59 3894.78 72.30 o 5 1 1 3100.97 3105.32 60.87 o 6 1 1 176.83 247.71 6.78 o 7 1 1 694.77 642.62 15.42 o 8 1 1 1054.40 1023.52 23.00 o 9 1 1 105.31 84.80 5.08 o 10 1 1 699.03 664.63 24.59 o 11 1 1 1547.60 1656.41 57.88 o 12 1 1 15.66 13.59 6.23 o 13 1 1 48.96 45.69 7.68 o 14 1 1 5.04 14.45 7.02 o -14 2 1 0.94 3.83 16.23 o -13 2 1 171.23 172.94 12.37 o -12 2 1 311.09 356.06 15.39 o -11 2 1 7.58 5.09 3.11 o -10 2 1 208.04 219.95 9.02 o -9 2 1 49.91 55.54 6.30 o -8 2 1 663.13 667.09 15.33 o -7 2 1 199.81 207.58 6.08 o -6 2 1 536.32 527.27 9.61 o -5 2 1 304.51 238.22 5.86 o -4 2 1 200.00 199.45 5.24 o -3 2 1 1790.02 1589.29 30.88 o -2 2 1 2511.92 2137.92 36.78 o -1 2 1 6866.48 6892.90 129.90 o 0 2 1 16443.42 15493.81 319.36 o 1 2 1 45007.51 43804.91 1319.62 o 2 2 1 50.12 45.86 3.34 o 3 2 1 159.82 145.29 5.19 o 4 2 1 3472.40 3251.98 69.93 o 5 2 1 6010.52 5986.26 96.30 o 6 2 1 421.90 420.69 11.73 o 7 2 1 10.45 17.29 2.92 o 8 2 1 146.36 149.79 9.91 o 9 2 1 80.28 76.03 5.16 o 10 2 1 427.63 418.49 16.02 o 11 2 1 664.88 650.01 36.30 o 12 2 1 18.56 29.95 10.15 o 13 2 1 27.92 34.16 12.26 o -14 3 1 60.56 48.94 25.56 o -13 3 1 39.06 38.41 14.53 o -12 3 1 88.19 68.20 8.71 o -11 3 1 50.67 57.05 5.29 o -10 3 1 3.45 4.29 3.77 o -9 3 1 858.43 913.91 22.48 o -8 3 1 210.52 209.04 7.30 o -7 3 1 72.95 87.68 4.29 o -6 3 1 164.25 146.71 4.97 o -5 3 1 276.11 248.62 8.39 o -4 3 1 208.83 216.46 6.67 o -3 3 1 255.75 281.24 6.76 o -2 3 1 340.32 296.08 8.08 o -1 3 1 140.43 136.18 4.95 o 0 3 1 102.95 101.18 5.59 o 1 3 1 410.02 456.57 11.59 o 2 3 1 97.40 107.51 7.49 o 3 3 1 30.32 31.99 3.04 o 4 3 1 2289.50 2215.26 40.61 o 5 3 1 198.39 193.58 6.74 o 6 3 1 59.11 57.83 5.02 o 7 3 1 0.71 0.14 2.51 o 8 3 1 573.04 626.82 17.44 o 9 3 1 22.64 17.59 3.71 o 10 3 1 163.52 165.80 9.28 o 11 3 1 158.71 172.77 9.64 o 12 3 1 242.75 160.90 38.74 o 13 3 1 9.28 -5.41 8.97 o -13 4 1 0.45 -2.91 26.10 o -12 4 1 69.82 50.98 11.49 o -11 4 1 3.07 7.72 5.64 o -10 4 1 15.75 24.59 5.11 o -9 4 1 69.76 74.56 5.28 o -8 4 1 1.76 3.59 2.82 o -7 4 1 3.98 5.34 3.01 o -6 4 1 66.90 59.70 5.52 o -5 4 1 231.95 248.76 8.30 o -4 4 1 80.99 75.97 4.76 o -3 4 1 19.65 23.13 3.43 o -2 4 1 2839.78 2972.68 54.29 o -1 4 1 2111.04 2326.12 46.56 o 0 4 1 1716.49 1707.13 38.65 o 1 4 1 572.31 567.43 16.39 o 2 4 1 230.42 220.17 7.86 o 3 4 1 227.58 226.98 9.91 o 4 4 1 634.09 619.70 15.47 o 5 4 1 310.29 340.94 11.08 o 6 4 1 136.40 119.86 7.18 o 7 4 1 52.98 54.16 6.22 o 8 4 1 0.04 -0.16 3.18 o 9 4 1 12.19 6.99 3.90 o 10 4 1 0.80 3.98 4.24 o 11 4 1 130.16 104.13 16.15 o 12 4 1 77.52 -22.12 43.53 o -12 5 1 330.30 333.35 35.95 o -11 5 1 17.64 16.37 10.94 o -10 5 1 258.62 267.13 14.64 o -9 5 1 1064.34 1143.52 32.70 o -8 5 1 493.96 555.14 16.53 o -7 5 1 5.85 5.71 3.34 o -6 5 1 776.81 790.35 23.60 o -5 5 1 227.17 204.17 10.21 o -4 5 1 102.88 101.31 6.11 o -3 5 1 212.41 216.86 7.39 o -2 5 1 153.37 132.53 6.58 o -1 5 1 60.43 65.76 6.24 o 0 5 1 13.01 7.52 4.16 o 1 5 1 156.15 150.27 7.32 o 2 5 1 351.79 352.88 16.80 o 3 5 1 81.05 82.39 9.14 o 4 5 1 1556.22 1575.93 45.30 o 5 5 1 621.52 628.27 18.73 o 6 5 1 141.87 129.77 7.46 o 7 5 1 199.21 209.52 8.65 o 8 5 1 1029.41 1109.67 37.53 o 9 5 1 275.40 285.20 14.52 o 10 5 1 562.85 569.43 40.61 o 11 5 1 470.05 539.47 38.67 o 12 5 1 189.87 189.42 34.83 o -11 6 1 11.18 9.24 11.99 o -10 6 1 125.67 93.53 25.65 o -9 6 1 17.52 7.31 6.43 o -8 6 1 104.63 111.25 9.11 o -7 6 1 32.72 40.65 5.93 o -6 6 1 44.03 39.60 6.67 o -5 6 1 474.01 480.40 17.83 o -4 6 1 201.93 212.28 8.59 o -3 6 1 329.68 321.59 14.06 o -2 6 1 2.91 5.55 4.55 o -1 6 1 0.73 3.30 3.56 o 0 6 1 852.44 849.31 24.72 o 1 6 1 4706.19 5118.55 142.97 o 2 6 1 121.10 110.31 7.62 o 3 6 1 0.08 1.06 4.28 o 4 6 1 482.96 460.24 18.44 o 5 6 1 375.62 369.83 14.46 o 6 6 1 1.69 4.34 5.34 o 7 6 1 58.82 54.44 8.14 o 8 6 1 122.28 119.36 11.75 o 9 6 1 19.14 9.38 5.98 o 10 6 1 218.50 203.12 21.95 o 11 6 1 48.36 45.33 16.72 o -10 7 1 111.22 124.95 19.80 o -9 7 1 73.92 28.89 13.63 o -8 7 1 7.61 13.44 9.02 o -7 7 1 157.48 163.22 13.64 o -6 7 1 32.86 23.89 13.51 o -5 7 1 5.81 11.46 12.81 o -4 7 1 21.48 23.13 7.89 o -3 7 1 244.12 236.09 13.64 o -2 7 1 57.96 42.67 5.95 o -1 7 1 12.90 11.75 4.96 o 0 7 1 41.44 34.85 5.69 o 1 7 1 512.81 506.55 21.97 o 2 7 1 409.99 431.72 20.07 o 3 7 1 0.21 0.28 7.48 o 4 7 1 217.09 211.51 21.94 o 5 7 1 0.11 5.87 6.58 o 6 7 1 164.46 157.12 12.64 o 7 7 1 10.78 8.47 6.79 o 8 7 1 0.11 9.20 9.82 o 9 7 1 32.02 39.06 11.39 o -8 8 1 0.07 -10.39 12.50 o -7 8 1 11.61 9.57 11.64 o -6 8 1 7.39 -4.66 9.82 o -5 8 1 15.73 0.69 16.81 o -4 8 1 18.79 9.17 7.22 o -3 8 1 99.60 79.51 13.99 o -2 8 1 159.72 152.28 21.38 o -1 8 1 89.68 96.54 21.83 o 0 8 1 373.90 343.38 37.32 o 1 8 1 849.98 900.61 59.75 o 2 8 1 78.96 95.84 13.75 o 3 8 1 73.54 87.42 15.63 o 4 8 1 284.09 286.12 21.67 o 5 8 1 35.40 8.19 9.92 o 6 8 1 12.79 5.62 15.38 o 7 8 1 2.21 14.62 21.39 o -5 9 1 4.69 0.85 11.96 o -4 9 1 23.67 35.90 13.62 o -3 9 1 41.55 47.40 19.30 o -2 9 1 93.93 111.85 19.81 o -1 9 1 0.93 4.46 17.15 o 0 9 1 21.13 29.42 12.98 o 1 9 1 3.34 3.32 12.53 o 2 9 1 2.12 -5.48 14.67 o 3 9 1 6.67 18.99 12.89 o 4 9 1 205.62 239.48 30.70 o -15 0 2 463.47 501.40 74.68 o -14 0 2 833.03 867.80 93.29 o -13 0 2 3.84 24.08 18.08 o -12 0 2 72.53 92.93 14.13 o -11 0 2 727.87 755.09 39.13 o -10 0 2 24.69 23.25 2.78 o -9 0 2 50.13 43.86 3.99 o -8 0 2 919.44 978.28 42.88 o -7 0 2 5017.51 5000.54 165.03 o -6 0 2 4619.40 4456.71 117.48 o -5 0 2 922.15 898.14 51.06 o -4 0 2 21849.19 20345.02 946.21 o -3 0 2 20889.93 19983.91 951.05 o -2 0 2 456.27 442.60 17.77 o -1 0 2 1.20 -3.07 2.05 o 0 0 2 268.63 162.81 17.90 o 1 0 2 14616.87 14167.05 627.54 o 2 0 2 12543.40 11071.28 1189.89 o 3 0 2 10.13 16.58 3.47 o 4 0 2 2152.20 2116.85 60.26 o 5 0 2 3177.12 3135.72 109.66 o 6 0 2 1235.08 1298.02 37.99 o 7 0 2 538.44 560.23 26.94 o 8 0 2 145.66 154.33 8.12 o 9 0 2 51.64 48.23 10.52 o 10 0 2 7.34 7.13 7.31 o 11 0 2 735.87 698.40 31.29 o 12 0 2 341.08 281.44 52.57 o 13 0 2 37.58 42.51 12.49 o -15 1 2 5.18 -30.74 24.08 o -14 1 2 95.78 65.39 26.65 o -13 1 2 9.58 1.38 3.11 o -12 1 2 235.36 222.88 11.49 o -11 1 2 121.89 118.23 6.02 o -10 1 2 95.11 89.39 4.18 o -9 1 2 81.31 80.19 3.76 o -8 1 2 2631.75 2575.34 43.96 o -7 1 2 24.84 21.33 1.87 o -6 1 2 19.77 32.87 2.68 o -5 1 2 1168.98 1074.67 18.03 o -4 1 2 2443.14 2263.31 42.33 o -3 1 2 1546.81 1483.56 26.91 o -2 1 2 117.96 114.63 4.46 o -1 1 2 56.24 49.90 3.09 o 0 1 2 0.61 -0.49 1.93 o 1 1 2 55.64 54.35 2.83 o 2 1 2 343.06 338.60 9.65 o 3 1 2 142.28 152.80 7.97 o 4 1 2 129.95 124.76 5.33 o 5 1 2 1974.14 1884.04 33.02 o 6 1 2 1640.22 1677.00 37.75 o 7 1 2 361.41 345.78 12.97 o 8 1 2 441.52 493.85 16.62 o 9 1 2 172.06 164.58 8.11 o 10 1 2 0.95 0.62 4.33 o 11 1 2 404.25 392.34 16.21 o 12 1 2 428.67 435.89 26.78 o 13 1 2 0.40 -5.20 7.12 o -14 2 2 73.64 66.48 14.23 o -13 2 2 0.09 0.55 6.75 o -12 2 2 29.77 24.59 4.00 o -11 2 2 2.23 -0.85 1.93 o -10 2 2 41.35 42.89 4.34 o -9 2 2 14.05 15.86 2.56 o -8 2 2 1.04 -1.67 1.63 o -7 2 2 112.30 111.09 3.99 o -6 2 2 372.02 378.85 7.48 o -5 2 2 2.50 2.24 1.48 o -4 2 2 880.53 829.69 13.58 o -3 2 2 448.22 501.00 10.00 o -2 2 2 86.18 76.34 2.89 o -1 2 2 55.70 74.63 3.16 o 0 2 2 721.23 841.43 21.45 o 1 2 2 51.93 61.68 3.78 o 2 2 2 298.95 281.24 8.19 o 3 2 2 234.06 238.43 8.47 o 4 2 2 978.22 1038.91 32.77 o 5 2 2 1.16 -1.46 2.85 o 6 2 2 14.71 19.59 3.23 o 7 2 2 1.42 4.48 3.80 o 8 2 2 74.01 75.00 4.98 o 9 2 2 61.64 55.22 5.40 o 10 2 2 0.07 4.68 4.69 o 11 2 2 141.57 135.31 9.01 o 12 2 2 12.89 8.55 9.56 o 13 2 2 26.31 25.11 10.88 o -14 3 2 46.03 18.27 13.62 o -13 3 2 5.14 7.10 10.55 o -12 3 2 254.84 258.34 14.20 o -11 3 2 334.62 339.89 13.35 o -10 3 2 6.51 4.05 2.71 o -9 3 2 72.62 66.27 4.39 o -8 3 2 2174.54 2202.20 43.05 o -7 3 2 568.21 565.45 14.12 o -6 3 2 2.86 7.47 3.85 o -5 3 2 2431.39 2314.06 39.49 o -4 3 2 1020.45 905.39 21.42 o -3 3 2 891.00 919.61 16.84 o -2 3 2 121.42 185.94 5.13 o -1 3 2 129.98 152.79 5.59 o 0 3 2 131.20 129.65 8.64 o 1 3 2 134.31 149.25 6.09 o 2 3 2 270.41 274.66 10.06 o 3 3 2 45.29 46.15 4.26 o 4 3 2 193.25 180.21 6.51 o 5 3 2 3482.63 3643.29 71.66 o 6 3 2 1354.94 1382.40 31.24 o 7 3 2 119.53 114.09 7.42 o 8 3 2 727.13 724.21 19.48 o 9 3 2 445.61 475.87 18.93 o 10 3 2 249.67 243.58 15.38 o 11 3 2 329.37 325.16 22.41 o 12 3 2 438.61 469.24 66.68 o 13 3 2 29.35 -5.85 21.88 o -13 4 2 0.00 -0.54 11.51 o -12 4 2 34.74 37.55 7.85 o -11 4 2 328.22 355.91 15.85 o -10 4 2 14.44 8.86 3.25 o -9 4 2 158.03 153.41 6.19 o -8 4 2 161.90 184.34 6.67 o -7 4 2 249.12 258.35 8.87 o -6 4 2 79.17 73.58 4.70 o -5 4 2 495.35 465.83 12.26 o -4 4 2 1240.80 1178.90 23.98 o -3 4 2 901.09 971.91 20.12 o -2 4 2 2.99 10.05 2.64 o -1 4 2 1298.12 1198.41 23.37 o 0 4 2 105.26 116.63 9.28 o 1 4 2 4525.37 4949.64 101.12 o 2 4 2 2993.78 2835.49 55.20 o 3 4 2 0.21 1.39 2.05 o 4 4 2 85.14 79.46 5.91 o 5 4 2 1853.73 2008.45 42.51 o 6 4 2 646.22 693.36 21.31 o 7 4 2 279.05 302.69 11.57 o 8 4 2 353.94 362.60 13.96 o 9 4 2 244.11 246.52 14.11 o 10 4 2 0.89 4.09 5.88 o 11 4 2 56.10 58.06 15.37 o 12 4 2 472.61 517.48 85.69 o -13 5 2 45.38 32.35 15.72 o -12 5 2 39.65 64.34 18.08 o -11 5 2 30.37 14.83 8.14 o -10 5 2 78.11 64.49 6.55 o -9 5 2 12.40 5.47 3.95 o -8 5 2 750.96 789.30 24.84 o -7 5 2 142.73 156.23 7.67 o -6 5 2 41.60 45.75 4.63 o -5 5 2 226.51 232.43 9.06 o -4 5 2 725.54 702.30 20.24 o -3 5 2 36.60 36.41 3.72 o -2 5 2 238.70 259.61 10.87 o -1 5 2 24.02 28.50 4.33 o 0 5 2 112.91 122.26 7.78 o 1 5 2 338.45 389.19 15.38 o 2 5 2 10.89 8.04 5.10 o 3 5 2 224.08 244.53 9.76 o 4 5 2 47.80 46.24 8.22 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