data_1542540 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.9771 _cell_length_b 12.8680 _cell_length_c 14.5449 _exptl_crystal_F_000 720.00 _reflns_d_resolution_high 0.7109 _cod_data_source_file wm4007Isup2.hkl _cod_data_source_block I _shelx_title ' Cs [N (C H3)4] [B12 H12] * H2 O (tir02, P212121)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 301.04 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 90626.06 82417.77 160.43 o 4 0 0 7318.83 6712.70 67.67 o 6 0 0 1894.78 1833.51 40.32 o 8 0 0 8.37 27.00 9.79 o 10 0 0 548.28 568.27 20.08 o 12 0 0 666.05 682.36 25.06 o 1 1 0 360.65 360.41 9.22 o 2 1 0 3650.01 3465.94 36.88 o 3 1 0 8738.72 8801.87 90.94 o 4 1 0 447.47 378.98 22.14 o 5 1 0 10961.85 10710.48 270.77 o 6 1 0 1011.66 962.66 21.46 o 7 1 0 7998.85 7659.16 248.44 o 8 1 0 1101.24 1098.10 21.66 o 9 1 0 4267.83 4139.03 80.62 o 10 1 0 411.99 417.68 12.70 o 11 1 0 1064.47 1026.60 57.45 o 12 1 0 34.19 23.07 21.93 o 0 2 0 15405.09 17535.37 61.69 o 1 2 0 2589.53 2808.83 116.93 o 2 2 0 8553.89 8579.97 59.71 o 3 2 0 11128.99 10999.58 76.80 o 4 2 0 2286.42 2297.67 43.82 o 5 2 0 1840.61 1872.24 44.25 o 6 2 0 13.18 34.61 8.35 o 7 2 0 19.61 22.22 10.18 o 8 2 0 330.47 334.73 15.62 o 9 2 0 182.11 203.55 13.25 o 10 2 0 258.90 250.55 15.46 o 11 2 0 287.00 303.81 17.33 o 12 2 0 581.95 593.09 23.73 o 1 3 0 370.58 395.07 19.73 o 2 3 0 1497.69 1574.84 30.61 o 3 3 0 4358.00 4284.35 52.17 o 4 3 0 3877.82 3671.68 54.85 o 5 3 0 2166.10 2068.37 46.89 o 6 3 0 3797.53 3606.34 67.75 o 7 3 0 1235.88 1247.52 36.09 o 8 3 0 2327.51 2419.84 56.02 o 9 3 0 1139.95 1152.20 29.99 o 10 3 0 2401.41 2484.75 58.46 o 11 3 0 250.36 228.33 16.04 o 12 3 0 687.20 723.50 25.95 o 0 4 0 3960.89 4100.61 44.75 o 1 4 0 48763.22 52180.18 194.89 o 2 4 0 928.57 971.88 22.88 o 3 4 0 25880.66 25751.32 130.60 o 4 4 0 187.12 172.09 9.44 o 5 4 0 3961.98 3640.45 62.58 o 6 4 0 95.40 94.32 10.10 o 7 4 0 97.75 81.07 12.04 o 8 4 0 225.40 223.40 12.31 o 9 4 0 164.63 176.20 12.66 o 10 4 0 3.32 21.37 12.12 o 11 4 0 488.05 485.53 21.95 o 12 4 0 107.00 96.22 15.85 o 1 5 0 8.67 24.26 4.22 o 2 5 0 3318.83 3468.48 50.27 o 3 5 0 125.88 149.44 8.55 o 4 5 0 6227.36 6326.73 76.99 o 5 5 0 242.24 244.11 12.24 o 6 5 0 8947.50 8120.89 102.75 o 7 5 0 458.51 441.13 17.64 o 8 5 0 6111.61 5875.62 102.86 o 9 5 0 10.52 0.35 11.23 o 10 5 0 3507.67 3443.23 79.52 o 11 5 0 0.90 19.11 13.17 o 12 5 0 1032.22 1010.14 33.10 o 0 6 0 4616.02 4912.52 60.33 o 1 6 0 8988.22 9837.93 59.77 o 2 6 0 1883.02 1898.65 41.80 o 3 6 0 5981.60 6257.55 75.59 o 4 6 0 153.49 166.10 10.06 o 5 6 0 1915.42 1850.60 42.50 o 6 6 0 24.67 28.40 9.83 o 7 6 0 255.76 238.32 13.40 o 8 6 0 81.83 93.27 10.72 o 9 6 0 728.25 676.61 23.07 o 10 6 0 530.43 528.07 21.44 o 11 6 0 912.18 943.67 29.10 o 1 7 0 754.48 823.01 28.49 o 2 7 0 612.19 589.29 17.67 o 3 7 0 1956.70 2210.78 51.43 o 4 7 0 746.91 714.49 21.48 o 5 7 0 2812.04 2651.01 61.80 o 6 7 0 1530.23 1514.08 38.88 o 7 7 0 3845.91 3527.29 80.60 o 8 7 0 1368.18 1295.27 33.91 o 9 7 0 1469.01 1411.80 38.15 o 10 7 0 829.84 813.43 26.73 o 11 7 0 309.96 283.73 17.05 o 0 8 0 19846.90 20641.54 138.68 o 1 8 0 2201.18 2416.85 143.11 o 2 8 0 14375.61 14443.70 121.35 o 3 8 0 783.68 859.30 22.76 o 4 8 0 3159.33 3107.14 66.97 o 5 8 0 2.44 -9.56 9.56 o 6 8 0 83.95 103.80 10.57 o 7 8 0 18.00 27.77 10.02 o 8 8 0 33.84 66.27 10.80 o 9 8 0 1.75 -10.02 11.50 o 10 8 0 210.32 179.35 14.96 o 11 8 0 18.62 27.39 14.18 o 1 9 0 91.37 110.44 7.20 o 2 9 0 52.17 62.04 9.36 o 3 9 0 2319.52 2260.96 48.95 o 4 9 0 214.31 216.56 13.56 o 5 9 0 6722.23 5995.15 96.88 o 6 9 0 61.82 48.40 9.98 o 7 9 0 4063.37 3759.04 89.11 o 8 9 0 85.74 58.31 11.65 o 9 9 0 1892.15 1807.87 43.51 o 10 9 0 26.03 31.19 13.01 o 0 10 0 12489.34 12962.13 127.45 o 1 10 0 83.71 98.17 12.28 o 2 10 0 10748.01 10677.31 119.84 o 3 10 0 66.69 72.37 9.79 o 4 10 0 3755.66 3703.57 78.12 o 5 10 0 39.64 31.08 9.52 o 6 10 0 280.76 248.03 14.10 o 7 10 0 316.68 310.53 15.11 o 8 10 0 106.08 112.19 12.31 o 9 10 0 81.08 85.34 13.36 o 10 10 0 462.42 436.70 19.15 o 1 11 0 560.89 575.41 18.47 o 2 11 0 920.68 884.51 23.93 o 3 11 0 2415.59 2316.79 53.30 o 4 11 0 1077.92 1039.66 26.61 o 5 11 0 1847.45 1640.10 38.15 o 6 11 0 439.42 413.39 16.94 o 7 11 0 1232.16 1164.78 32.90 o 8 11 0 851.22 793.07 25.25 o 9 11 0 1033.55 992.11 29.21 o 10 11 0 181.47 168.36 16.04 o 0 12 0 2319.02 2402.36 55.16 o 1 12 0 6613.13 6797.43 265.02 o 2 12 0 1887.97 1799.67 43.51 o 3 12 0 2875.83 2706.10 60.91 o 4 12 0 517.10 468.17 16.94 o 5 12 0 1435.34 1269.01 31.00 o 6 12 0 86.31 79.32 11.69 o 7 12 0 33.45 25.37 12.39 o 8 12 0 118.12 98.47 13.52 o 9 12 0 100.70 102.40 14.41 o 1 13 0 65.23 76.67 7.40 o 2 13 0 246.11 258.32 13.63 o 3 13 0 156.79 144.31 12.08 o 4 13 0 1211.20 1121.00 31.00 o 5 13 0 1.67 5.13 10.22 o 6 13 0 1644.77 1536.85 39.31 o 7 13 0 0.91 -6.76 12.59 o 8 13 0 1614.07 1573.79 41.99 o 0 14 0 187.00 203.01 12.86 o 1 14 0 4144.68 4173.91 205.09 o 2 14 0 74.27 79.13 10.80 o 3 14 0 1600.02 1662.08 39.16 o 4 14 0 14.94 31.39 11.15 o 5 14 0 869.91 827.95 23.39 o 6 14 0 4.28 1.40 12.55 o 7 14 0 79.92 89.69 13.71 o 8 14 0 7.36 1.59 13.32 o 1 15 0 3.74 8.70 7.92 o 2 15 0 36.33 24.20 11.27 o 3 15 0 1.26 1.09 11.11 o 4 15 0 860.74 839.72 24.63 o 5 15 0 150.44 146.14 13.52 o 6 15 0 1029.94 1053.65 29.41 o 7 15 0 123.00 124.58 14.61 o 0 16 0 549.81 546.83 20.36 o 1 16 0 1335.80 1341.78 25.96 o 2 16 0 1312.56 1237.27 33.68 o 3 16 0 255.54 264.69 15.19 o 4 16 0 834.88 816.69 24.51 o 5 16 0 27.32 3.42 12.62 o 1 17 0 109.79 116.72 15.91 o 2 17 0 34.20 26.41 12.94 o 3 17 0 317.84 279.69 16.12 o 4 17 0 4.05 -1.28 12.70 o 0 18 0 966.79 1011.77 21.42 o 1 18 0 17.59 8.21 18.06 o 1 0 1 9122.63 9317.63 107.50 o 2 0 1 4551.35 4891.48 177.87 o 3 0 1 3964.13 3699.73 31.85 o 4 0 1 7071.12 6876.78 48.95 o 5 0 1 986.34 889.60 16.20 o 6 0 1 6689.35 6400.84 68.87 o 7 0 1 0.27 3.43 6.61 o 8 0 1 2901.44 3126.00 131.88 o 9 0 1 131.89 130.36 10.60 o 10 0 1 1638.89 1649.36 44.11 o 11 0 1 226.03 217.57 19.38 o 12 0 1 247.77 251.10 12.90 o -12 1 1 273.49 253.14 12.42 o -11 1 1 499.83 534.48 37.39 o -10 1 1 659.69 678.32 23.11 o -9 1 1 179.54 158.72 13.63 o -8 1 1 1495.66 1456.01 35.82 o -7 1 1 234.17 227.71 14.37 o -6 1 1 2070.70 1848.78 40.24 o -5 1 1 4686.10 4610.54 64.76 o -4 1 1 3189.73 3165.33 49.10 o -3 1 1 18945.63 17920.99 94.51 o -2 1 1 2042.89 2159.58 32.44 o -1 1 1 4641.53 4338.80 58.96 o 0 1 1 3104.07 3483.27 49.47 o 1 1 1 4999.97 4756.31 48.74 o 2 1 1 2098.25 2275.72 56.94 o 3 1 1 19303.73 19576.76 181.35 o 4 1 1 3195.01 3299.92 45.93 o 5 1 1 4853.77 4705.60 55.19 o 6 1 1 1992.29 1996.07 39.62 o 7 1 1 285.77 288.43 20.32 o 8 1 1 1454.58 1431.08 28.94 o 9 1 1 165.25 175.06 7.38 o 10 1 1 674.53 671.11 13.47 o 11 1 1 509.25 534.81 15.64 o 12 1 1 264.12 267.04 30.34 o -2 2 1 3978.99 4236.45 43.70 o -1 2 1 22497.00 22960.05 315.15 o 0 2 1 17.16 18.74 4.51 o 1 2 1 22046.11 22936.86 445.15 o 2 2 1 3724.96 3639.09 40.94 o 3 2 1 4766.05 4895.66 109.25 o 4 2 1 5346.44 5052.07 43.77 o 5 2 1 7096.34 6955.05 183.70 o 6 2 1 7356.21 7010.83 130.35 o 7 2 1 4504.69 4426.25 113.84 o 8 2 1 3942.00 3955.87 99.52 o 9 2 1 1373.53 1420.51 51.00 o 10 2 1 1470.44 1495.19 53.37 o 11 2 1 298.81 330.70 23.00 o 12 2 1 368.12 372.06 14.61 o -5 3 1 3579.46 3322.54 57.96 o -4 3 1 4045.67 3563.14 55.43 o -3 3 1 4690.08 4985.90 56.48 o -2 3 1 13082.26 13323.66 80.14 o -1 3 1 4593.70 4962.90 32.53 o 0 3 1 39958.56 46611.31 614.83 o 1 3 1 4317.80 4547.69 196.15 o 2 3 1 13280.58 12719.93 78.43 o 3 3 1 4541.65 4393.23 53.33 o 4 3 1 4019.97 3664.84 56.02 o 5 3 1 3684.02 3522.12 59.82 o 6 3 1 1765.68 1632.25 28.68 o 7 3 1 2641.58 2669.95 62.62 o 8 3 1 334.77 353.81 11.57 o 9 3 1 975.78 994.37 23.48 o 10 3 1 789.82 805.12 19.24 o 11 3 1 595.05 621.94 17.38 o 12 3 1 584.09 650.40 34.42 o -7 4 1 5747.20 5234.90 90.16 o -6 4 1 1837.69 1754.69 41.80 o -5 4 1 8092.82 7523.99 87.13 o -4 4 1 5661.49 5879.81 71.71 o -3 4 1 8726.22 9482.31 80.72 o -2 4 1 8443.75 8801.70 71.40 o -1 4 1 1793.39 1908.41 23.69 o 0 4 1 7664.80 7884.57 42.99 o 1 4 1 1880.33 1969.87 34.18 o 2 4 1 8733.54 8849.75 71.36 o 3 4 1 8580.35 8530.20 77.19 o 4 4 1 5824.89 5804.53 71.32 o 5 4 1 8065.37 7441.05 86.55 o 6 4 1 1887.21 1802.86 41.91 o 7 4 1 5877.28 5353.22 92.49 o 8 4 1 110.29 106.69 8.03 o 9 4 1 2037.09 2160.16 36.26 o 10 4 1 639.12 630.92 16.35 o 11 4 1 176.38 213.73 22.38 o 12 4 1 365.09 352.18 14.50 o -10 5 1 363.85 333.68 18.02 o -9 5 1 536.34 504.56 19.97 o -8 5 1 251.61 255.91 13.98 o -7 5 1 833.16 757.88 24.12 o -6 5 1 817.82 766.73 23.62 o -5 5 1 1659.18 1516.18 37.68 o -4 5 1 6144.07 6232.73 77.26 o -3 5 1 957.74 988.35 23.23 o -2 5 1 12208.15 12384.96 90.94 o -1 5 1 146.59 161.81 6.17 o 0 5 1 14391.47 15302.54 134.64 o 1 5 1 156.43 150.08 6.52 o 2 5 1 12203.08 11760.21 88.72 o 3 5 1 897.47 828.96 22.14 o 4 5 1 6329.53 5993.09 75.83 o 5 5 1 1629.30 1529.15 37.56 o 6 5 1 770.04 768.56 23.39 o 7 5 1 917.93 916.02 27.00 o 8 5 1 257.00 266.71 13.79 o 9 5 1 519.80 500.84 20.28 o 10 5 1 368.09 360.33 17.83 o 11 5 1 508.33 535.90 17.56 o 12 5 1 720.63 718.54 26.45 o -11 6 1 290.57 312.90 16.66 o -10 6 1 666.31 622.50 23.11 o -9 6 1 1879.04 1803.60 44.01 o -8 6 1 615.52 593.44 20.04 o -7 6 1 4946.89 4401.31 88.45 o -6 6 1 1216.05 1247.68 35.54 o -5 6 1 7890.65 7141.87 91.60 o -4 6 1 3095.61 2976.42 57.30 o -3 6 1 5299.34 5398.40 70.85 o -2 6 1 5007.14 5612.56 68.29 o -1 6 1 496.31 519.09 11.54 o 0 6 1 5662.43 6395.04 47.94 o 1 6 1 500.55 530.13 11.96 o 2 6 1 4949.67 5312.36 66.00 o 3 6 1 5107.94 5171.54 69.22 o 4 6 1 3245.14 3119.76 60.21 o 5 6 1 7568.60 6624.60 89.46 o 6 6 1 1245.71 1179.16 35.74 o 7 6 1 4849.54 4430.64 87.32 o 8 6 1 599.24 605.37 20.47 o 9 6 1 1941.98 1887.04 45.14 o 10 6 1 641.27 643.67 22.57 o 11 6 1 338.95 361.15 18.37 o -11 7 1 251.50 284.97 16.28 o -10 7 1 260.60 244.07 15.89 o -9 7 1 537.47 502.86 19.69 o -8 7 1 456.46 424.74 18.14 o -7 7 1 1068.79 971.99 26.88 o -6 7 1 1304.51 1264.11 32.40 o -5 7 1 2030.13 1905.88 45.41 o -4 7 1 3062.59 2942.78 61.73 o -3 7 1 5107.89 5184.83 73.50 o -2 7 1 4643.57 4600.28 66.74 o -1 7 1 6055.34 6531.80 74.86 o 0 7 1 6008.87 6509.97 52.27 o 1 7 1 6191.92 6698.49 54.26 o 2 7 1 4869.83 5160.16 70.08 o 3 7 1 4989.18 5183.12 73.53 o 4 7 1 3253.65 3051.82 63.01 o 5 7 1 1928.76 1920.76 45.06 o 6 7 1 1369.08 1260.93 33.29 o 7 7 1 1066.78 987.03 29.25 o 8 7 1 442.52 458.84 17.60 o 9 7 1 490.43 484.79 19.46 o 10 7 1 251.97 241.62 15.62 o 11 7 1 241.84 205.69 16.24 o -11 8 1 237.11 240.57 16.08 o -10 8 1 784.31 776.41 25.64 o -9 8 1 429.92 372.92 17.33 o -8 8 1 2155.98 2101.31 50.93 o -7 8 1 696.54 683.06 21.33 o -6 8 1 2725.65 2698.87 57.10 o -5 8 1 2569.39 2809.54 55.32 o -4 8 1 3440.45 3315.47 69.38 o -3 8 1 4825.91 4753.06 76.06 o -2 8 1 2156.60 2338.93 53.65 o -1 8 1 6667.70 7172.55 129.39 o 0 8 1 269.62 284.33 9.45 o 1 8 1 6688.94 7055.32 165.66 o 2 8 1 2202.07 2312.01 52.71 o 3 8 1 4764.44 4615.70 74.70 o 4 8 1 3497.13 3344.02 68.33 o 5 8 1 2561.28 2292.90 50.38 o 6 8 1 2729.48 2656.02 56.29 o 7 8 1 732.49 662.94 21.33 o 8 8 1 2188.83 1999.22 51.98 o 9 8 1 429.44 420.77 17.71 o 10 8 1 857.20 886.96 27.08 o 11 8 1 226.85 205.30 15.85 o -10 9 1 435.61 373.42 19.11 o -9 9 1 124.34 100.45 13.32 o -8 9 1 740.20 737.25 22.96 o -7 9 1 184.35 172.86 13.21 o -6 9 1 1258.69 1274.17 31.31 o -5 9 1 2020.07 2004.47 43.20 o -4 9 1 1600.78 1464.32 37.76 o -3 9 1 3811.03 3763.16 71.71 o -2 9 1 581.74 627.47 18.68 o -1 9 1 5423.35 5781.55 59.24 o 0 9 1 21.69 34.09 6.47 o 1 9 1 5406.50 5909.06 368.95 o 2 9 1 578.25 600.94 19.42 o 3 9 1 3598.84 3597.10 71.05 o 4 9 1 1717.38 1637.84 39.04 o 5 9 1 1928.21 1929.92 42.50 o 6 9 1 1269.75 1225.69 31.12 o 7 9 1 179.51 169.44 12.43 o 8 9 1 686.56 684.34 23.31 o 9 9 1 126.80 123.22 13.40 o 10 9 1 448.00 457.06 19.54 o -10 10 1 545.04 545.90 21.17 o -9 10 1 117.10 116.30 13.83 o -8 10 1 2286.31 2204.95 49.45 o -7 10 1 416.52 424.12 17.29 o -6 10 1 2758.45 2789.89 62.97 o -5 10 1 342.49 359.44 14.22 o -4 10 1 1971.07 1944.30 42.77 o -3 10 1 765.14 769.41 23.39 o -2 10 1 1039.46 1131.73 27.42 o -1 10 1 2436.17 2696.27 44.74 o 0 10 1 213.47 202.17 17.62 o 1 10 1 2456.96 2661.15 137.49 o 2 10 1 1003.90 1047.16 26.96 o 3 10 1 754.13 805.31 23.11 o 4 10 1 2050.22 1959.37 41.72 o 5 10 1 429.16 449.64 15.15 o 6 10 1 2814.38 2543.10 60.64 o 7 10 1 462.66 450.06 17.71 o 8 10 1 2245.13 2179.58 49.18 o 9 10 1 112.13 123.53 13.83 o 10 10 1 538.47 541.04 21.64 o -10 11 1 192.04 175.74 15.62 o -9 11 1 55.55 40.94 13.87 o -8 11 1 141.65 130.87 12.94 o -7 11 1 364.06 362.08 16.28 o -6 11 1 436.21 424.00 17.60 o -5 11 1 967.15 888.98 23.31 o -4 11 1 845.99 811.09 22.84 o -3 11 1 1741.52 1637.30 41.76 o -2 11 1 2420.11 2325.60 54.34 o -1 11 1 2289.01 2346.39 37.45 o 0 11 1 3084.54 3187.59 50.27 o 1 11 1 2249.77 2351.14 37.34 o 2 11 1 2319.61 2473.29 53.02 o 3 11 1 1705.55 1789.46 42.07 o 4 11 1 869.03 899.43 23.73 o 5 11 1 1066.09 1060.41 24.71 o 6 11 1 407.23 385.11 17.13 o 7 11 1 441.85 412.81 18.34 o 8 11 1 103.25 114.91 12.97 o 9 11 1 68.82 91.95 13.48 o 10 11 1 193.06 207.44 15.89 o -9 12 1 331.56 324.59 15.89 o -8 12 1 534.12 457.13 20.32 o -7 12 1 946.65 900.01 28.09 o -6 12 1 1331.75 1219.98 33.64 o -5 12 1 2012.08 1839.06 39.35 o -4 12 1 1285.23 1222.04 33.37 o -3 12 1 1114.98 1168.67 27.66 o -2 12 1 662.04 700.11 21.02 o -1 12 1 382.61 401.32 11.05 o 0 12 1 624.91 656.18 14.88 o 1 12 1 378.67 381.63 11.21 o 2 12 1 677.73 666.01 20.98 o 3 12 1 1088.59 1085.42 30.42 o 4 12 1 1298.54 1292.47 33.10 o 5 12 1 2059.96 2084.18 40.36 o 6 12 1 1314.40 1178.30 32.94 o 7 12 1 1022.84 935.24 28.63 o 8 12 1 504.89 457.13 19.42 o 9 12 1 366.47 360.84 16.98 o -8 13 1 10.83 9.56 13.60 o -7 13 1 696.69 708.39 22.96 o -6 13 1 98.79 76.53 12.82 o -5 13 1 818.71 735.93 21.33 o -4 13 1 1177.75 1112.22 28.51 o -3 13 1 648.98 615.66 20.16 o -2 13 1 2679.15 2616.83 52.29 o -1 13 1 332.37 335.21 12.45 o 0 13 1 1897.68 1903.92 32.55 o 1 13 1 331.27 323.28 11.11 o 2 13 1 2853.17 2913.38 64.68 o 3 13 1 615.08 582.06 19.35 o 4 13 1 1179.20 1138.06 28.67 o 5 13 1 866.79 766.34 21.64 o 6 13 1 66.56 77.81 12.24 o 7 13 1 787.02 786.35 24.82 o 8 13 1 14.60 36.75 13.17 o -7 14 1 1237.90 1208.37 33.56 o -6 14 1 45.57 29.95 12.66 o -5 14 1 1279.05 1149.21 27.31 o -4 14 1 204.56 218.51 12.94 o -3 14 1 1231.92 1184.75 32.24 o -2 14 1 932.06 955.76 25.64 o -1 14 1 474.39 496.35 13.56 o 0 14 1 2267.81 2319.17 36.79 o 1 14 1 439.67 483.08 12.70 o 2 14 1 1005.57 942.31 27.81 o 3 14 1 1212.69 1227.17 29.99 o 4 14 1 231.88 217.85 13.48 o 5 14 1 1250.47 1253.62 29.68 o 6 14 1 37.79 46.89 12.82 o 7 14 1 1223.58 1217.11 33.02 o -7 15 1 248.66 221.96 15.62 o -6 15 1 207.84 211.67 15.62 o -5 15 1 224.35 198.15 14.06 o -4 15 1 815.65 768.09 22.65 o -3 15 1 168.12 167.54 13.05 o -2 15 1 1411.05 1371.75 34.42 o -1 15 1 1196.46 1204.29 33.80 o 0 15 1 1007.99 986.51 20.23 o 1 15 1 1132.11 1121.43 22.16 o 2 15 1 1436.46 1389.27 34.53 o 3 15 1 137.45 143.65 13.01 o 4 15 1 863.63 835.10 24.86 o 5 15 1 207.69 208.95 13.79 o 6 15 1 197.78 185.29 14.96 o 7 15 1 237.33 213.07 15.54 o -5 16 1 686.46 617.37 19.81 o -4 16 1 501.53 474.38 18.72 o -3 16 1 816.47 798.78 26.03 o -2 16 1 290.48 317.56 14.76 o -1 16 1 280.66 295.80 11.22 o 0 16 1 213.99 187.13 21.62 o 1 16 1 229.78 258.06 15.25 o 2 16 1 294.10 287.07 15.50 o 3 16 1 788.16 760.71 25.21 o 4 16 1 501.78 482.66 18.34 o 5 16 1 676.05 648.25 19.77 o -4 17 1 284.50 252.15 14.99 o -3 17 1 223.53 220.99 15.27 o -2 17 1 369.61 370.39 17.01 o -1 17 1 861.32 923.46 47.72 o 0 17 1 375.67 389.63 12.61 o 1 17 1 835.63 841.19 39.62 o 2 17 1 390.79 437.87 17.71 o 3 17 1 213.27 228.64 15.19 o 4 17 1 317.94 327.43 16.20 o -1 18 1 471.02 484.20 14.03 o 0 18 1 57.33 46.59 14.49 o 1 18 1 454.55 485.01 13.68 o 0 0 2 7988.45 8466.19 33.52 o 1 0 2 2440.88 2627.12 20.78 o 2 0 2 3942.77 4101.97 42.61 o 3 0 2 3205.54 3411.41 43.97 o 4 0 2 2939.11 3032.28 49.33 o 5 0 2 7275.01 7543.26 81.23 o 6 0 2 1041.53 1037.56 29.56 o 7 0 2 8209.15 8538.87 107.80 o 8 0 2 4.20 -2.02 10.29 o 9 0 2 3103.36 3109.39 67.01 o 10 0 2 513.80 547.76 19.66 o 11 0 2 559.51 581.75 20.94 o 12 0 2 284.97 292.08 17.67 o -2 1 2 18842.91 19151.23 86.98 o -1 1 2 8819.65 9484.97 172.80 o 0 1 2 4709.85 4443.19 22.78 o 1 1 2 8953.72 9486.06 258.23 o 2 1 2 18556.45 18513.58 85.81 o 3 1 2 3027.77 3190.90 49.43 o 4 1 2 9954.44 10541.74 418.39 o 5 1 2 3820.39 3764.17 135.57 o 6 1 2 1537.68 1458.88 24.38 o 7 1 2 2645.56 2616.75 98.14 o 8 1 2 148.98 178.63 8.79 o 9 1 2 1226.51 1188.18 23.44 o 10 1 2 715.16 765.43 17.59 o 11 1 2 457.32 449.50 26.71 o 12 1 2 581.24 631.82 44.07 o -2 2 2 9846.39 10013.05 67.13 o -1 2 2 1800.65 1809.70 29.52 o 0 2 2 19010.67 19536.27 74.62 o 1 2 2 1908.95 1986.56 30.53 o 3 2 2 5972.61 5844.11 59.08 o 4 2 2 6964.60 7470.69 75.32 o 5 2 2 8754.88 8229.46 86.39 o 6 2 2 4390.91 4355.01 72.17 o 7 2 2 4544.44 4764.95 83.91 o 8 2 2 2547.00 2597.64 58.23 o 9 2 2 1217.17 1316.94 34.61 o 10 2 2 836.96 890.69 27.00 o 11 2 2 781.59 812.49 27.08 o 12 2 2 401.99 408.03 21.21 o -4 3 2 3069.45 3169.37 53.10 o -3 3 2 9644.04 9633.18 78.20 o -2 3 2 4471.32 4798.08 50.46 o -1 3 2 12411.77 12559.38 72.95 o 0 3 2 2406.26 2735.39 35.70 o 1 3 2 12528.49 12613.57 73.34 o 5 3 2 3649.46 3578.60 60.91 o 6 3 2 2665.78 2580.39 61.03 o 7 3 2 1071.81 1071.71 32.79 o 8 3 2 1555.88 1661.54 43.08 o 9 3 2 655.09 742.73 22.80 o 10 3 2 1274.88 1349.84 35.89 o 11 3 2 348.93 392.22 19.23 o 12 3 2 253.30 285.90 18.80 o -5 4 2 1998.65 1953.97 48.67 o -4 4 2 4801.36 4840.31 66.43 o -3 4 2 6318.16 6723.93 70.19 o -2 4 2 1640.18 1745.29 36.01 o -1 4 2 8926.70 9677.35 70.89 o 0 4 2 213.35 196.25 9.44 o 1 4 2 9226.49 10018.57 72.56 o 6 4 2 5700.39 5548.27 85.30 o 7 4 2 1239.49 1237.35 33.91 o 8 4 2 4474.32 4398.59 92.14 o 9 4 2 221.28 224.95 14.96 o 10 4 2 1009.17 988.39 30.77 o 11 4 2 26.18 45.29 14.22 o 12 4 2 62.71 56.09 16.32 o -7 5 2 161.73 159.93 12.00 o -6 5 2 1084.53 1059.36 29.60 o -5 5 2 2683.87 2686.94 57.57 o -4 5 2 996.32 936.33 25.48 o -3 5 2 7307.88 7186.15 76.80 o -2 5 2 582.55 558.68 16.74 o -1 5 2 15729.16 16373.12 100.96 o 0 5 2 80.17 112.89 7.69 o 1 5 2 15920.03 16611.86 101.70 o 8 5 2 870.99 918.27 27.31 o 9 5 2 81.13 103.02 12.20 o 10 5 2 700.34 750.30 25.13 o 11 5 2 312.74 344.13 19.50 o 12 5 2 243.39 247.37 18.34 o -10 6 2 882.42 815.21 26.34 o -9 6 2 637.89 577.63 21.05 o -8 6 2 2972.39 2834.25 64.44 o -7 6 2 1206.61 1163.62 29.56 o -6 6 2 4501.81 4079.67 79.28 o -5 6 2 3347.08 3354.74 66.43 o -4 6 2 6448.39 6477.22 82.24 o -3 6 2 4303.94 4490.43 65.45 o -2 6 2 3543.00 3743.93 56.68 o -1 6 2 7137.49 7886.96 77.77 o 0 6 2 641.00 644.33 19.77 o 1 6 2 7255.72 7968.69 77.77 o 11 6 2 323.19 333.10 18.61 o -11 7 2 172.20 115.53 15.69 o -10 7 2 673.84 679.25 24.08 o -9 7 2 193.72 194.62 13.21 o -8 7 2 790.35 759.82 23.39 o -7 7 2 708.57 698.21 21.37 o -6 7 2 1873.47 1928.49 42.23 o -5 7 2 2183.60 2177.41 47.35 o -4 7 2 3243.42 3183.93 65.11 o -3 7 2 2751.61 2821.93 56.87 o -2 7 2 5503.32 5880.47 75.44 o -1 7 2 2664.47 2785.15 52.60 o 0 7 2 9242.70 10132.58 92.61 o 1 7 2 2713.26 2761.99 51.98 o -11 8 2 330.68 308.24 17.60 o -10 8 2 347.65 322.81 17.48 o -9 8 2 1342.08 1270.52 35.19 o -8 8 2 268.84 263.41 14.06 o -7 8 2 2452.73 2347.12 59.24 o -6 8 2 1669.04 1590.41 41.14 o -5 8 2 3286.86 3228.68 72.06 o -4 8 2 3973.67 3927.24 73.85 o -3 8 2 2063.27 2174.57 44.94 o -2 8 2 4981.10 5336.48 76.64 o -1 8 2 878.95 869.87 25.83 o 0 8 2 5497.03 5821.00 78.08 o 1 8 2 905.21 925.30 27.23 o -10 9 2 144.62 136.66 14.53 o -9 9 2 645.25 627.98 22.30 o -8 9 2 40.46 47.31 11.61 o -7 9 2 1234.45 1221.23 33.33 o -6 9 2 363.82 352.13 16.63 o -5 9 2 2158.32 1965.93 43.47 o -4 9 2 2841.68 2881.09 68.14 o -3 9 2 1279.20 1226.04 30.53 o -2 9 2 4960.63 4887.35 80.14 o -1 9 2 321.79 335.51 14.22 o 0 9 2 5525.73 5736.36 83.32 o 1 9 2 303.92 317.13 14.33 o -10 10 2 166.41 146.68 15.11 o -9 10 2 1414.97 1296.28 35.39 o -8 10 2 197.95 211.13 13.40 o -7 10 2 2903.27 2780.72 67.75 o -6 10 2 714.59 728.82 24.74 o -5 10 2 2755.77 2631.51 57.18 o -4 10 2 695.80 697.20 21.25 o -3 10 2 2970.76 2880.36 68.21 o -2 10 2 1803.23 1861.87 47.78 o -1 10 2 793.19 800.37 24.82 o 0 10 2 2384.65 2422.56 62.39 o 1 10 2 830.42 891.58 25.68 o -9 11 2 539.62 516.10 21.17 o -8 11 2 241.96 205.61 15.07 o -7 11 2 796.14 744.98 24.24 o -6 11 2 851.62 829.51 24.71 o -5 11 2 903.40 857.55 21.40 o -4 11 2 1273.31 1266.67 31.15 o -3 11 2 1727.17 1692.42 41.60 o -2 11 2 1943.62 2006.22 42.81 o -1 11 2 2888.08 2926.27 70.97 o 0 11 2 2805.08 2827.88 68.56 o 1 11 2 2936.68 3099.64 71.59 o -9 12 2 390.52 354.50 18.18 o -8 12 2 886.06 917.14 26.26 o -7 12 2 1071.10 1007.11 29.21 o -6 12 2 1711.81 1740.24 39.74 o -5 12 2 1099.48 1022.45 27.27 o -4 12 2 1256.46 1211.28 32.47 o -3 12 2 566.73 547.06 19.23 o -2 12 2 1083.49 1036.17 29.76 o -1 12 2 676.37 667.29 20.98 o 0 12 2 583.36 598.73 19.73 o 1 12 2 648.34 693.08 22.30 o -8 13 2 504.70 511.13 18.96 o -7 13 2 145.95 146.53 13.83 o -6 13 2 697.81 698.17 24.16 o -5 13 2 276.42 258.87 12.94 o -4 13 2 654.62 594.26 20.28 o -3 13 2 1779.73 1673.62 41.14 o -2 13 2 348.44 334.38 14.64 o -1 13 2 2184.82 2176.83 50.23 o 0 13 2 129.47 146.53 11.58 o 1 13 2 2121.81 2133.05 48.05 o -7 14 2 19.25 11.07 13.75 o -6 14 2 1180.89 1178.53 33.64 o -5 14 2 92.25 86.31 12.08 o -4 14 2 1160.38 1029.37 29.52 o -3 14 2 380.81 371.01 15.81 o -2 14 2 640.43 609.72 20.12 o -1 14 2 1284.88 1329.72 35.19 o 0 14 2 127.32 139.03 11.54 o 1 14 2 1247.62 1415.88 35.70 o -6 15 2 281.35 243.13 15.81 o -5 15 2 354.24 334.15 15.93 o -4 15 2 258.31 235.44 14.99 o -3 15 2 1180.20 1160.82 31.62 o -2 15 2 359.95 409.78 16.00 o -1 15 2 811.74 802.98 24.78 o 0 15 2 936.66 945.69 26.34 o 1 15 2 841.36 902.07 26.49 o -5 16 2 532.14 477.68 18.41 o -4 16 2 502.42 478.38 19.11 o -3 16 2 538.80 530.51 20.39 o -2 16 2 420.52 419.26 18.45 o -1 16 2 239.09 246.94 14.14 o 0 16 2 47.64 61.49 12.51 o 1 16 2 237.18 245.43 15.42 o -4 17 2 228.99 234.12 15.27 o -3 17 2 170.62 163.66 14.99 o -2 17 2 596.34 582.92 19.97 o -1 17 2 279.43 272.50 16.70 o 0 17 2 1497.19 1572.00 40.75 o 1 17 2 285.27 313.37 16.32 o 0 18 2 467.39 491.75 20.70 o 1 0 3 83453.14 77464.10 641.79 o 2 0 3 2.16 6.56 7.46 o 3 0 3 27582.60 28000.16 125.39 o 4 0 3 48.29 55.47 8.35 o 5 0 3 7695.27 7380.22 82.62 o 6 0 3 3.19 4.70 7.89 o 7 0 3 538.79 571.22 21.25 o 8 0 3 221.29 226.31 14.57 o 9 0 3 153.47 168.51 13.75 o 10 0 3 34.62 46.77 12.31 o 11 0 3 674.33 735.38 26.10 o 12 0 3 0.05 -12.74 14.53 o -2 1 3 4069.60 4226.00 45.99 o -1 1 3 594.80 630.90 16.48 o 0 1 3 2512.41 2391.03 33.56 o 1 1 3 596.99 673.41 18.92 o 2 1 3 3874.31 3714.76 43.93 o 3 1 3 2945.15 2895.49 30.90 o 4 1 3 8447.66 8734.23 169.93 o 5 1 3 2502.11 2401.69 82.62 o 6 1 3 6987.22 6844.67 220.58 o 7 1 3 911.07 976.43 21.64 o 8 1 3 5733.40 5794.86 70.55 o 9 1 3 467.84 452.43 13.49 o 10 1 3 2263.56 2252.07 40.06 o 11 1 3 231.69 241.90 11.32 o 12 1 3 605.42 572.17 16.97 o -3 2 3 3885.75 3976.31 51.78 o -2 2 3 12139.14 12002.61 77.34 o -1 2 3 10962.56 11127.77 68.37 o 0 2 3 9189.11 9244.92 59.71 o 1 2 3 11314.78 11803.91 69.96 o 4 2 3 3948.17 4043.39 58.27 o 5 2 3 1686.36 1656.30 35.50 o 6 2 3 428.66 458.03 17.40 o 7 2 3 22.80 15.77 11.30 o 8 2 3 221.11 195.55 14.06 o 9 2 3 273.05 295.81 15.03 o 10 2 3 77.14 84.02 12.66 o 11 2 3 451.04 452.98 21.40 o 12 2 3 359.17 378.32 19.54 o -4 3 3 3555.85 3573.17 56.87 o -3 3 3 3724.80 3700.00 52.99 o -2 3 3 2705.07 2733.21 41.29 o -1 3 3 616.69 602.57 18.41 o 0 3 3 581.73 565.75 18.30 o 1 3 3 613.53 566.45 19.00 o 5 3 3 5477.86 5604.32 75.55 o 6 3 3 1389.93 1447.07 39.70 o 7 3 3 4744.02 4870.41 88.02 o 8 3 3 1638.66 1659.64 38.50 o 9 3 3 2475.73 2565.47 55.01 o 10 3 3 838.67 889.25 27.81 o 11 3 3 986.26 1114.09 32.05 o 12 3 3 216.22 187.59 17.64 o -5 4 3 239.91 223.09 12.04 o -4 4 3 6023.81 6114.48 75.67 o -3 4 3 1047.41 1095.02 27.39 o -2 4 3 29330.79 32129.95 142.25 o -1 4 3 976.44 1023.62 22.92 o 0 4 3 53903.66 54330.28 169.09 o 1 4 3 835.82 885.37 22.30 o 6 4 3 675.24 659.25 22.80 o 7 4 3 359.60 357.73 17.52 o 8 4 3 32.11 51.74 10.72 o 9 4 3 3.64 4.35 11.50 o 10 4 3 368.76 350.78 18.80 o 11 4 3 36.27 21.60 14.76 o 12 4 3 527.60 560.04 25.21 o -6 5 3 284.82 304.74 14.45 o -5 5 3 10856.66 10623.55 109.62 o -4 5 3 128.43 160.00 10.33 o -3 5 3 5968.03 5798.00 71.24 o -2 5 3 1842.66 1946.39 41.18 o -1 5 3 1080.86 1120.38 26.30 o 0 5 3 930.42 1036.32 24.74 o 1 5 3 1091.83 1125.78 26.41 o 7 5 3 6940.63 7199.40 108.50 o 8 5 3 102.22 98.20 11.42 o 9 5 3 3086.83 3088.30 70.62 o 10 5 3 371.42 340.36 18.45 o 11 5 3 1664.44 1792.14 47.86 o -8 6 3 96.49 113.23 11.61 o -7 6 3 25.60 36.13 9.63 o -6 6 3 248.60 257.24 13.87 o -5 6 3 445.48 503.94 16.47 o -4 6 3 2369.32 2361.15 54.77 o -3 6 3 2087.32 2177.64 49.37 o -2 6 3 10300.79 11067.01 96.92 o -1 6 3 1968.79 1980.46 43.20 o 0 6 3 13913.42 14705.28 105.15 o 1 6 3 1748.57 1788.45 41.49 o 9 6 3 318.36 371.48 17.67 o 10 6 3 609.54 690.91 23.19 o 11 6 3 254.26 261.90 17.99 o -10 7 3 860.49 833.24 27.27 o -9 7 3 1034.80 964.15 27.66 o -8 7 3 2221.30 2298.88 52.87 o -7 7 3 1935.11 1865.75 44.44 o -6 7 3 3188.45 3241.39 74.23 o -5 7 3 1647.07 1655.29 37.99 o -4 7 3 2382.48 2348.91 55.98 o -3 7 3 2366.58 2489.45 55.43 o -2 7 3 1717.39 1874.45 38.15 o -1 7 3 1546.99 1561.63 34.38 o 0 7 3 205.26 237.54 10.84 o 1 7 3 1555.58 1553.59 34.96 o 11 7 3 393.14 410.52 19.81 o -11 8 3 357.70 376.49 18.92 o -10 8 3 59.64 51.66 13.79 o -9 8 3 170.79 172.12 13.09 o -8 8 3 1.11 1.90 10.80 o -7 8 3 95.61 102.44 11.19 o -6 8 3 63.63 62.27 9.71 o -5 8 3 1486.97 1486.00 34.30 o -4 8 3 430.41 414.02 17.09 o -3 8 3 6375.59 6564.23 89.50 o -2 8 3 2201.25 2355.75 56.40 o -1 8 3 12197.36 12612.33 115.72 o 0 8 3 2744.42 2798.63 57.06 o 1 8 3 12310.03 12953.23 116.34 o -10 9 3 1327.17 1312.55 36.44 o -9 9 3 17.42 14.41 12.62 o -8 9 3 2353.06 2367.05 54.97 o -7 9 3 23.04 43.78 10.64 o -6 9 3 4419.75 4118.75 88.61 o -5 9 3 41.65 69.34 9.21 o -4 9 3 3936.86 3781.81 76.60 o -3 9 3 11.55 15.38 9.05 o -2 9 3 1137.12 1180.17 32.20 o -1 9 3 207.18 215.51 12.66 o 0 9 3 3.61 13.87 8.51 o 1 9 3 220.42 251.45 12.86 o -10 10 3 57.92 68.91 13.98 o -9 10 3 141.80 121.20 14.41 o -8 10 3 139.92 161.09 12.47 o -7 10 3 153.63 160.12 12.51 o -6 10 3 2.50 1.90 10.29 o -5 10 3 1353.56 1294.57 29.06 o -4 10 3 166.55 167.00 11.30 o -3 10 3 5059.20 5266.83 91.21 o -2 10 3 71.96 98.05 10.14 o -1 10 3 8588.44 9102.67 112.22 o 0 10 3 97.00 93.77 10.72 o 1 10 3 8412.88 8948.80 111.49 o -9 11 3 755.73 747.43 26.96 o -8 11 3 1016.76 965.54 29.29 o -7 11 3 1271.27 1277.94 34.07 o -6 11 3 1903.89 1795.01 43.31 o -5 11 3 817.24 769.80 20.04 o -4 11 3 2206.49 2112.46 46.50 o -3 11 3 527.42 555.61 18.06 o -2 11 3 381.81 369.96 15.77 o -1 11 3 154.83 196.36 11.73 o 0 11 3 1.79 19.11 9.09 o 1 11 3 175.88 177.21 11.96 o -9 12 3 10.45 40.55 13.48 o -8 12 3 52.24 7.92 13.60 o -7 12 3 0.30 -5.09 11.93 o -6 12 3 268.54 318.65 14.49 o -5 12 3 147.46 126.91 11.23 o -4 12 3 2027.29 1900.98 47.31 o -3 12 3 1003.24 933.77 27.42 o -2 12 3 4236.28 4160.63 88.49 o -1 12 3 1759.58 1745.56 44.21 o 0 12 3 6315.34 6511.29 107.10 o 1 12 3 1800.07 1885.99 43.90 o -8 13 3 181.88 179.00 14.92 o -7 13 3 1585.95 1503.36 39.31 o -6 13 3 10.14 12.47 11.85 o -5 13 3 1628.32 1426.52 32.32 o -4 13 3 2.24 13.09 10.06 o -3 13 3 1106.96 1165.91 30.42 o -2 13 3 24.85 26.57 10.22 o -1 13 3 104.94 115.37 11.27 o 0 13 3 20.16 7.07 10.41 o 1 13 3 84.88 105.31 10.92 o -7 14 3 3.49 23.89 12.82 o -6 14 3 364.78 292.04 16.98 o -5 14 3 19.35 9.52 11.50 o -4 14 3 1147.68 1170.45 31.19 o -3 14 3 49.45 53.53 11.38 o -2 14 3 2351.83 2224.45 53.22 o -1 14 3 45.74 61.96 11.19 o 0 14 3 4541.04 4739.74 101.39 o 1 14 3 44.22 57.03 10.80 o -6 15 3 187.10 166.57 14.76 o -5 15 3 1190.28 1080.64 26.10 o -4 15 3 172.16 164.63 13.91 o -3 15 3 846.35 826.24 23.70 o -2 15 3 124.96 152.00 11.96 o -1 15 3 78.79 103.64 12.12 o 0 15 3 56.82 57.34 11.65 o 1 15 3 86.85 86.16 12.08 o -5 16 3 185.19 176.24 14.37 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