Crystallography Open Database

Information card for entry 1542883

Preview

Structure parameters

Chemical name	Bis[2,6-bis(trimethylsilylamino)pyridine-κ<i>N</i>^1^]{[6-bis(trimethylsilylamino)pyridin-2-yl-κ<i>N</i>^1^](trimethylsilyl)azanido-κ<i>N</i>}lithium
Formula	C33 H68 Li N9 Si6
Calculated formula	C33 H68 Li N9 Si6
SMILES	[Si](N1c2[n](c(N[Si](C)(C)C)ccc2)[Li]1([n]1c(N[Si](C)(C)C)cccc1N[Si](C)(C)C)[n]1c(N[Si](C)(C)C)cccc1N[Si](C)(C)C)(C)(C)C
Title of publication	Bis[2,6-bis(trimethylsilylamino)pyridine-κ<i>N</i>^1^]{[6-bis(trimethylsilylamino)pyridin-2-yl-κ<i>N</i>^1^](trimethylsilyl)azanido-κ<i>N</i>}lithium
Authors of publication	Rave, Justin A.; Garcia, Diego A.; Hillesheim, Patrick C.; Guillet, Gary L.
Journal of publication	IUCrData
Year of publication	2016
Journal volume	1
Journal issue	3
Pages of publication	x160338
a	23.077 ± 0.011 Å
b	18.798 ± 0.009 Å
c	11.169 ± 0.006 Å
α	90°
β	98.744 ± 0.007°
γ	90°
Cell volume	4789 ± 4 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1312
Residual factor for significantly intense reflections	0.0681
Weighted residual factors for significantly intense reflections	0.1345
Weighted residual factors for all reflections included in the refinement	0.1745
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

Version history

Revision	Date	Message	Files
181861 (current)	2016-04-06	hkl/ (antanas@echidna.ibt.lt) Adding IUCr specific svn headers to multiple entries in range 1.	1542883.cif 1542883.hkl
178210	2016-03-15	cif/ hkl/ Adding structures of 1542883 via cif-deposit CGI script.	1542883.cif 1542883.hkl