Crystallography Open Database

Information card for entry 1543034

Preview

Coordinates	1543034.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H49 N O2 Si
Calculated formula	C24 H49 N O2 Si
Title of publication	Enantioselective Total Synthesis of Fluvirucinin B1.
Authors of publication	Guignard, Guillaume; Llor, Núria; Molins, Elies; Bosch, Joan; Amat, Mercedes
Journal of publication	Organic letters
Year of publication	2016
Journal volume	18
Journal issue	8
Pages of publication	1788 - 1791
a	9.6625 ± 0.0002 Å
b	21.1407 ± 0.0006 Å
c	13.3829 ± 0.0003 Å
α	90°
β	95.786 ± 0.002°
γ	90°
Cell volume	2719.82 ± 0.11 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0878
Residual factor for significantly intense reflections	0.0666
Weighted residual factors for significantly intense reflections	0.1759
Weighted residual factors for all reflections included in the refinement	0.1855
Goodness-of-fit parameter for all reflections included in the refinement	1.153
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
182526 (current)	2016-05-04	cif/ Updating files of 1543034 Original log message: Adding full bibliography for 1543034.cif.	1543034.cif
181815	2016-04-06	cif/ Adding structures of 1543034 via cif-deposit CGI script.	1543034.cif