#------------------------------------------------------------------------------ #$Date: 2016-04-16 04:56:33 +0300 (Sat, 16 Apr 2016) $ #$Revision: 182160 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/31/1543127.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1543127 _cell_angle_alpha 90.000 _cell_angle_beta 92.618 _cell_angle_gamma 90.000 _cell_length_a 10.5765 _cell_length_b 11.8088 _cell_length_c 39.1512 _exptl_crystal_F_000 2136.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file hb4037Isup2.hkl _cod_data_source_block I _shelx_title ' s92 in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 387.53 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9613.88 9076.69 353.52 o 3 0 0 21438.83 22724.34 667.73 o 4 0 0 28615.07 27996.66 681.91 o 5 0 0 7566.98 8727.28 293.78 o 6 0 0 20874.70 21298.80 519.06 o 7 0 0 2330.93 2678.06 175.11 o 8 0 0 3670.57 4321.49 235.75 o 9 0 0 713.79 785.18 63.01 o 10 0 0 4905.94 5182.23 391.82 o 11 0 0 523.44 553.67 109.21 o 12 0 0 269.16 406.58 74.18 o 13 0 0 191.14 217.54 103.59 o 2 1 0 1206.28 982.60 94.82 o 3 1 0 16813.80 17000.44 645.21 o 4 1 0 3364.14 3439.47 170.53 o 5 1 0 10586.75 11023.08 934.06 o 6 1 0 38.58 66.16 15.90 o 7 1 0 4117.83 4223.59 90.61 o 8 1 0 12.86 29.76 18.83 o 9 1 0 3756.63 4165.92 229.30 o 10 1 0 630.87 729.03 168.80 o 11 1 0 1083.96 1163.76 75.22 o 12 1 0 230.51 213.01 65.25 o 13 1 0 18.81 -0.43 62.60 o 0 2 0 14851.68 11688.06 409.81 o 1 2 0 3175.44 3041.40 217.03 o 3 2 0 15753.13 14017.00 970.25 o 4 2 0 25345.25 9065.12 6212.43 o 5 2 0 793.59 889.93 36.59 o 6 2 0 395.98 299.43 40.60 o 7 2 0 227.29 182.33 52.97 o 8 2 0 949.98 1048.06 48.58 o 9 2 0 1075.39 1058.83 101.47 o 10 2 0 164.28 138.97 39.45 o 11 2 0 95.18 169.56 57.80 o 12 2 0 536.53 604.37 81.53 o 13 2 0 488.21 347.09 101.36 o 1 3 0 51109.57 43936.57 1761.83 o 2 3 0 23.46 56.79 7.64 o 3 3 0 77266.80 71431.96 4286.19 o 4 3 0 16258.15 17015.65 969.83 o 5 3 0 171.40 147.51 13.23 o 6 3 0 1384.74 1146.94 85.27 o 7 3 0 888.00 1107.65 46.15 o 8 3 0 347.22 407.43 139.14 o 9 3 0 21.52 20.00 24.16 o 10 3 0 30.34 195.96 92.15 o 11 3 0 67.35 181.67 107.64 o 12 3 0 262.22 312.85 115.78 o 13 3 0 124.87 -154.40 232.08 o 0 4 0 2760.19 2344.39 104.22 o 1 4 0 6489.16 5736.09 155.16 o 2 4 0 14442.97 12662.69 560.90 o 3 4 0 11696.34 12390.99 815.49 o 4 4 0 1.55 0.63 14.09 o 5 4 0 1337.49 1310.79 131.36 o 6 4 0 277.97 242.03 29.26 o 7 4 0 150.95 192.85 31.14 o 8 4 0 706.55 631.09 102.78 o 9 4 0 4.21 8.70 41.74 o 10 4 0 782.32 664.70 76.50 o 11 4 0 1879.83 2031.45 269.88 o 12 4 0 68.92 119.64 85.32 o 1 5 0 5256.43 5058.51 264.55 o 2 5 0 15873.55 16956.11 1170.28 o 3 5 0 7110.72 6622.66 336.30 o 4 5 0 7408.03 6566.28 425.64 o 5 5 0 35.83 6.97 16.37 o 6 5 0 4493.77 4535.46 334.46 o 7 5 0 841.07 808.97 158.57 o 8 5 0 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3447.16 198.44 o 3 2 1 6449.10 6495.71 406.35 o 4 2 1 387.31 360.13 23.78 o 5 2 1 90.59 74.20 9.81 o 6 2 1 681.88 691.90 37.02 o 7 2 1 37.31 70.93 17.76 o 8 2 1 423.18 470.88 53.06 o 9 2 1 180.38 104.24 48.97 o 10 2 1 0.24 57.15 37.17 o 11 2 1 291.23 281.50 48.34 o 12 2 1 0.14 73.53 57.45 o 13 2 1 0.26 -53.57 53.57 o -13 3 1 44.81 -105.60 105.60 o -12 3 1 0.08 8.40 80.22 o -11 3 1 75.15 26.25 91.89 o -10 3 1 1054.12 1015.48 84.80 o -9 3 1 86.38 95.55 28.56 o -8 3 1 1103.56 1089.13 58.80 o -7 3 1 633.56 694.61 44.25 o -6 3 1 2789.51 2694.68 203.93 o -5 3 1 817.80 828.18 84.54 o -4 3 1 2170.46 2023.80 127.32 o -3 3 1 1855.62 1713.41 96.90 o -2 3 1 25515.97 21764.41 1275.19 o -1 3 1 1609.16 1453.22 42.93 o 0 3 1 25.73 26.25 11.32 o 1 3 1 1611.34 1324.63 68.42 o 2 3 1 9589.42 10511.19 706.80 o 3 3 1 230.19 226.22 30.82 o 4 3 1 491.72 407.02 14.68 o 5 3 1 291.38 254.25 23.41 o 6 3 1 11.56 18.46 14.40 o 7 3 1 265.00 257.46 24.06 o 8 3 1 61.84 97.42 26.68 o 9 3 1 38.06 16.66 24.93 o 10 3 1 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