#------------------------------------------------------------------------------ #$Date: 2016-05-21 04:38:42 +0300 (Sat, 21 May 2016) $ #$Revision: 183061 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/33/1543345.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1543345 _cell_angle_alpha 90.000 _cell_angle_beta 105.746 _cell_angle_gamma 90.000 _cell_length_a 6.3283 _cell_length_b 19.6204 _cell_length_c 10.1245 _exptl_crystal_F_000 512.00 _reflns_d_resolution_high 0.8087 _cod_data_source_file hb4045Isup2.hkl _cod_data_source_block I _shelx_title ' JTM600_0m_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 172.41 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 20.73 21.76 0.76 o 2 0 0 1074.81 1140.45 40.13 o 3 0 0 2.65 5.72 1.31 o 4 0 0 133.74 130.82 4.08 o 5 0 0 22.29 26.14 3.25 o 6 0 0 227.24 228.63 5.99 o 7 0 0 119.77 106.35 3.77 o 1 1 0 178.58 192.47 2.46 o 2 1 0 1160.19 1091.27 17.36 o 3 1 0 1274.58 1300.59 22.82 o 4 1 0 526.18 521.13 8.14 o 5 1 0 941.20 983.90 14.65 o 6 1 0 6.65 5.48 1.03 o 7 1 0 1.30 4.07 0.98 o 0 2 0 6969.29 6867.56 117.68 o 1 2 0 505.57 462.92 5.73 o 2 2 0 61.12 74.48 1.49 o 3 2 0 446.86 489.90 9.01 o 4 2 0 67.87 60.64 1.98 o 5 2 0 682.88 705.37 10.90 o 6 2 0 1.73 3.88 1.02 o 7 2 0 163.54 149.83 3.09 o 1 3 0 1922.76 1809.38 41.87 o 2 3 0 2609.45 2363.67 47.29 o 3 3 0 2041.51 2093.64 43.55 o 4 3 0 50.13 55.52 1.90 o 5 3 0 52.82 61.92 3.35 o 6 3 0 119.32 121.56 2.98 o 7 3 0 11.09 12.18 1.20 o 0 4 0 2797.15 2678.41 77.39 o 1 4 0 14252.84 14525.52 223.16 o 2 4 0 0.03 0.42 0.43 o 3 4 0 2113.42 2032.75 35.43 o 4 4 0 3.67 2.57 0.96 o 5 4 0 7.30 7.76 1.62 o 6 4 0 127.96 120.73 3.02 o 7 4 0 123.02 115.50 2.53 o 1 5 0 3002.98 2800.42 67.74 o 2 5 0 1130.16 1019.43 20.65 o 3 5 0 213.72 207.86 4.84 o 4 5 0 22.66 22.87 1.97 o 5 5 0 85.42 80.30 2.44 o 6 5 0 164.93 197.11 3.74 o 7 5 0 20.79 21.29 2.18 o 0 6 0 50.82 60.57 2.43 o 1 6 0 3926.41 3760.90 87.06 o 2 6 0 0.02 1.10 0.51 o 3 6 0 0.18 0.07 0.71 o 4 6 0 168.73 159.45 3.00 o 5 6 0 1.61 2.07 1.13 o 6 6 0 191.76 201.49 3.77 o 7 6 0 0.00 0.03 1.15 o 1 7 0 185.75 188.94 3.08 o 2 7 0 1633.77 1647.94 33.14 o 3 7 0 534.65 505.81 13.66 o 4 7 0 3.37 3.75 1.38 o 5 7 0 2.97 3.41 0.99 o 6 7 0 95.94 113.56 2.66 o 7 7 0 366.44 374.52 6.94 o 0 8 0 55.76 63.01 1.52 o 1 8 0 1533.05 1461.50 31.02 o 2 8 0 658.48 711.58 14.76 o 3 8 0 127.42 126.89 3.84 o 4 8 0 10.39 8.35 1.18 o 5 8 0 203.80 180.76 3.48 o 6 8 0 45.48 50.41 1.83 o 7 8 0 27.39 22.73 2.50 o 1 9 0 402.88 397.34 10.33 o 2 9 0 648.23 641.34 13.40 o 3 9 0 586.28 573.76 7.71 o 4 9 0 122.83 113.91 2.89 o 5 9 0 119.47 105.70 2.73 o 6 9 0 18.01 21.04 1.50 o 0 10 0 4.80 4.74 1.75 o 1 10 0 613.91 637.01 16.20 o 2 10 0 273.54 290.65 8.30 o 3 10 0 61.12 57.56 1.89 o 4 10 0 37.98 33.20 2.10 o 5 10 0 2.35 0.99 0.97 o 6 10 0 14.68 11.54 1.23 o 1 11 0 849.70 875.65 31.60 o 2 11 0 34.73 33.68 3.64 o 3 11 0 19.21 15.56 1.37 o 4 11 0 281.73 285.57 4.72 o 5 11 0 24.97 20.80 1.70 o 6 11 0 21.73 23.07 1.49 o 0 12 0 67.13 66.39 4.24 o 1 12 0 11.40 12.48 2.99 o 2 12 0 75.04 72.14 2.09 o 3 12 0 26.20 26.10 1.84 o 4 12 0 6.64 2.83 1.75 o 5 12 0 38.27 35.29 2.09 o 6 12 0 0.11 1.57 0.71 o 1 13 0 87.00 88.97 2.35 o 2 13 0 13.31 14.87 1.16 o 3 13 0 52.71 53.99 1.97 o 4 13 0 197.89 206.25 3.72 o 5 13 0 1.25 1.37 0.80 o 6 13 0 25.96 27.74 1.34 o 0 14 0 301.76 283.16 9.16 o 1 14 0 5.90 5.86 0.97 o 2 14 0 11.10 15.26 1.35 o 3 14 0 38.15 41.60 1.85 o 4 14 0 117.05 119.27 2.64 o 5 14 0 10.75 16.58 1.42 o 6 14 0 14.96 13.71 1.15 o 1 15 0 40.86 38.14 1.95 o 2 15 0 306.41 318.20 5.06 o 3 15 0 23.37 29.30 1.92 o 4 15 0 46.59 47.08 1.82 o 5 15 0 56.20 61.87 1.85 o 0 16 0 69.33 66.07 3.71 o 1 16 0 78.48 77.53 2.13 o 2 16 0 0.42 1.05 0.90 o 3 16 0 360.72 374.58 5.38 o 4 16 0 2.64 0.40 0.79 o 5 16 0 211.97 211.98 3.86 o 1 17 0 47.63 55.21 2.06 o 2 17 0 12.94 12.29 1.95 o 3 17 0 11.72 14.51 1.25 o 4 17 0 1.33 1.50 0.87 o 5 17 0 0.59 0.00 0.61 o 0 18 0 3.91 8.00 3.10 o 1 18 0 101.74 99.01 2.44 o 2 18 0 128.54 134.25 2.73 o 3 18 0 56.37 53.32 1.72 o 4 18 0 3.25 2.89 0.68 o 5 18 0 1.69 0.37 0.58 o 1 19 0 194.80 219.06 3.55 o 2 19 0 80.80 87.71 2.14 o 3 19 0 36.64 32.75 1.36 o 4 19 0 24.11 24.44 1.33 o 0 20 0 207.33 208.13 5.43 o 1 20 0 17.96 22.71 2.05 o 2 20 0 71.42 75.25 1.85 o 3 20 0 29.91 28.63 1.32 o 4 20 0 13.82 16.83 1.38 o 1 21 0 1.11 2.17 0.73 o 2 21 0 235.91 225.28 3.84 o 3 21 0 3.28 4.28 0.97 o 0 22 0 112.02 115.40 3.84 o 1 22 0 54.69 53.32 1.51 o 2 22 0 203.45 191.48 3.23 o 3 22 0 3.53 3.64 0.66 o 1 23 0 95.39 90.11 1.88 o 2 23 0 41.08 43.71 1.38 o 0 24 0 147.42 140.06 6.73 o 1 24 0 11.87 13.27 1.15 o -7 1 1 17.82 16.90 1.83 o -6 1 1 3.14 3.42 1.00 o -5 1 1 0.52 0.75 1.25 o -4 1 1 1011.41 997.02 18.04 o -3 1 1 66.16 68.83 1.83 o -2 1 1 11.15 13.06 0.56 o -1 1 1 780.45 738.31 11.09 o 0 1 1 46.10 40.19 1.13 o 1 1 1 92.32 88.24 1.49 o 2 1 1 133.37 129.81 2.89 o 3 1 1 58.97 58.37 1.66 o 4 1 1 1.60 1.71 0.85 o 5 1 1 20.68 22.37 1.76 o 6 1 1 161.34 164.35 3.61 o 7 1 1 0.47 -0.08 0.69 o -7 2 1 2.66 1.57 0.82 o -6 2 1 100.79 105.60 2.68 o -5 2 1 5.55 4.59 1.16 o -4 2 1 296.78 301.34 6.21 o -3 2 1 492.60 529.77 9.67 o -2 2 1 0.47 0.21 0.25 o -1 2 1 417.39 388.44 7.09 o 0 2 1 1736.21 1594.07 19.38 o 1 2 1 349.88 324.51 9.64 o 2 2 1 148.31 162.32 2.81 o 3 2 1 470.55 503.10 8.32 o 4 2 1 758.99 753.90 9.33 o 5 2 1 1054.46 1058.11 14.48 o 6 2 1 105.71 114.70 2.86 o 7 2 1 15.58 18.27 1.80 o -7 3 1 63.12 63.48 1.91 o -6 3 1 171.92 174.30 3.78 o -5 3 1 0.08 2.30 1.10 o -4 3 1 0.52 -0.60 1.03 o -3 3 1 2037.32 2128.60 33.10 o -2 3 1 162.04 153.92 3.02 o -1 3 1 3711.75 3435.13 45.19 o 0 3 1 696.30 665.53 9.54 o 1 3 1 887.48 919.17 22.66 o 2 3 1 21.22 21.28 1.05 o 3 3 1 138.66 140.37 3.30 o 4 3 1 27.64 32.29 2.05 o 5 3 1 20.06 20.41 1.58 o 6 3 1 86.98 83.19 2.41 o 7 3 1 78.42 79.92 2.20 o -7 4 1 1.61 0.83 0.76 o -6 4 1 7.94 8.55 1.51 o -5 4 1 1.25 1.55 1.48 o -4 4 1 121.93 124.07 3.00 o -3 4 1 68.77 61.55 1.70 o -2 4 1 7.00 4.12 0.49 o -1 4 1 26.34 21.14 0.78 o 0 4 1 4521.94 4394.04 72.77 o 1 4 1 488.33 454.95 10.97 o 2 4 1 1303.95 1243.54 25.19 o 3 4 1 141.75 144.05 3.39 o 4 4 1 1532.62 1515.29 17.05 o 5 4 1 0.51 1.12 0.96 o 6 4 1 5.72 5.20 0.95 o 7 4 1 2.42 5.96 1.65 o -7 5 1 35.43 41.45 1.61 o -6 5 1 53.85 54.57 2.01 o -5 5 1 25.33 24.22 2.08 o -4 5 1 4.94 4.79 1.03 o -3 5 1 37.15 45.32 1.97 o -2 5 1 1337.32 1341.87 19.04 o -1 5 1 23453.47 24234.08 515.07 o 0 5 1 229.08 219.32 4.96 o 1 5 1 6485.83 6444.51 194.50 o 2 5 1 8.87 13.14 1.01 o 3 5 1 0.99 -0.20 0.70 o 4 5 1 0.01 1.15 0.99 o 5 5 1 0.34 0.78 0.95 o 6 5 1 68.28 65.09 2.99 o 7 5 1 34.68 33.33 1.73 o -7 6 1 3.16 1.44 0.76 o -6 6 1 375.71 353.53 5.85 o -5 6 1 544.36 560.51 9.60 o -4 6 1 65.78 66.17 2.12 o -3 6 1 175.06 178.64 3.95 o -2 6 1 430.40 441.30 6.50 o -1 6 1 4187.61 4011.83 114.14 o 0 6 1 0.32 0.20 0.23 o 1 6 1 1265.74 1178.76 48.42 o 2 6 1 213.64 262.57 5.92 o 3 6 1 392.58 417.73 8.10 o 4 6 1 182.27 203.70 3.19 o 5 6 1 0.18 1.05 1.03 o 6 6 1 207.83 182.25 5.58 o 7 6 1 0.04 1.51 0.73 o -7 7 1 1.36 2.13 0.77 o -6 7 1 46.21 51.16 1.91 o -5 7 1 21.91 16.20 1.68 o -4 7 1 29.33 38.70 1.96 o -3 7 1 11.60 8.39 1.36 o -2 7 1 290.01 336.01 11.33 o -1 7 1 289.23 237.49 5.25 o 0 7 1 527.92 513.76 11.98 o 1 7 1 1180.94 1171.99 34.51 o 2 7 1 1381.49 1426.16 28.84 o 3 7 1 176.47 185.40 4.34 o 4 7 1 14.79 13.35 1.49 o 5 7 1 36.84 34.33 2.32 o 6 7 1 580.08 558.99 8.51 o 7 7 1 49.05 49.62 1.78 o -7 8 1 41.82 37.01 1.57 o -6 8 1 5.49 7.22 1.25 o -5 8 1 278.69 264.60 4.79 o -4 8 1 4.21 5.12 1.15 o -2 8 1 3.05 4.66 1.10 o -1 8 1 239.90 242.48 13.96 o 0 8 1 1.01 1.88 0.79 o 1 8 1 62.86 41.14 1.84 o 2 8 1 127.44 128.60 3.40 o 3 8 1 767.27 758.19 8.47 o 4 8 1 8.52 9.02 1.12 o 5 8 1 9.68 14.25 1.36 o 6 8 1 73.20 86.47 2.17 o -7 9 1 0.04 0.02 0.95 o -6 9 1 31.79 39.11 1.79 o -5 9 1 11.38 6.00 1.12 o -4 9 1 120.15 106.36 3.09 o -3 9 1 6.25 8.33 2.06 o -2 9 1 5729.13 5331.97 129.87 o -1 9 1 97.03 96.09 3.62 o 0 9 1 522.92 479.53 17.21 o 1 9 1 5.86 4.12 0.75 o 2 9 1 903.77 973.40 20.04 o 3 9 1 5.27 4.64 0.90 o 4 9 1 4.91 3.03 1.43 o 5 9 1 29.95 22.12 1.71 o 6 9 1 0.01 0.50 0.78 o -7 10 1 168.23 172.01 3.94 o -6 10 1 23.03 23.63 1.71 o -5 10 1 5.59 0.43 1.32 o -4 10 1 2.64 3.22 2.28 o -3 10 1 3.85 4.11 0.92 o -2 10 1 2995.32 2857.23 70.25 o -1 10 1 32.39 32.75 1.85 o 0 10 1 0.14 0.87 0.71 o 1 10 1 302.93 263.82 7.32 o 2 10 1 204.03 214.56 5.28 o 3 10 1 945.01 960.30 11.69 o 4 10 1 179.60 178.67 3.41 o 5 10 1 8.93 3.03 0.93 o 6 10 1 13.21 11.56 1.33 o -6 11 1 85.96 89.10 2.30 o -5 11 1 65.50 47.85 2.41 o -4 11 1 237.28 224.33 6.74 o -3 11 1 0.16 0.41 0.89 o -2 11 1 1001.95 937.07 28.46 o -1 11 1 165.81 164.67 5.03 o 0 11 1 18.63 16.98 1.37 o 1 11 1 70.83 72.63 4.49 o 2 11 1 120.53 118.72 2.48 o 3 11 1 163.21 165.58 2.92 o 4 11 1 98.22 96.69 2.54 o 5 11 1 16.97 24.08 1.61 o 6 11 1 24.10 23.94 1.44 o -6 12 1 22.77 21.14 2.05 o -5 12 1 49.22 49.39 3.42 o -4 12 1 170.10 159.75 3.53 o -3 12 1 15.66 17.11 1.54 o -2 12 1 312.16 299.96 4.55 o -1 12 1 90.82 97.11 5.49 o 0 12 1 13.21 21.09 2.29 o 1 12 1 2.20 3.62 1.01 o 2 12 1 194.38 192.24 3.17 o 3 12 1 57.15 61.16 1.98 o 4 12 1 0.57 1.76 1.91 o 5 12 1 18.20 25.65 1.55 o 6 12 1 4.00 1.14 0.65 o -6 13 1 61.99 58.49 2.09 o -5 13 1 26.14 28.25 1.98 o -4 13 1 171.47 150.33 3.34 o -3 13 1 1.32 2.16 0.95 o -2 13 1 256.31 271.70 4.22 o -1 13 1 3.14 5.93 1.27 o 0 13 1 25.14 29.50 1.95 o 1 13 1 1622.50 1650.28 19.45 o 2 13 1 1.03 1.74 0.90 o 3 13 1 3.85 2.51 0.89 o 4 13 1 100.41 89.78 2.33 o 5 13 1 19.47 21.14 1.44 o 6 13 1 29.21 30.31 1.36 o -6 14 1 1.22 0.16 0.65 o -5 14 1 5.17 7.30 1.39 o -4 14 1 49.89 59.31 2.16 o -3 14 1 1027.38 1050.60 13.44 o -2 14 1 237.00 238.09 4.17 o -1 14 1 16.62 15.16 1.90 o 0 14 1 33.70 29.02 1.85 o 1 14 1 0.01 -0.09 0.82 o 2 14 1 2.52 2.48 0.89 o 3 14 1 55.27 53.60 1.89 o 4 14 1 6.00 1.22 0.88 o 5 14 1 3.91 4.36 0.80 o -6 15 1 0.09 0.37 0.63 o -5 15 1 3.29 4.80 0.87 o -4 15 1 199.76 194.30 3.85 o -3 15 1 54.37 58.99 1.97 o -2 15 1 43.72 41.90 1.99 o -1 15 1 42.32 39.08 1.97 o 0 15 1 35.01 39.18 1.95 o 1 15 1 47.27 38.85 1.78 o 2 15 1 142.26 148.00 2.73 o 3 15 1 19.87 26.00 1.62 o 4 15 1 209.23 213.08 3.60 o 5 15 1 23.56 20.82 1.26 o -5 16 1 10.00 8.50 0.98 o -4 16 1 9.84 8.62 1.11 o -3 16 1 393.69 406.28 5.75 o -2 16 1 9.10 9.28 1.06 o -1 16 1 2.26 2.92 0.99 o 0 16 1 7.47 9.82 1.19 o 1 16 1 6.93 6.21 0.98 o 2 16 1 138.95 151.89 2.74 o 3 16 1 18.32 17.72 1.39 o 4 16 1 0.47 1.73 0.73 o 5 16 1 27.53 28.39 1.47 o -5 17 1 12.38 19.21 1.47 o -4 17 1 67.58 64.35 1.95 o -3 17 1 32.55 34.07 1.81 o -2 17 1 66.62 65.81 2.08 o -1 17 1 6.19 5.57 0.98 o 0 17 1 187.35 197.93 3.60 o 1 17 1 149.12 164.72 2.99 o 2 17 1 5.36 4.78 0.85 o 3 17 1 124.75 128.01 2.45 o 4 17 1 17.58 15.25 1.21 o 5 17 1 1.30 0.64 0.54 o -5 18 1 54.82 47.95 1.53 o -4 18 1 11.25 7.32 1.18 o -3 18 1 141.07 149.98 2.84 o -2 18 1 47.38 51.22 1.87 o -1 18 1 133.95 139.14 2.88 o 0 18 1 201.07 196.78 3.56 o 1 18 1 2.40 4.11 1.24 o 2 18 1 236.85 250.19 3.88 o 3 18 1 30.32 28.06 1.46 o 4 18 1 4.76 4.18 1.29 o -4 19 1 36.94 32.97 1.45 o -3 19 1 16.94 14.46 1.31 o -2 19 1 229.68 254.84 4.15 o -1 19 1 2.94 2.19 0.86 o 0 19 1 21.04 20.97 1.61 o 1 19 1 43.93 48.66 1.72 o 2 19 1 8.32 8.24 1.02 o 3 19 1 11.31 12.46 1.23 o 4 19 1 0.24 1.51 0.59 o -4 20 1 64.35 64.38 1.91 o -3 20 1 36.81 33.40 1.34 o -2 20 1 324.40 327.35 4.94 o -1 20 1 121.40 128.69 2.76 o 0 20 1 34.15 33.77 1.63 o 1 20 1 0.06 0.09 0.95 o 2 20 1 3.77 5.30 0.83 o 3 20 1 29.15 30.29 1.27 o 4 20 1 1.61 1.29 0.66 o -3 21 1 71.78 65.59 1.69 o -2 21 1 51.03 50.31 1.59 o -1 21 1 54.87 55.88 1.91 o 0 21 1 40.88 40.15 1.56 o 1 21 1 46.24 47.70 1.60 o 2 21 1 60.58 59.59 1.61 o 3 21 1 0.34 0.00 0.68 o -3 22 1 10.15 11.51 1.52 o -2 22 1 82.85 78.22 1.76 o -1 22 1 139.26 134.51 2.58 o 0 22 1 4.99 5.98 1.12 o 1 22 1 27.60 26.16 1.18 o 2 22 1 0.27 1.04 0.57 o -2 23 1 22.11 24.29 1.12 o -1 23 1 169.03 163.73 2.87 o 0 23 1 22.10 24.75 1.90 o 1 23 1 0.09 0.16 0.62 o 2 23 1 3.53 2.28 0.75 o -1 24 1 120.21 113.04 2.21 o 0 24 1 219.69 201.02 3.21 o -7 0 2 78.94 78.19 3.16 o -6 0 2 212.29 216.80 5.79 o -5 0 2 5.27 5.55 2.16 o -4 0 2 408.09 425.21 11.84 o -3 0 2 1391.83 1376.43 48.39 o -2 0 2 141.64 125.18 3.71 o -1 0 2 690.54 673.25 14.81 o 0 0 2 29726.79 34148.21 854.60 o 1 0 2 1565.38 1578.99 50.83 o 2 0 2 248.44 204.08 5.65 o 3 0 2 7.96 9.13 1.43 o 4 0 2 249.05 229.44 4.85 o 5 0 2 105.94 110.37 3.44 o 6 0 2 398.03 383.64 8.66 o 7 0 2 16.14 19.34 1.73 o -7 1 2 22.40 16.76 1.83 o -6 1 2 2.49 0.68 1.01 o -5 1 2 35.98 33.36 2.53 o -4 1 2 591.35 588.19 9.03 o -3 1 2 112.81 123.10 2.81 o -2 1 2 402.93 398.57 7.23 o -1 1 2 3860.68 3690.78 83.17 o 0 1 2 171.85 150.32 2.31 o 1 1 2 4008.73 3547.67 92.99 o 2 1 2 960.33 965.73 19.84 o 3 1 2 213.47 229.78 3.89 o 4 1 2 265.61 259.21 4.11 o 5 1 2 82.34 97.63 2.40 o 6 1 2 79.96 68.85 1.97 o 7 1 2 0.20 0.13 0.83 o -7 2 2 15.99 17.66 1.59 o -6 2 2 1.41 -0.52 0.95 o -5 2 2 226.68 242.01 5.11 o -4 2 2 19.60 18.47 1.58 o -3 2 2 178.52 137.74 2.79 o -2 2 2 0.15 0.16 0.26 o -1 2 2 483.41 482.44 7.66 o 0 2 2 250.12 226.10 3.67 o 1 2 2 197.45 227.59 4.27 o 2 2 2 104.67 106.76 2.94 o 3 2 2 59.73 63.56 1.72 o 4 2 2 206.39 201.80 3.47 o 5 2 2 1098.74 1160.93 15.81 o 6 2 2 73.63 67.11 1.86 o 7 2 2 0.89 -0.35 1.11 o -7 3 2 7.36 7.65 1.06 o -6 3 2 53.98 54.31 2.18 o -5 3 2 74.07 66.40 2.78 o -4 3 2 1303.05 1279.56 20.46 o -3 3 2 35.04 34.63 1.31 o -2 3 2 14.24 20.36 0.80 o -1 3 2 63.23 61.70 1.47 o 0 3 2 177.42 183.15 3.24 o 1 3 2 149.18 135.24 5.23 o 2 3 2 5.92 5.78 0.91 o 3 3 2 111.17 121.98 2.81 o 4 3 2 752.70 722.91 9.84 o 5 3 2 252.16 251.75 4.19 o 6 3 2 539.16 530.98 7.54 o 7 3 2 9.24 12.32 1.96 o -7 4 2 0.84 2.24 1.12 o -6 4 2 60.92 56.05 2.93 o -5 4 2 479.46 468.67 8.19 o -4 4 2 227.35 222.26 4.53 o -3 4 2 464.02 508.77 8.42 o -2 4 2 663.09 653.98 11.61 o -1 4 2 17891.59 17623.43 246.79 o 0 4 2 227.26 259.30 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