#------------------------------------------------------------------------------ #$Date: 2016-06-11 05:20:56 +0300 (Sat, 11 Jun 2016) $ #$Revision: 183357 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/34/1543418.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1543418 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.1780 _cell_length_b 6.9190 _cell_length_c 7.6410 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.6616 _cod_data_source_file sj4042Isup2.hkl _cod_data_source_block I _shelx_title ' DMP4_test6 in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 178.74 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1066.82 1188.69 57.01 o 6 0 0 15133.63 15701.90 373.46 o 8 0 0 3163.87 3460.57 201.10 o 10 0 0 8967.59 9136.66 363.43 o 12 0 0 66.44 79.23 40.06 o 14 0 0 1307.15 1310.72 171.32 o 16 0 0 1326.09 1445.64 195.88 o 18 0 0 84.08 101.90 62.20 o 2 1 0 1631.97 1655.25 32.85 o 4 1 0 30884.10 27654.30 229.98 o 6 1 0 11740.44 11206.71 173.54 o 8 1 0 77.83 66.58 20.21 o 10 1 0 5251.87 5384.28 202.96 o 12 1 0 889.67 859.85 87.92 o 14 1 0 1917.20 1996.22 147.49 o 16 1 0 310.99 392.31 74.05 o 18 1 0 5.48 65.38 57.16 o 20 1 0 523.75 701.16 160.73 o 2 2 0 331.58 350.48 15.11 o 4 2 0 478.00 509.05 25.63 o 6 2 0 10066.85 9401.70 142.16 o 8 2 0 2082.86 2177.81 170.24 o 10 2 0 6218.65 6381.61 379.20 o 12 2 0 51.69 0.67 24.96 o 14 2 0 927.61 893.50 145.93 o 16 2 0 935.72 1086.27 174.55 o 18 2 0 61.53 124.76 72.21 o 2 3 0 860.15 899.14 30.30 o 4 3 0 11697.72 11228.94 145.09 o 6 3 0 5175.27 5006.59 119.59 o 8 3 0 17.35 71.65 40.19 o 10 3 0 2502.17 2864.74 235.96 o 12 3 0 458.05 476.77 97.24 o 14 3 0 944.90 1037.70 161.26 o 16 3 0 181.93 204.77 78.50 o 18 3 0 1.57 61.16 54.77 o 0 4 0 25291.28 23830.46 597.48 o 2 4 0 54.11 45.43 6.86 o 4 4 0 85.43 66.57 17.87 o 6 4 0 3202.03 3062.28 92.13 o 8 4 0 688.34 725.85 71.15 o 10 4 0 2102.53 2319.80 156.35 o 12 4 0 19.71 3.89 24.43 o 14 4 0 331.67 295.94 89.51 o 16 4 0 333.18 405.37 112.47 o 18 4 0 24.24 33.27 46.49 o 2 5 0 165.06 150.67 15.12 o 4 5 0 2435.14 2029.85 171.64 o 6 5 0 1184.06 1347.28 92.04 o 8 5 0 2.15 3.90 25.41 o 10 5 0 558.50 643.93 75.25 o 12 5 0 127.83 146.35 26.78 o 14 5 0 226.80 274.00 48.90 o 16 5 0 63.98 79.11 50.91 o 0 6 0 4241.18 4201.32 375.23 o 2 6 0 21.22 21.81 7.56 o 4 6 0 12.03 6.29 22.08 o 6 6 0 561.82 610.90 63.46 o 8 6 0 135.01 143.28 32.70 o 10 6 0 357.01 367.44 55.37 o 12 6 0 2.97 -2.22 7.06 o 14 6 0 60.88 85.84 30.58 o 16 6 0 61.91 87.06 61.22 o 2 7 0 12.14 21.12 14.23 o 4 7 0 272.90 317.21 55.60 o 6 7 0 148.03 148.28 63.93 o 8 7 0 0.09 0.37 28.02 o 10 7 0 56.67 87.32 29.19 o 12 7 0 20.98 16.35 12.01 o 14 7 0 25.98 71.90 51.53 o 0 8 0 512.92 648.48 112.93 o 2 8 0 12.95 15.90 18.61 o 4 8 0 1.03 7.46 21.55 o 6 8 0 63.44 101.07 47.64 o 8 8 0 17.24 32.69 29.37 o 10 8 0 31.31 83.00 47.96 o 12 8 0 0.14 42.41 35.18 o 2 9 0 0.24 34.67 30.29 o 4 9 0 14.14 41.09 37.52 o 6 9 0 10.42 25.77 28.50 o 8 9 0 0.03 14.27 23.59 o 1 0 1 959.96 962.77 36.22 o 2 0 1 11169.20 10786.23 288.81 o 3 0 1 786.25 845.81 38.67 o 4 0 1 49.59 93.72 13.09 o 5 0 1 7429.46 7555.58 154.25 o 6 0 1 6464.97 6432.82 167.95 o 7 0 1 924.92 1059.02 72.73 o 8 0 1 10137.25 9317.51 242.29 o 9 0 1 222.80 232.70 43.53 o 10 0 1 77.37 40.51 20.38 o 11 0 1 1518.73 1495.66 111.95 o 12 0 1 319.37 354.59 58.05 o 13 0 1 171.95 205.50 44.30 o 14 0 1 386.21 387.75 68.28 o 15 0 1 232.07 257.49 75.20 o 16 0 1 580.28 624.11 123.79 o 17 0 1 2.32 16.89 25.47 o 18 0 1 619.11 771.43 153.17 o 19 0 1 141.28 284.09 96.42 o 20 0 1 7.99 97.87 68.52 o 0 1 1 49.49 56.56 9.20 o 1 1 1 9471.21 9581.05 78.11 o 2 1 1 11008.48 11009.53 88.79 o 3 1 1 206.20 216.88 9.29 o 4 1 1 12557.17 11987.71 94.33 o 5 1 1 1909.40 1887.32 36.55 o 6 1 1 2765.94 2737.18 49.46 o 7 1 1 405.40 337.95 19.79 o 8 1 1 300.56 305.74 20.15 o 9 1 1 3659.28 3495.10 172.13 o 10 1 1 335.38 294.48 21.69 o 11 1 1 179.44 175.77 17.16 o 12 1 1 2505.55 2549.20 126.69 o 13 1 1 102.34 92.13 17.98 o 14 1 1 1006.58 1101.69 89.22 o 15 1 1 922.22 978.02 89.53 o 16 1 1 2.66 16.48 9.16 o 17 1 1 2.34 11.74 14.33 o 18 1 1 79.56 129.08 48.27 o 19 1 1 13.11 75.83 43.12 o 20 1 1 0.27 60.50 56.93 o 1 2 1 339.53 425.87 14.20 o 2 2 1 7532.05 7521.01 75.57 o 3 2 1 471.69 513.25 14.02 o 4 2 1 69.99 75.88 6.14 o 5 2 1 4808.43 4676.14 85.00 o 6 2 1 4118.12 3845.31 100.37 o 7 2 1 619.74 644.96 29.99 o 8 2 1 6698.50 6193.30 116.18 o 9 2 1 153.60 156.92 17.32 o 10 2 1 47.59 59.54 11.60 o 11 2 1 1051.01 1096.78 78.43 o 12 2 1 232.09 258.29 41.57 o 13 2 1 119.95 96.85 33.26 o 14 2 1 285.73 307.89 49.01 o 15 2 1 161.46 182.48 39.18 o 16 2 1 411.45 422.69 60.58 o 17 2 1 1.94 31.81 38.35 o 18 2 1 441.97 548.88 131.16 o 19 2 1 100.24 179.64 86.23 o 0 3 1 89.76 92.63 9.55 o 1 3 1 3586.36 3595.24 54.80 o 2 3 1 4645.90 4570.96 57.76 o 3 3 1 94.79 108.42 10.87 o 4 3 1 4686.21 4296.74 76.76 o 5 3 1 817.82 795.45 26.38 o 6 3 1 1387.66 1276.64 40.78 o 7 3 1 190.61 173.49 15.88 o 8 3 1 143.60 139.43 20.39 o 9 3 1 1775.34 1714.38 87.54 o 10 3 1 177.81 172.29 30.65 o 11 3 1 73.59 91.27 32.79 o 12 3 1 1122.23 1210.47 71.45 o 13 3 1 56.38 50.72 30.28 o 14 3 1 518.85 572.75 83.69 o 15 3 1 477.66 538.16 87.09 o 16 3 1 1.97 -5.37 24.58 o 17 3 1 0.61 19.62 33.13 o 18 3 1 36.83 83.55 36.38 o 1 4 1 53.58 49.78 8.79 o 2 4 1 2406.17 2383.06 50.09 o 3 4 1 125.70 137.20 12.64 o 4 4 1 28.49 16.40 2.57 o 5 4 1 1440.70 1298.27 49.36 o 6 4 1 1272.90 1188.46 39.51 o 7 4 1 225.12 235.94 19.38 o 8 4 1 2116.62 2189.48 62.19 o 9 4 1 48.23 50.85 12.15 o 10 4 1 17.38 33.46 9.77 o 11 4 1 351.94 381.79 33.66 o 12 4 1 92.89 107.40 16.75 o 13 4 1 40.64 51.64 24.25 o 14 4 1 115.22 120.40 33.92 o 15 4 1 54.21 40.25 41.06 o 16 4 1 150.17 168.77 52.74 o 17 4 1 1.12 5.80 25.89 o 18 4 1 162.02 280.44 70.92 o 0 5 1 21.82 29.29 7.27 o 1 5 1 766.31 783.86 28.82 o 2 5 1 987.42 1047.80 37.13 o 3 5 1 25.57 21.29 6.17 o 4 5 1 978.57 932.85 43.82 o 5 5 1 190.40 168.19 18.17 o 6 5 1 312.36 313.64 32.60 o 7 5 1 42.56 55.44 14.13 o 8 5 1 28.66 32.50 10.08 o 9 5 1 454.62 463.83 36.24 o 10 5 1 63.98 55.43 11.83 o 11 5 1 9.68 19.57 14.69 o 12 5 1 223.76 249.01 32.26 o 13 5 1 17.86 24.29 21.17 o 14 5 1 146.03 171.84 56.16 o 15 5 1 132.81 157.31 94.60 o 16 5 1 0.91 12.52 45.34 o 17 5 1 0.70 25.89 71.32 o 1 6 1 25.83 18.61 5.78 o 2 6 1 377.78 365.25 24.84 o 3 6 1 14.35 14.47 6.04 o 4 6 1 1.81 4.99 5.90 o 5 6 1 200.65 193.09 22.04 o 6 6 1 231.44 228.64 33.79 o 7 6 1 57.53 65.46 19.40 o 8 6 1 337.72 420.96 48.36 o 9 6 1 6.02 20.30 21.44 o 10 6 1 5.60 36.22 16.84 o 11 6 1 57.65 52.45 30.37 o 12 6 1 22.46 19.24 17.70 o 13 6 1 6.58 -18.43 31.80 o 14 6 1 26.51 30.64 52.58 o 15 6 1 8.69 6.92 11.37 o 16 6 1 29.70 35.56 55.06 o 0 7 1 2.75 -8.75 8.75 o 1 7 1 92.81 100.65 17.62 o 2 7 1 106.79 144.62 22.73 o 3 7 1 4.48 1.89 8.63 o 4 7 1 118.05 146.12 23.50 o 5 7 1 27.18 27.73 14.26 o 6 7 1 33.55 46.22 16.40 o 7 7 1 4.76 11.92 11.66 o 8 7 1 2.19 7.94 15.81 o 9 7 1 67.55 64.12 18.43 o 10 7 1 16.71 21.07 10.34 o 11 7 1 0.20 -5.54 12.83 o 12 7 1 16.65 9.50 11.14 o 13 7 1 3.46 4.93 7.19 o 14 7 1 24.31 12.86 24.76 o 15 7 1 21.44 102.72 69.11 o 1 8 1 14.22 33.04 17.61 o 2 8 1 32.00 32.83 15.33 o 3 8 1 0.31 6.15 13.93 o 4 8 1 0.02 -0.62 5.36 o 5 8 1 10.52 15.25 11.41 o 6 8 1 26.43 31.92 19.32 o 7 8 1 11.42 15.21 11.89 o 8 8 1 25.22 42.57 19.53 o 9 8 1 0.16 -12.19 17.81 o 10 8 1 1.29 11.04 4.12 o 11 8 1 4.56 2.34 13.20 o 12 8 1 3.63 -10.52 10.52 o 13 8 1 0.47 -15.40 21.61 o 0 9 1 0.43 27.68 37.43 o 1 9 1 6.34 56.02 28.48 o 2 9 1 5.73 27.63 22.56 o 3 9 1 0.66 28.15 32.49 o 4 9 1 7.56 21.19 17.78 o 5 9 1 2.64 7.79 9.41 o 6 9 1 1.84 -2.27 26.07 o 7 9 1 0.33 -1.41 12.37 o 8 9 1 0.03 7.70 11.07 o 9 9 1 6.77 4.11 13.29 o 0 0 2 8489.50 9483.60 193.73 o 1 0 2 1637.87 1681.14 49.74 o 2 0 2 237.92 212.34 17.96 o 3 0 2 31947.14 27531.74 339.15 o 4 0 2 44.72 44.58 13.89 o 5 0 2 0.36 4.79 10.59 o 6 0 2 26.18 55.93 27.09 o 7 0 2 4638.14 4441.70 232.56 o 8 0 2 22.79 13.04 4.43 o 9 0 2 631.49 607.18 93.22 o 10 0 2 793.40 792.78 113.42 o 11 0 2 3094.34 3103.12 236.21 o 12 0 2 96.60 88.49 44.61 o 13 0 2 3455.66 3699.91 277.75 o 14 0 2 177.36 104.50 27.63 o 15 0 2 22.53 -30.39 49.52 o 16 0 2 42.96 -13.17 32.33 o 17 0 2 74.86 93.49 49.60 o 18 0 2 16.66 -17.99 17.99 o 19 0 2 62.76 77.74 52.42 o 20 0 2 0.86 95.81 65.39 o 1 1 2 13881.18 13146.11 267.86 o 2 1 2 91.32 98.81 12.25 o 3 1 2 6598.93 7152.83 88.57 o 4 1 2 3767.80 3846.06 66.43 o 5 1 2 314.70 355.24 16.95 o 6 1 2 436.64 401.41 47.50 o 7 1 2 15138.04 14197.34 289.22 o 8 1 2 14.97 3.38 9.78 o 9 1 2 5233.43 5035.53 139.69 o 10 1 2 1126.00 981.74 75.13 o 11 1 2 1615.51 1647.82 121.48 o 12 1 2 6.97 4.08 18.05 o 13 1 2 620.70 638.00 84.98 o 14 1 2 200.82 144.22 37.49 o 15 1 2 18.82 -3.72 38.04 o 16 1 2 26.53 -5.09 21.17 o 17 1 2 1255.78 1423.09 142.99 o 18 1 2 5.34 7.34 16.20 o 19 1 2 38.80 60.91 30.36 o 20 1 2 50.09 74.17 37.55 o 0 2 2 4459.02 4542.20 135.51 o 1 2 2 1056.44 1070.90 39.80 o 2 2 2 120.90 138.80 12.30 o 3 2 2 19826.42 19472.30 168.07 o 4 2 2 44.37 42.20 9.21 o 5 2 2 0.13 1.61 1.89 o 6 2 2 32.58 24.29 3.87 o 7 2 2 3148.24 3080.55 75.63 o 8 2 2 11.45 13.01 10.88 o 9 2 2 432.85 415.27 29.67 o 10 2 2 558.62 574.94 34.91 o 11 2 2 2167.66 2163.11 69.29 o 12 2 2 73.79 56.90 10.99 o 13 2 2 2391.58 2590.95 163.96 o 14 2 2 130.08 184.50 65.56 o 15 2 2 17.94 9.68 44.96 o 16 2 2 28.45 22.59 67.49 o 17 2 2 53.08 77.36 31.44 o 18 2 2 12.42 20.97 55.65 o 19 2 2 42.47 24.77 67.39 o 1 3 2 5500.71 5254.21 84.67 o 2 3 2 2.44 16.51 10.47 o 3 3 2 2776.52 2873.30 78.20 o 4 3 2 1394.53 1464.53 39.65 o 5 3 2 113.88 99.62 8.82 o 6 3 2 210.88 229.15 13.36 o 7 3 2 6910.91 6631.69 87.80 o 8 3 2 3.05 -4.99 8.38 o 9 3 2 2543.65 2576.29 80.87 o 10 3 2 608.88 621.70 41.12 o 11 3 2 856.51 862.80 49.90 o 12 3 2 6.86 17.42 11.18 o 13 3 2 343.07 396.15 57.28 o 14 3 2 100.44 121.18 39.90 o 15 3 2 10.74 -7.09 58.09 o 16 3 2 12.73 12.95 31.21 o 17 3 2 649.47 782.60 160.75 o 18 3 2 2.64 -66.82 66.82 o 0 4 2 1074.40 1112.89 58.88 o 1 4 2 331.73 301.17 30.55 o 2 4 2 34.16 29.95 4.97 o 3 4 2 5727.10 5992.73 96.52 o 4 4 2 23.60 13.53 6.82 o 5 4 2 0.48 8.90 12.39 o 6 4 2 9.42 12.09 10.41 o 7 4 2 1045.39 1000.11 39.50 o 8 4 2 1.61 4.61 10.02 o 9 4 2 148.22 175.30 20.81 o 10 4 2 190.03 217.59 23.24 o 11 4 2 770.40 825.65 56.47 o 12 4 2 29.57 36.00 19.42 o 13 4 2 796.22 1115.64 129.98 o 14 4 2 51.01 129.92 52.13 o 15 4 2 9.24 -85.50 85.50 o 16 4 2 8.19 -45.29 65.89 o 17 4 2 18.89 -13.67 38.40 o 1 5 2 1133.43 1051.95 52.63 o 2 5 2 0.10 -1.04 3.95 o 3 5 2 620.38 630.07 42.27 o 4 5 2 308.82 338.14 31.04 o 5 5 2 26.19 32.80 21.03 o 6 5 2 44.65 53.79 15.32 o 7 5 2 1596.44 1634.51 64.77 o 8 5 2 1.22 11.38 11.30 o 9 5 2 662.63 743.58 55.07 o 10 5 2 183.59 203.71 28.84 o 11 5 2 263.16 280.91 34.79 o 12 5 2 5.62 -1.46 8.45 o 13 5 2 112.20 198.75 45.17 o 14 5 2 24.14 98.49 42.70 o 15 5 2 3.80 -18.69 79.10 o 16 5 2 2.63 6.47 85.30 o 0 6 2 164.68 166.74 29.17 o 1 6 2 57.48 34.76 13.11 o 2 6 2 6.97 26.42 14.49 o 3 6 2 873.52 994.98 59.62 o 4 6 2 7.82 -0.23 8.70 o 5 6 2 1.15 -6.62 8.57 o 6 6 2 0.54 -7.56 7.56 o 7 6 2 185.18 198.30 31.47 o 8 6 2 0.26 6.62 13.99 o 9 6 2 28.03 42.14 16.83 o 10 6 2 31.04 40.48 21.13 o 11 6 2 147.15 177.38 31.46 o 12 6 2 6.00 -23.32 30.02 o 13 6 2 126.54 104.92 131.15 o 14 6 2 10.92 -46.26 46.26 o 15 6 2 3.24 -62.34 65.45 o 1 7 2 126.21 147.06 25.01 o 2 7 2 0.10 -2.16 7.13 o 3 7 2 81.39 42.38 16.92 o 4 7 2 43.48 39.08 7.22 o 5 7 2 5.49 -2.10 6.98 o 6 7 2 3.53 -1.66 8.51 o 7 7 2 196.02 208.12 43.81 o 8 7 2 0.74 9.29 37.15 o 9 7 2 100.85 156.40 46.53 o 10 7 2 35.04 55.17 31.80 o 11 7 2 53.02 74.51 57.34 o 12 7 2 2.91 41.45 41.73 o 13 7 2 24.27 -68.29 68.29 o 14 7 2 2.74 -62.42 62.42 o 15 7 2 0.91 26.03 23.47 o 0 8 2 12.65 47.00 31.74 o 1 8 2 6.00 21.94 12.51 o 2 8 2 0.64 5.67 15.69 o 3 8 2 66.55 115.31 33.83 o 4 8 2 2.37 -2.29 14.56 o 5 8 2 0.75 3.22 16.82 o 6 8 2 1.66 -34.10 34.10 o 7 8 2 18.79 24.99 9.70 o 8 8 2 0.42 -6.90 27.76 o 9 8 2 3.14 -11.26 12.82 o 10 8 2 2.53 -12.46 12.46 o 11 8 2 15.99 -3.28 17.85 o 12 8 2 0.73 -82.93 82.93 o 1 9 2 7.39 39.01 27.64 o 2 9 2 0.00 28.50 22.30 o 3 9 2 6.83 22.01 20.19 o 4 9 2 3.82 -6.54 26.54 o 5 9 2 1.08 11.17 16.87 o 6 9 2 0.07 -14.04 22.23 o 1 0 3 1079.75 1136.42 69.97 o 2 0 3 3580.14 3895.29 114.17 o 3 0 3 1090.85 1031.50 57.00 o 4 0 3 121.80 228.67 27.72 o 5 0 3 22937.49 22840.10 536.45 o 6 0 3 19.84 36.21 20.39 o 7 0 3 679.12 768.49 105.92 o 8 0 3 1425.37 1524.27 148.32 o 9 0 3 302.50 227.63 53.90 o 10 0 3 10.17 -27.46 32.28 o 11 0 3 3377.09 3274.28 254.21 o 12 0 3 7.43 21.74 25.16 o 13 0 3 244.56 285.19 85.61 o 14 0 3 82.61 136.70 62.66 o 15 0 3 903.95 1045.31 163.52 o 16 0 3 87.89 6.77 52.11 o 17 0 3 17.07 -14.01 34.85 o 18 0 3 21.66 5.85 32.94 o 19 0 3 184.20 142.40 62.02 o 20 0 3 23.86 70.35 46.47 o 0 1 3 370.81 452.69 54.28 o 1 1 3 17695.38 18219.91 229.14 o 2 1 3 3057.06 3351.42 61.25 o 3 1 3 138.02 171.81 30.38 o 4 1 3 8.61 9.60 8.15 o 5 1 3 1032.58 978.51 41.80 o 6 1 3 232.74 202.23 14.68 o 7 1 3 1228.18 1273.23 94.02 o 8 1 3 172.07 184.37 34.74 o 9 1 3 5461.26 5435.35 211.25 o 10 1 3 11.37 0.44 37.21 o 11 1 3 1788.90 1815.72 133.19 o 12 1 3 304.58 369.77 62.52 o 13 1 3 38.27 45.02 28.88 o 14 1 3 50.44 22.79 36.07 o 15 1 3 1315.82 1324.82 137.56 o 16 1 3 0.33 -29.91 29.91 o 17 1 3 92.26 52.54 11.99 o 18 1 3 9.38 -6.66 30.60 o 19 1 3 59.46 62.46 32.00 o 20 1 3 8.46 58.07 52.81 o 1 2 3 732.36 667.92 60.53 o 2 2 3 2059.09 2288.45 87.33 o 3 2 3 701.03 733.54 51.28 o 4 2 3 112.36 125.06 15.37 o 5 2 3 15278.19 14939.92 292.08 o 6 2 3 14.76 17.23 6.80 o 7 2 3 468.68 468.55 28.61 o 8 2 3 1028.15 997.16 86.86 o 9 2 3 209.16 190.10 35.81 o 10 2 3 5.66 -3.69 31.07 o 11 2 3 2380.32 2339.52 149.63 o 12 2 3 5.30 22.89 13.32 o 13 2 3 170.49 133.56 34.82 o 14 2 3 58.05 32.35 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