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Information card for entry 1543590
Preview
| Coordinates | 1543590.cif |
|---|---|
| Structure factors | 1543590.hkl |
| Original paper (by DOI) | HTML |
| Formula | C17 H37 Cl2 N4 O9 Rh |
|---|---|
| Calculated formula | C17 H37 Cl2 N4 O9 Rh |
| Title of publication | Preparation and reactivity of macrocyclic rhodium(III) alkyl complexes |
| Authors of publication | Jack M. Carraher; Arkady Ellern; Andreja Bakac |
| Journal of publication | Inorganica Chimica Acta |
| Year of publication | 2014 |
| Pages of publication | 254 - 258 |
| a | 7.9942 ± 0.0012 Å |
| b | 15.505 ± 0.002 Å |
| c | 10.2975 ± 0.0015 Å |
| α | 90° |
| β | 102.377 ± 0.002° |
| γ | 90° |
| Cell volume | 1246.7 ± 0.3 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.045 |
| Residual factor for significantly intense reflections | 0.038 |
| Weighted residual factors for significantly intense reflections | 0.0929 |
| Weighted residual factors for all reflections included in the refinement | 0.0963 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.152 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 211137 (current) | 2018-09-24 | cif/ Removing DOI prefixes from 127 CIF files using cif_fix_values r6433. |
1543590.cif 1543590.hkl |
| 184115 | 2016-07-01 | cif/ hkl/ Adding structures of 1543590 via cif-deposit CGI script. |
1543590.cif 1543590.hkl |
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Users of the data should acknowledge the original authors of the
structural data.