#------------------------------------------------------------------------------ #$Date: 2016-08-13 04:39:31 +0300 (Sat, 13 Aug 2016) $ #$Revision: 185791 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/38/1543887.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1543887 _cell_angle_alpha 90.000 _cell_angle_beta 107.553 _cell_angle_gamma 90.000 _cell_length_a 17.5105 _cell_length_b 7.7068 _cell_length_c 10.6885 _exptl_crystal_F_000 680.00 _reflns_d_resolution_high 0.8395 _cod_data_source_file zl4011Isup3.hkl _cod_data_source_block I _shelx_title ' ZS15-15 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 210.40 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 972.82 901.99 15.20 o 4 0 0 58.17 80.15 4.18 o 6 0 0 1332.73 1356.51 18.96 o 8 0 0 590.46 601.36 12.84 o 10 0 0 430.52 426.22 10.42 o 12 0 0 380.81 384.84 11.98 o 14 0 0 1603.90 1673.39 25.42 o 16 0 0 277.44 316.21 15.12 o 18 0 0 8.03 8.87 9.71 o 1 1 0 17.23 -3.06 2.04 o 3 1 0 25.56 31.87 2.04 o 5 1 0 5223.16 5264.54 46.89 o 7 1 0 10303.58 10703.70 77.26 o 9 1 0 31.73 50.29 3.19 o 11 1 0 1210.65 1211.31 14.07 o 13 1 0 415.00 415.27 8.90 o 15 1 0 253.45 289.25 10.28 o 17 1 0 67.16 62.30 7.39 o 19 1 0 1.08 8.47 15.20 o 0 2 0 0.32 -0.33 2.82 o 2 2 0 44269.73 41378.70 390.88 o 4 2 0 6362.02 6524.52 42.94 o 6 2 0 96.44 103.23 4.13 o 8 2 0 179.06 179.82 5.53 o 10 2 0 288.10 291.99 7.55 o 12 2 0 77.33 84.14 4.57 o 14 2 0 44.86 44.05 6.55 o 16 2 0 433.20 513.72 15.84 o 18 2 0 6.01 2.36 4.94 o 1 3 0 949.03 900.80 11.49 o 3 3 0 238.20 219.43 7.50 o 5 3 0 7599.26 7808.33 52.46 o 7 3 0 66.28 65.69 6.34 o 9 3 0 636.41 596.59 10.41 o 11 3 0 4.53 9.16 4.84 o 13 3 0 380.41 389.01 13.73 o 15 3 0 54.65 50.47 7.38 o 17 3 0 128.67 120.56 10.54 o 0 4 0 2.92 4.54 4.02 o 2 4 0 1685.70 1750.77 19.37 o 4 4 0 2847.34 2764.84 26.46 o 6 4 0 632.64 669.72 10.00 o 8 4 0 403.84 403.00 9.40 o 10 4 0 163.93 163.15 10.30 o 12 4 0 684.42 652.36 17.63 o 14 4 0 206.10 181.00 11.78 o 16 4 0 0.02 0.65 5.75 o 1 5 0 0.66 -0.70 5.42 o 3 5 0 25.80 29.79 4.37 o 5 5 0 45.58 53.11 4.93 o 7 5 0 13.22 11.59 4.46 o 9 5 0 0.03 -2.79 5.18 o 11 5 0 194.02 186.88 11.70 o 13 5 0 37.95 26.94 7.29 o 15 5 0 25.28 19.77 8.30 o 0 6 0 123.62 134.38 10.90 o 2 6 0 150.50 148.80 7.91 o 4 6 0 495.04 495.91 12.13 o 6 6 0 1150.14 1045.21 27.62 o 8 6 0 63.66 61.05 9.85 o 10 6 0 0.90 3.22 9.50 o 12 6 0 7.58 2.31 10.56 o 14 6 0 21.73 11.91 13.09 o 1 7 0 42.05 39.77 5.94 o 3 7 0 168.75 177.64 9.69 o 5 7 0 497.99 486.02 20.01 o 7 7 0 37.54 49.73 11.61 o 9 7 0 0.03 1.60 7.39 o 11 7 0 1.27 4.30 7.57 o 0 8 0 14.20 1.87 7.15 o 2 8 0 9.88 8.12 5.94 o 4 8 0 28.97 36.34 16.89 o 6 8 0 16.43 12.96 8.34 o 8 8 0 261.63 199.22 17.02 o 1 9 0 118.21 130.59 13.58 o 3 9 0 68.10 67.68 11.35 o -19 1 1 43.20 45.44 7.55 o -17 1 1 87.94 92.10 7.40 o -15 1 1 31.07 30.22 4.59 o -13 1 1 316.41 334.39 8.26 o -11 1 1 329.91 358.60 8.72 o -9 1 1 5912.70 6284.61 50.14 o -7 1 1 1260.64 1474.25 15.63 o -5 1 1 1337.91 1295.88 13.20 o -3 1 1 185.66 183.46 4.23 o -1 1 1 4921.71 4472.27 32.30 o 1 1 1 6498.05 6318.32 51.52 o 3 1 1 1.69 10.98 2.68 o 5 1 1 3.28 3.72 1.44 o 7 1 1 703.80 779.61 8.86 o 9 1 1 1.15 0.00 1.85 o 11 1 1 1.17 2.07 2.35 o 13 1 1 589.87 605.18 13.60 o 15 1 1 295.61 302.37 12.92 o 17 1 1 34.61 46.47 15.20 o 19 1 1 68.34 73.20 11.72 o -18 2 1 105.68 102.57 9.67 o -16 2 1 166.39 158.91 10.48 o -14 2 1 39.16 44.15 7.42 o -12 2 1 15.55 20.07 3.86 o -10 2 1 527.00 539.04 11.58 o -8 2 1 409.29 393.30 9.57 o -6 2 1 4714.77 4783.25 33.87 o -4 2 1 2140.72 1965.56 16.10 o -2 2 1 40047.09 38325.79 256.58 o 0 2 1 3689.88 3372.95 51.51 o 2 2 1 23230.92 22441.16 136.00 o 4 2 1 24.51 25.95 3.40 o 6 2 1 157.78 162.84 7.20 o 8 2 1 27.13 30.26 2.19 o 10 2 1 2.24 1.13 2.17 o 12 2 1 4120.06 4037.60 46.61 o 14 2 1 15.18 8.22 5.18 o 16 2 1 1008.99 1028.13 20.04 o 18 2 1 100.42 95.66 12.80 o -19 3 1 0.02 2.81 7.61 o -17 3 1 12.73 13.89 11.34 o -15 3 1 232.82 243.68 12.04 o -13 3 1 170.99 173.79 10.46 o -11 3 1 1634.91 1541.42 19.61 o -9 3 1 1253.53 1207.33 15.94 o -7 3 1 1654.21 1673.73 16.26 o -5 3 1 4180.27 4319.19 32.01 o -3 3 1 68.02 71.70 4.10 o -1 3 1 63.43 87.94 4.21 o 1 3 1 849.20 812.84 13.82 o 3 3 1 4558.44 4516.13 32.51 o 5 3 1 36.79 34.88 2.43 o 7 3 1 146.47 150.68 8.28 o 9 3 1 53.44 43.26 6.06 o 11 3 1 509.01 566.98 24.32 o 13 3 1 54.87 75.70 8.26 o 15 3 1 43.57 47.47 7.60 o 17 3 1 2.86 8.41 5.37 o -18 4 1 44.26 70.83 11.65 o -16 4 1 108.20 125.59 13.43 o -14 4 1 24.47 7.22 5.64 o -12 4 1 35.95 12.96 5.50 o -10 4 1 49.02 58.33 5.31 o -8 4 1 25.51 23.88 3.48 o -6 4 1 327.94 345.72 8.32 o -4 4 1 15957.51 15573.69 125.49 o -2 4 1 1456.06 1341.36 16.52 o 0 4 1 141.12 142.29 7.68 o 2 4 1 168.44 168.67 6.09 o 4 4 1 2755.14 2718.06 28.52 o 6 4 1 529.14 531.70 10.13 o 8 4 1 636.04 644.07 16.32 o 10 4 1 845.90 847.43 19.66 o 12 4 1 5.82 -3.27 5.90 o 14 4 1 224.18 278.32 17.13 o 16 4 1 41.85 37.93 8.18 o -17 5 1 41.79 52.39 10.90 o -15 5 1 392.01 384.86 19.40 o -13 5 1 41.63 20.27 10.77 o -11 5 1 179.42 162.57 10.71 o -9 5 1 770.59 768.67 23.44 o -7 5 1 56.72 51.82 5.13 o -5 5 1 1039.31 1046.55 16.07 o -3 5 1 1015.62 1079.28 16.24 o -1 5 1 160.10 172.02 7.38 o 1 5 1 468.75 492.05 10.84 o 3 5 1 1404.82 1384.63 18.00 o 5 5 1 197.39 216.80 8.40 o 7 5 1 2456.99 2456.65 43.30 o 9 5 1 8.46 11.25 6.26 o 11 5 1 123.46 126.45 12.09 o 13 5 1 12.14 7.09 6.48 o 15 5 1 67.98 62.93 9.48 o -14 6 1 177.80 161.54 15.23 o -12 6 1 102.22 108.92 13.94 o -10 6 1 51.69 44.91 16.47 o -8 6 1 223.40 227.49 15.52 o -6 6 1 986.17 950.65 16.64 o -4 6 1 17.05 19.06 5.16 o -2 6 1 108.64 100.30 7.00 o 0 6 1 134.20 147.81 8.07 o 2 6 1 34.06 26.65 5.00 o 4 6 1 927.98 919.51 18.75 o 6 6 1 1316.71 1251.18 46.87 o 8 6 1 879.92 884.90 26.42 o 10 6 1 489.06 445.21 35.05 o 12 6 1 12.17 17.05 7.16 o 14 6 1 3.40 10.71 8.47 o -13 7 1 16.43 13.30 8.66 o -11 7 1 117.56 100.86 20.06 o -9 7 1 10.78 12.46 9.08 o -7 7 1 38.97 59.78 10.00 o -5 7 1 71.31 71.41 6.90 o -3 7 1 178.85 182.51 9.49 o -1 7 1 65.41 66.79 6.77 o 1 7 1 158.80 167.03 9.14 o 3 7 1 29.14 25.34 8.36 o 5 7 1 237.48 232.20 16.72 o 7 7 1 97.33 91.36 12.88 o 9 7 1 138.05 135.10 14.78 o 11 7 1 11.09 9.02 8.11 o -10 8 1 59.94 76.35 18.79 o -8 8 1 95.07 59.58 10.90 o -6 8 1 0.57 8.37 7.61 o -4 8 1 0.07 0.23 7.09 o -2 8 1 28.37 18.21 5.68 o 0 8 1 0.02 -5.59 4.73 o 2 8 1 0.19 -7.50 12.67 o 4 8 1 64.60 54.66 13.72 o 6 8 1 897.35 836.59 28.21 o 8 8 1 870.35 831.66 51.94 o -3 9 1 14.65 10.79 21.11 o -1 9 1 81.79 65.47 11.47 o 1 9 1 35.53 27.28 9.92 o 3 9 1 77.68 64.46 11.93 o -20 0 2 98.52 58.70 14.78 o -18 0 2 90.86 82.16 9.54 o -16 0 2 9.49 10.06 4.59 o -14 0 2 84.50 67.37 8.45 o -12 0 2 78.23 99.66 12.25 o -10 0 2 1535.37 1706.85 38.85 o -8 0 2 19851.37 21184.48 294.33 o -6 0 2 18284.65 18182.50 251.26 o -4 0 2 2867.42 2629.53 44.76 o -2 0 2 78.98 84.78 4.45 o 0 0 2 23912.33 21361.87 326.06 o 2 0 2 7.83 11.29 2.68 o 4 0 2 11.64 5.07 2.35 o 6 0 2 338.53 377.22 8.12 o 8 0 2 2415.55 2450.06 27.27 o 10 0 2 1468.19 1458.94 20.64 o 12 0 2 828.00 904.67 16.82 o 14 0 2 15822.56 15468.93 249.14 o 16 0 2 1.29 -0.42 8.45 o 18 0 2 162.43 172.71 22.80 o -19 1 2 163.64 169.29 11.82 o -17 1 2 68.09 57.71 5.82 o -15 1 2 337.09 341.06 9.10 o -13 1 2 1930.38 1845.94 25.64 o -11 1 2 1161.27 1191.61 16.32 o -9 1 2 550.59 571.86 13.66 o -7 1 2 5510.75 5766.80 64.16 o -5 1 2 32.01 27.54 3.85 o -3 1 2 204.13 185.78 5.98 o -1 1 2 6670.66 6123.64 62.84 o 1 1 2 6313.55 5682.76 37.60 o 3 1 2 4256.56 4296.92 33.19 o 5 1 2 61.16 38.86 2.10 o 7 1 2 4700.69 4750.14 31.37 o 9 1 2 1302.19 1338.12 13.14 o 11 1 2 67.14 78.07 8.07 o 13 1 2 78.50 92.24 10.84 o 15 1 2 130.45 129.18 9.99 o 17 1 2 46.28 42.07 10.00 o -20 2 2 0.03 -6.95 6.25 o -18 2 2 348.84 385.23 14.51 o -16 2 2 99.40 71.22 9.22 o -14 2 2 241.34 257.45 9.13 o -12 2 2 154.22 153.63 7.12 o -10 2 2 825.55 836.63 16.82 o -8 2 2 398.66 342.92 7.56 o -6 2 2 9137.41 9429.49 61.71 o -4 2 2 240.53 208.34 5.74 o -2 2 2 6990.26 6778.71 50.35 o 0 2 2 508.70 523.19 14.02 o 2 2 2 2.95 4.17 1.32 o 4 2 2 99.37 110.44 6.42 o 6 2 2 99.73 107.90 7.72 o 8 2 2 352.12 375.25 11.19 o 10 2 2 2107.30 2110.11 29.50 o 12 2 2 3226.98 3157.84 35.32 o 14 2 2 34.28 56.59 6.39 o 16 2 2 2092.23 2115.27 30.14 o 18 2 2 218.85 204.55 17.47 o -19 3 2 79.63 99.33 14.36 o -17 3 2 65.13 74.28 25.13 o -15 3 2 85.78 49.61 6.78 o -13 3 2 844.21 864.61 15.29 o -11 3 2 374.65 345.63 9.37 o -9 3 2 303.44 317.74 8.39 o -7 3 2 423.74 431.60 9.58 o -5 3 2 9.04 6.53 2.79 o -3 3 2 2358.21 2246.70 22.12 o -1 3 2 2827.63 2641.48 24.33 o 1 3 2 958.43 1002.20 12.12 o 3 3 2 1.75 2.42 1.77 o 5 3 2 999.00 1112.72 22.60 o 7 3 2 0.00 4.06 3.98 o 9 3 2 1478.83 1520.11 25.24 o 11 3 2 14.75 15.85 7.42 o 13 3 2 5.48 2.14 5.87 o 15 3 2 222.83 229.85 11.68 o 17 3 2 22.94 27.42 6.33 o -18 4 2 174.23 190.95 16.55 o -16 4 2 0.13 -8.59 6.12 o -14 4 2 25.28 29.63 12.25 o -12 4 2 76.98 88.62 8.17 o -10 4 2 0.36 -2.51 3.56 o -8 4 2 204.72 208.63 6.93 o -6 4 2 296.11 309.77 8.68 o -4 4 2 838.00 806.42 12.97 o -2 4 2 512.84 538.81 10.21 o 0 4 2 807.34 848.59 12.58 o 2 4 2 2938.08 2858.52 26.71 o 4 4 2 404.93 433.62 15.94 o 6 4 2 339.93 326.97 12.25 o 8 4 2 414.59 411.53 14.37 o 10 4 2 1644.78 1641.73 28.59 o 12 4 2 83.70 101.16 9.51 o 14 4 2 6.88 17.60 6.90 o 16 4 2 398.54 413.05 16.91 o -17 5 2 147.15 161.70 19.64 o -15 5 2 23.15 21.09 8.47 o -13 5 2 117.03 87.35 19.85 o -11 5 2 77.92 75.80 9.85 o -9 5 2 2.02 3.17 4.10 o -7 5 2 30.91 30.22 4.85 o -5 5 2 397.32 416.44 10.75 o -3 5 2 388.96 362.50 10.02 o -1 5 2 10.47 11.00 3.76 o 1 5 2 1.49 -0.73 3.47 o 3 5 2 696.21 724.60 12.42 o 5 5 2 84.95 110.26 11.17 o 7 5 2 21.88 17.24 8.98 o 9 5 2 44.72 41.03 7.67 o 11 5 2 6.88 5.83 8.14 o 13 5 2 1.57 0.37 6.26 o 15 5 2 23.70 14.37 9.65 o -14 6 2 0.83 -0.42 7.46 o -12 6 2 2.50 2.74 6.97 o -10 6 2 22.37 20.06 7.46 o -8 6 2 44.73 38.68 5.62 o -6 6 2 160.45 132.63 8.00 o -4 6 2 752.12 768.93 16.76 o -2 6 2 111.80 120.58 7.57 o 0 6 2 89.35 88.41 6.73 o 2 6 2 29.15 35.15 5.15 o 4 6 2 2.12 1.69 6.71 o 6 6 2 33.44 31.36 8.47 o 8 6 2 921.55 950.93 32.73 o 10 6 2 114.84 113.97 14.57 o 12 6 2 5.91 5.98 6.77 o -13 7 2 5.58 -2.89 7.61 o -11 7 2 1.53 -1.42 7.45 o -9 7 2 73.59 95.35 11.84 o -7 7 2 4.71 14.99 7.46 o -5 7 2 0.84 -1.69 4.51 o -3 7 2 856.74 903.04 22.19 o -1 7 2 62.64 70.63 6.95 o 1 7 2 24.63 21.92 5.85 o 3 7 2 0.79 3.83 8.02 o 5 7 2 35.84 48.89 10.00 o 7 7 2 227.67 221.17 19.21 o 9 7 2 236.51 196.21 17.17 o 11 7 2 74.40 74.60 12.24 o -10 8 2 1.74 -7.21 7.45 o -8 8 2 110.18 110.55 35.26 o -6 8 2 4.06 4.10 12.67 o -4 8 2 17.67 15.84 5.70 o -2 8 2 47.68 45.94 6.78 o 0 8 2 36.47 28.71 9.56 o 2 8 2 46.93 46.72 10.03 o 4 8 2 217.64 228.65 24.91 o 6 8 2 243.60 269.45 19.38 o 8 8 2 7.09 1.17 8.77 o -3 9 2 8.39 14.86 7.78 o -1 9 2 115.81 82.67 12.67 o 1 9 2 34.24 35.28 10.82 o -19 1 3 733.40 681.76 18.60 o -17 1 3 360.37 298.82 9.05 o -15 1 3 233.90 239.03 9.76 o -13 1 3 221.11 208.96 8.11 o -11 1 3 49.37 54.76 6.79 o -9 1 3 696.26 731.18 46.66 o -7 1 3 87.83 79.17 8.45 o -5 1 3 941.31 914.75 13.73 o -3 1 3 510.67 425.25 10.55 o -1 1 3 45.34 47.09 2.93 o 1 1 3 2333.71 2186.88 23.66 o 3 1 3 915.75 913.94 8.85 o 5 1 3 6582.94 7074.54 44.51 o 7 1 3 105.83 142.66 4.43 o 9 1 3 37.09 42.45 3.90 o 11 1 3 12.81 8.64 4.82 o 13 1 3 452.09 447.45 12.97 o 15 1 3 242.73 252.71 22.38 o 17 1 3 23.10 13.49 8.77 o -20 2 3 69.41 74.38 11.19 o -18 2 3 125.89 111.65 22.38 o -16 2 3 12.33 7.77 5.23 o -14 2 3 0.66 4.45 3.86 o -12 2 3 14.02 18.19 3.87 o -10 2 3 1390.02 1374.06 17.33 o -8 2 3 3013.45 2924.34 30.81 o -6 2 3 170.42 149.92 6.62 o -4 2 3 700.07 568.97 11.13 o -2 2 3 2279.49 2062.93 18.89 o 0 2 3 0.19 -0.60 2.24 o 2 2 3 55.14 56.75 3.38 o 4 2 3 1766.06 1879.59 24.81 o 6 2 3 1401.52 1414.05 21.62 o 8 2 3 67.06 66.30 5.76 o 10 2 3 16.86 14.16 4.91 o 12 2 3 4348.93 4442.47 45.62 o 14 2 3 716.95 732.16 16.85 o 16 2 3 557.20 555.79 54.90 o -19 3 3 2.99 -2.91 7.15 o -17 3 3 335.89 330.41 24.91 o -15 3 3 72.17 42.16 12.88 o -13 3 3 99.45 90.02 6.89 o -11 3 3 844.54 820.31 13.94 o -9 3 3 168.68 169.77 6.15 o -7 3 3 0.63 -0.29 2.78 o -5 3 3 1.19 2.18 2.74 o -3 3 3 22.27 19.48 3.10 o -1 3 3 1384.56 1302.97 15.43 o 1 3 3 619.35 651.38 11.78 o 3 3 3 2286.99 2382.57 19.80 o 5 3 3 1085.91 1037.94 19.15 o 7 3 3 1603.04 1715.64 26.94 o 9 3 3 272.38 282.40 13.61 o 11 3 3 321.69 314.89 16.99 o 13 3 3 7.20 9.79 5.09 o 15 3 3 0.02 -1.13 5.17 o -18 4 3 55.81 40.50 10.00 o -16 4 3 220.06 236.26 17.17 o -14 4 3 62.50 47.70 8.94 o -12 4 3 222.22 237.38 12.33 o -10 4 3 131.39 117.95 7.11 o -8 4 3 280.89 313.63 12.64 o -6 4 3 18.24 24.44 4.06 o -4 4 3 441.60 449.62 10.24 o -2 4 3 400.20 426.35 9.55 o 0 4 3 49.38 53.06 4.18 o 2 4 3 230.21 243.92 6.84 o 4 4 3 1.22 1.91 3.35 o 6 4 3 125.79 130.27 9.80 o 8 4 3 563.46 606.91 17.71 o 10 4 3 3612.18 3596.32 47.41 o 12 4 3 254.54 269.12 17.55 o 14 4 3 10.30 5.59 5.47 o -17 5 3 89.74 98.29 13.29 o -15 5 3 278.72 291.33 21.96 o -13 5 3 275.48 182.67 14.78 o -11 5 3 32.72 31.68 6.28 o -9 5 3 1.37 4.77 4.79 o -7 5 3 10.58 10.67 4.52 o -5 5 3 579.36 566.10 12.45 o -3 5 3 527.23 511.97 11.72 o -1 5 3 1244.21 1300.77 18.19 o 1 5 3 0.60 8.31 4.27 o 3 5 3 101.96 98.61 6.83 o 5 5 3 405.43 444.75 23.65 o 7 5 3 32.83 30.84 7.02 o 9 5 3 879.08 884.71 24.28 o 11 5 3 55.28 29.80 7.79 o 13 5 3 7.85 11.21 7.30 o -14 6 3 135.81 133.70 14.32 o -12 6 3 4.12 4.07 6.97 o -10 6 3 200.28 208.24 15.49 o -8 6 3 241.04 206.96 9.74 o -6 6 3 523.55 525.13 13.34 o -4 6 3 324.08 370.49 11.37 o -2 6 3 45.12 61.14 6.77 o 0 6 3 499.80 534.36 12.68 o 2 6 3 174.33 165.24 14.02 o 4 6 3 11.60 15.66 13.51 o 6 6 3 335.57 316.27 17.72 o 8 6 3 684.76 768.79 66.09 o 10 6 3 19.42 16.18 13.97 o 12 6 3 20.21 2.81 9.29 o -13 7 3 14.13 11.32 8.77 o -11 7 3 104.85 118.23 18.16 o -9 7 3 258.59 282.51 18.48 o -7 7 3 0.07 -0.23 5.67 o -5 7 3 240.37 250.39 10.53 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