#------------------------------------------------------------------------------ #$Date: 2016-10-01 05:05:09 +0300 (Sat, 01 Oct 2016) $ #$Revision: 186861 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/42/1544228.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1544228 _cell_angle_alpha 90.000 _cell_angle_beta 108.041 _cell_angle_gamma 90.000 _cell_length_a 11.0789 _cell_length_b 4.9866 _cell_length_c 15.0495 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.8186 _cod_data_source_file sj4060Isup2.hkl _cod_data_source_block I _shelx_title ' UMD654_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 161.21 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 772.32 710.79 31.69 o 2 0 0 352.48 286.01 13.28 o 3 0 0 735.43 694.54 56.25 o 4 0 0 3502.20 3527.19 149.16 o 5 0 0 2014.63 2169.01 115.36 o 6 0 0 499.39 439.44 28.77 o 7 0 0 1621.61 1572.84 51.83 o 8 0 0 1845.50 1675.70 55.54 o 9 0 0 19.22 16.87 7.55 o 10 0 0 16.83 14.35 5.69 o 11 0 0 63.52 45.30 11.09 o 12 0 0 48.40 42.82 4.53 o 1 1 0 755.18 734.87 13.03 o 2 1 0 4917.39 4528.41 89.66 o 3 1 0 90.62 74.67 2.12 o 4 1 0 591.52 549.10 11.57 o 5 1 0 888.38 783.29 17.38 o 6 1 0 802.48 832.96 33.13 o 7 1 0 332.78 342.09 9.63 o 8 1 0 1189.11 1135.91 25.44 o 9 1 0 2884.30 2765.59 83.06 o 10 1 0 488.54 469.61 15.07 o 11 1 0 111.91 104.57 5.91 o 12 1 0 377.78 351.14 11.75 o 0 2 0 4590.59 4536.72 128.06 o 1 2 0 1712.32 1659.57 39.43 o 2 2 0 424.09 439.57 10.76 o 3 2 0 1903.73 1904.58 36.76 o 4 2 0 1648.87 1655.81 33.27 o 5 2 0 68.37 65.16 5.78 o 6 2 0 300.76 327.03 10.99 o 7 2 0 776.18 750.10 20.62 o 8 2 0 87.24 93.71 5.89 o 9 2 0 32.39 38.00 4.26 o 10 2 0 70.74 72.46 5.30 o 11 2 0 10.10 5.36 3.20 o 12 2 0 36.39 30.57 8.56 o 1 3 0 423.65 457.40 13.44 o 2 3 0 292.11 289.15 10.82 o 3 3 0 133.04 165.61 9.22 o 4 3 0 146.47 163.38 7.93 o 5 3 0 88.38 95.04 5.56 o 6 3 0 483.68 497.63 14.51 o 7 3 0 1395.45 1315.29 36.02 o 8 3 0 7.22 3.56 3.87 o 9 3 0 138.31 139.13 7.11 o 10 3 0 101.20 104.20 8.16 o 11 3 0 223.70 223.08 9.50 o 0 4 0 69.76 70.47 11.09 o 1 4 0 386.11 388.29 15.37 o 2 4 0 1558.13 1779.03 57.75 o 3 4 0 671.82 683.14 24.33 o 4 4 0 31.78 29.20 4.60 o 5 4 0 170.76 197.27 9.04 o 6 4 0 382.12 378.01 13.27 o 7 4 0 101.56 113.92 6.26 o 8 4 0 29.11 29.39 3.69 o 9 4 0 22.83 20.11 4.44 o 1 5 0 198.39 224.27 17.13 o 2 5 0 102.78 99.33 7.92 o 3 5 0 166.97 155.58 11.17 o 4 5 0 14.63 2.05 5.22 o 5 5 0 5.58 -0.56 3.99 o 6 5 0 68.91 39.21 5.51 o 7 5 0 803.87 795.77 26.22 o 0 6 0 22.56 20.37 8.83 o 1 6 0 314.04 229.35 19.47 o 2 6 0 139.06 113.08 10.71 o -12 1 1 268.66 270.21 9.29 o -11 1 1 0.59 -1.24 6.19 o -10 1 1 419.30 409.25 12.15 o -9 1 1 205.08 214.95 8.58 o -8 1 1 723.51 700.24 15.56 o -7 1 1 102.79 118.99 5.22 o -6 1 1 8.50 6.72 3.24 o -5 1 1 16.34 17.47 2.29 o -4 1 1 299.45 297.97 7.10 o -3 1 1 6934.74 6862.79 143.38 o -2 1 1 15187.96 12113.70 379.49 o -1 1 1 195.92 220.38 4.03 o 0 1 1 176.32 167.09 3.41 o 1 1 1 2233.20 2199.15 49.00 o 2 1 1 26.18 35.04 1.11 o 3 1 1 682.53 696.93 13.58 o 4 1 1 728.09 712.31 15.63 o 5 1 1 0.10 -0.48 2.40 o 6 1 1 1552.19 1598.75 34.90 o 7 1 1 96.02 106.04 6.05 o 8 1 1 47.99 51.83 4.49 o 9 1 1 2.92 5.02 4.27 o 10 1 1 14.68 15.74 3.96 o 11 1 1 64.44 42.74 4.68 o 12 1 1 61.68 62.65 4.84 o -12 2 1 48.08 51.09 5.64 o -11 2 1 95.60 91.56 6.51 o -10 2 1 688.08 706.43 16.71 o -9 2 1 515.69 539.82 15.58 o -8 2 1 489.83 468.19 11.78 o -7 2 1 147.71 146.59 6.77 o -6 2 1 0.86 16.34 4.72 o -5 2 1 1792.73 1683.12 49.02 o -4 2 1 972.46 1058.58 24.57 o -3 2 1 1173.71 1151.69 26.40 o -2 2 1 681.46 671.12 14.03 o -1 2 1 7567.37 7608.47 143.75 o 0 2 1 111.37 120.04 3.02 o 1 2 1 813.53 794.99 16.53 o 2 2 1 15.52 13.60 1.83 o 3 2 1 72.88 52.56 3.83 o 4 2 1 129.53 119.55 5.12 o 5 2 1 2159.72 1983.91 40.93 o 6 2 1 54.75 59.47 5.42 o 7 2 1 968.96 964.81 33.69 o 8 2 1 347.97 323.07 11.65 o 9 2 1 363.57 364.52 10.59 o 10 2 1 90.08 87.99 6.29 o 11 2 1 35.91 32.97 6.15 o -11 3 1 0.42 1.18 3.21 o -10 3 1 178.70 184.07 6.99 o -9 3 1 137.34 151.49 7.08 o -8 3 1 245.33 228.86 10.33 o -7 3 1 16.34 17.81 4.00 o -6 3 1 2.43 -1.48 3.46 o -5 3 1 106.24 106.29 7.14 o -4 3 1 706.59 704.40 18.84 o -3 3 1 339.75 341.78 15.93 o -2 3 1 1300.35 1271.68 35.13 o -1 3 1 240.51 286.97 9.43 o 0 3 1 443.85 420.12 12.34 o 1 3 1 929.83 990.59 27.31 o 2 3 1 1041.39 991.30 38.25 o 3 3 1 37.97 49.69 6.32 o 4 3 1 234.30 201.39 9.78 o 5 3 1 64.70 67.02 5.09 o 6 3 1 1377.64 1293.59 35.39 o 7 3 1 411.58 380.12 15.49 o 8 3 1 22.91 22.52 4.14 o 9 3 1 5.14 8.98 3.67 o 10 3 1 428.44 399.38 13.62 o -9 4 1 74.78 73.09 6.06 o -8 4 1 70.95 80.31 5.99 o -7 4 1 16.63 27.51 5.16 o -6 4 1 19.47 20.63 4.26 o -5 4 1 454.90 445.82 16.81 o -4 4 1 57.72 78.68 7.70 o -3 4 1 20.28 21.67 4.90 o -2 4 1 8.65 12.94 3.75 o -1 4 1 413.07 439.74 14.81 o 0 4 1 89.56 106.51 7.29 o 1 4 1 139.56 134.10 8.31 o 2 4 1 4.23 9.49 3.93 o 3 4 1 3.41 5.06 5.40 o 4 4 1 7.07 14.77 4.20 o 5 4 1 29.18 32.46 4.32 o 6 4 1 2.54 2.63 4.17 o 7 4 1 156.60 140.06 7.52 o 8 4 1 39.86 31.55 3.54 o 9 4 1 196.62 195.20 7.88 o -7 5 1 0.06 1.60 3.37 o -6 5 1 28.04 29.69 4.62 o -5 5 1 0.12 3.64 4.20 o -4 5 1 3.00 7.31 4.51 o -3 5 1 3.80 7.35 4.80 o -2 5 1 17.96 24.17 4.96 o -1 5 1 190.59 220.58 14.87 o 0 5 1 14.37 13.46 4.88 o 1 5 1 78.74 110.52 10.75 o 2 5 1 116.24 128.89 9.06 o 3 5 1 20.13 22.04 5.88 o 4 5 1 56.89 45.29 7.10 o 5 5 1 65.87 63.46 7.61 o 6 5 1 0.25 -2.64 3.69 o 7 5 1 19.10 17.53 3.32 o -2 6 1 2.75 0.12 10.30 o -1 6 1 119.62 95.01 10.53 o 0 6 1 210.27 155.98 12.18 o 1 6 1 42.03 34.90 6.65 o -13 0 2 119.77 113.18 8.53 o -12 0 2 1701.57 1682.77 62.63 o -11 0 2 2350.70 2506.69 92.67 o -10 0 2 120.02 123.05 11.66 o -9 0 2 718.87 700.37 26.96 o -8 0 2 938.62 910.35 24.41 o -7 0 2 1723.51 1587.32 46.60 o -6 0 2 26.73 19.93 7.15 o -5 0 2 8.47 25.27 9.05 o -4 0 2 9966.53 8655.44 332.15 o -3 0 2 4223.77 3746.52 166.52 o -2 0 2 3362.86 3052.36 95.73 o -1 0 2 265.40 253.19 9.71 o 0 0 2 1119.26 1137.88 35.82 o 1 0 2 2685.87 2455.39 77.51 o 2 0 2 1413.92 1246.62 45.43 o 3 0 2 1019.45 1032.80 39.81 o 4 0 2 5940.46 6105.90 282.01 o 5 0 2 4.72 3.24 3.48 o 6 0 2 2355.05 2542.81 104.31 o 7 0 2 1532.73 1626.50 61.98 o 8 0 2 30.03 58.29 14.49 o 9 0 2 155.75 136.68 10.70 o 10 0 2 1049.17 1027.88 39.50 o 11 0 2 335.27 322.84 18.16 o 12 0 2 36.28 46.49 6.06 o -13 1 2 81.94 91.31 4.89 o -12 1 2 324.04 319.21 10.38 o -11 1 2 101.68 110.95 8.93 o -10 1 2 405.66 423.01 13.11 o -9 1 2 152.27 163.54 6.81 o -8 1 2 8.90 27.24 5.90 o -7 1 2 947.37 912.93 22.77 o -6 1 2 280.07 276.13 10.53 o -5 1 2 40.78 54.10 3.29 o -4 1 2 3717.43 3658.09 91.17 o -3 1 2 25988.38 22349.90 808.32 o -2 1 2 5782.73 5166.51 107.77 o -1 1 2 27.85 23.56 1.14 o 0 1 2 1720.88 1688.27 33.64 o 1 1 2 6081.31 5914.32 130.96 o 2 1 2 2653.79 2589.60 57.52 o 3 1 2 67.42 75.75 2.30 o 4 1 2 588.68 599.40 15.37 o 5 1 2 5792.50 5828.85 224.71 o 6 1 2 380.65 366.06 11.27 o 7 1 2 629.05 643.24 15.04 o 8 1 2 96.21 95.58 7.17 o 9 1 2 98.17 103.78 9.53 o 10 1 2 302.88 300.71 10.12 o 11 1 2 62.14 59.52 4.33 o 12 1 2 126.82 125.83 6.76 o -12 2 2 355.47 348.01 12.74 o -11 2 2 268.06 254.61 8.73 o -10 2 2 100.16 111.16 6.24 o -9 2 2 664.03 662.71 15.66 o -8 2 2 511.54 481.06 12.84 o -7 2 2 921.71 855.07 20.28 o -6 2 2 1.56 5.39 3.97 o -5 2 2 4239.62 4210.11 109.04 o -4 2 2 328.27 283.11 7.83 o -3 2 2 456.28 427.60 10.46 o -2 2 2 789.59 850.13 20.06 o -1 2 2 46.03 51.94 2.19 o 0 2 2 1364.23 1380.25 26.72 o 1 2 2 1.11 2.54 1.38 o 2 2 2 20.30 39.30 2.83 o 3 2 2 0.21 -1.21 2.52 o 4 2 2 3.37 1.52 3.14 o 5 2 2 63.47 64.91 5.21 o 6 2 2 520.80 505.19 14.56 o 7 2 2 1142.39 1182.09 32.73 o 8 2 2 239.40 242.33 9.21 o 9 2 2 507.19 484.82 15.63 o 10 2 2 298.45 264.05 9.20 o 11 2 2 119.90 120.77 7.77 o -11 3 2 68.82 89.63 9.60 o -10 3 2 33.34 39.57 3.50 o -9 3 2 54.66 60.45 4.82 o -8 3 2 13.20 14.34 4.51 o -7 3 2 49.56 63.54 5.19 o -6 3 2 121.73 127.92 6.19 o -5 3 2 736.70 720.34 18.69 o -4 3 2 794.81 816.09 21.04 o -3 3 2 88.86 85.57 5.27 o -2 3 2 238.12 211.10 6.31 o -1 3 2 583.49 544.60 13.48 o 0 3 2 1170.65 1148.34 34.39 o 1 3 2 806.65 816.71 23.39 o 2 3 2 332.37 336.67 14.73 o 3 3 2 820.73 807.19 27.85 o 4 3 2 1936.31 1927.25 63.63 o 5 3 2 719.14 701.30 20.53 o 6 3 2 6.57 10.59 3.79 o 7 3 2 81.94 80.63 6.02 o 8 3 2 288.94 298.26 14.09 o 9 3 2 109.21 105.57 6.73 o 10 3 2 100.36 88.75 6.28 o -10 4 2 493.39 496.96 18.32 o -9 4 2 274.01 322.43 11.44 o -8 4 2 144.39 121.05 6.73 o -7 4 2 80.09 79.55 5.77 o -6 4 2 663.74 642.21 18.96 o -5 4 2 506.16 454.35 14.01 o -4 4 2 189.24 187.20 9.04 o -3 4 2 155.87 163.67 10.51 o -2 4 2 1110.13 1148.44 34.08 o -1 4 2 89.72 103.11 6.84 o 0 4 2 14.48 14.16 4.30 o 1 4 2 145.29 184.21 9.05 o 2 4 2 135.57 141.41 8.28 o 3 4 2 130.34 145.49 7.32 o 4 4 2 2090.58 2168.47 52.83 o 5 4 2 61.48 60.58 4.93 o 6 4 2 15.96 27.26 5.72 o 7 4 2 66.73 58.54 5.05 o 8 4 2 486.74 449.23 19.78 o 9 4 2 21.46 24.96 4.19 o -7 5 2 27.11 28.20 4.38 o -6 5 2 4.23 -2.99 3.86 o -5 5 2 492.21 399.07 15.12 o -4 5 2 291.51 280.61 12.28 o -3 5 2 463.00 477.06 20.29 o -2 5 2 499.99 503.79 17.99 o -1 5 2 397.02 438.38 28.23 o 0 5 2 481.52 523.04 21.82 o 1 5 2 2.90 2.07 4.44 o 2 5 2 184.13 171.39 13.03 o 3 5 2 606.66 628.97 26.33 o 4 5 2 260.62 259.85 11.30 o 5 5 2 12.85 2.06 3.77 o 6 5 2 100.04 70.60 5.92 o -2 6 2 250.41 212.32 14.10 o -1 6 2 266.67 209.45 32.93 o 0 6 2 108.62 99.59 12.90 o 1 6 2 28.23 21.73 7.47 o -13 1 3 257.27 247.54 8.65 o -12 1 3 0.56 3.81 3.24 o -11 1 3 97.75 112.82 6.45 o -10 1 3 12.04 13.29 3.81 o -9 1 3 4.07 5.03 3.97 o -8 1 3 101.63 110.04 6.70 o -7 1 3 497.14 475.66 12.08 o -6 1 3 377.23 401.76 12.89 o -5 1 3 597.69 583.45 17.59 o -4 1 3 604.26 581.00 13.80 o -3 1 3 502.80 510.07 10.04 o -2 1 3 755.63 775.29 16.72 o -1 1 3 541.04 487.31 11.29 o 0 1 3 872.38 798.96 18.06 o 1 1 3 853.42 856.08 15.69 o 2 1 3 953.48 932.06 19.83 o 3 1 3 1215.34 1335.09 43.29 o 4 1 3 253.25 215.19 7.68 o 5 1 3 40.33 58.24 4.83 o 6 1 3 16.90 26.07 3.68 o 7 1 3 112.37 102.86 9.03 o 8 1 3 6.66 8.29 4.02 o 9 1 3 143.72 138.93 7.72 o 10 1 3 389.52 343.56 10.69 o 11 1 3 115.84 114.79 6.36 o -12 2 3 390.87 400.77 14.85 o -11 2 3 189.01 193.10 7.57 o -10 2 3 17.13 24.04 4.00 o -9 2 3 107.82 125.28 5.60 o -8 2 3 333.13 339.48 11.23 o -7 2 3 86.51 88.80 6.10 o -6 2 3 3894.94 3638.28 95.19 o -5 2 3 791.21 780.17 23.75 o -4 2 3 2286.88 2347.70 73.14 o -3 2 3 118.14 82.11 3.63 o -2 2 3 574.19 528.92 13.47 o -1 2 3 108.29 96.46 3.46 o 0 2 3 110.49 110.27 3.18 o 1 2 3 376.34 341.52 9.95 o 2 2 3 1316.42 1251.14 29.07 o 3 2 3 2911.95 3073.21 87.94 o 4 2 3 361.19 387.50 12.33 o 5 2 3 23.05 37.31 4.10 o 6 2 3 9.80 12.48 4.26 o 7 2 3 152.22 150.93 7.35 o 8 2 3 5.85 0.84 4.02 o 9 2 3 216.32 221.08 8.39 o 10 2 3 12.79 11.22 3.71 o 11 2 3 164.19 162.01 9.49 o -11 3 3 136.40 152.95 8.24 o -10 3 3 14.99 22.61 3.25 o -9 3 3 116.49 138.11 7.63 o -8 3 3 1414.75 1374.70 30.81 o -7 3 3 112.34 126.07 6.21 o -6 3 3 34.80 52.78 4.72 o -5 3 3 694.24 670.81 16.03 o -4 3 3 1421.42 1349.94 32.11 o -3 3 3 80.61 83.21 4.92 o -2 3 3 601.58 597.08 15.71 o -1 3 3 11.17 16.21 4.51 o 0 3 3 215.91 201.76 8.96 o 1 3 3 159.47 160.03 8.54 o 2 3 3 1014.99 967.02 30.09 o 3 3 3 487.30 494.41 22.03 o 4 3 3 579.28 627.95 21.76 o 5 3 3 656.64 613.15 21.48 o 6 3 3 1099.37 1151.87 29.22 o 7 3 3 30.83 34.14 4.19 o 8 3 3 27.30 25.10 4.18 o 9 3 3 48.34 55.01 5.01 o 10 3 3 178.93 178.56 7.90 o -10 4 3 44.03 52.16 4.03 o -9 4 3 17.05 10.22 3.07 o -8 4 3 38.07 47.97 5.95 o -7 4 3 51.18 44.51 4.07 o -6 4 3 91.51 91.86 6.00 o -5 4 3 619.88 551.06 17.16 o -4 4 3 0.46 0.05 3.72 o -3 4 3 50.63 51.74 5.10 o -2 4 3 439.67 502.18 19.28 o -1 4 3 146.30 182.00 8.78 o 0 4 3 59.72 90.23 7.95 o 1 4 3 483.11 546.65 25.66 o 2 4 3 4.33 2.10 4.95 o 3 4 3 1105.23 1092.14 27.97 o 4 4 3 31.25 38.66 4.22 o 5 4 3 93.00 100.26 6.56 o 6 4 3 229.00 265.25 10.44 o 7 4 3 166.12 158.42 9.46 o 8 4 3 148.58 131.67 8.39 o -7 5 3 4.31 8.21 3.45 o -6 5 3 42.29 32.34 4.74 o -5 5 3 26.14 24.80 4.45 o -4 5 3 0.13 6.20 4.12 o -3 5 3 213.35 190.09 9.91 o -2 5 3 0.02 -3.91 3.91 o -1 5 3 60.98 72.19 9.07 o 0 5 3 7.48 10.77 4.46 o 1 5 3 350.95 350.35 25.48 o 2 5 3 118.15 120.98 8.45 o 3 5 3 8.88 6.93 3.90 o 4 5 3 19.05 25.53 4.49 o 5 5 3 0.06 6.77 3.42 o 6 5 3 71.31 68.71 6.11 o -13 0 4 4.33 7.85 4.66 o -12 0 4 260.70 244.54 12.17 o -11 0 4 349.54 377.53 18.85 o -10 0 4 0.60 -1.71 5.78 o -9 0 4 477.67 519.96 16.66 o -8 0 4 234.03 250.65 9.95 o -7 0 4 5183.44 4940.68 127.37 o -5 0 4 882.34 753.58 35.80 o -4 0 4 34.13 43.69 2.93 o -3 0 4 485.45 487.36 13.15 o -2 0 4 6155.02 5783.53 181.14 o -1 0 4 3414.39 3257.10 139.46 o 0 0 4 1223.24 1318.19 44.07 o 1 0 4 1439.60 1602.78 41.20 o 2 0 4 11122.66 10340.05 323.87 o 5 0 4 796.89 862.07 56.13 o 6 0 4 539.71 480.24 20.37 o 7 0 4 2611.75 2600.48 95.91 o 8 0 4 302.18 308.14 13.59 o 9 0 4 1038.29 996.84 33.81 o 10 0 4 348.41 343.88 14.15 o 11 0 4 59.62 59.62 5.67 o -13 1 4 23.71 19.86 2.94 o -12 1 4 117.98 115.35 6.68 o -11 1 4 357.36 377.16 12.36 o -10 1 4 976.59 965.92 20.98 o -9 1 4 74.43 79.67 4.61 o -8 1 4 57.68 58.06 4.62 o -7 1 4 1121.92 1098.34 23.73 o -6 1 4 2884.69 2677.14 82.04 o -5 1 4 1343.66 1368.21 47.44 o -4 1 4 1621.51 1746.16 47.83 o -3 1 4 610.04 526.52 11.08 o -2 1 4 3542.34 3392.65 67.47 o -1 1 4 201.45 242.85 5.61 o 0 1 4 23.53 32.67 1.45 o 1 1 4 6823.22 6693.93 132.41 o 2 1 4 716.71 772.04 16.55 o 3 1 4 18.73 41.44 4.39 o 4 1 4 1136.73 1311.08 48.40 o 5 1 4 951.04 979.70 24.76 o 6 1 4 3.07 5.76 3.51 o 7 1 4 460.53 460.48 14.40 o 8 1 4 385.97 371.54 11.10 o 9 1 4 21.21 18.06 3.59 o 10 1 4 28.95 30.65 4.04 o 11 1 4 354.70 344.13 11.48 o -12 2 4 56.05 71.27 6.00 o -11 2 4 327.32 332.03 9.78 o -10 2 4 9.20 12.16 3.14 o -9 2 4 216.81 248.68 9.19 o -8 2 4 0.53 1.52 3.24 o -7 2 4 826.64 807.27 21.93 o -6 2 4 250.11 243.41 9.82 o -5 2 4 1744.85 1744.61 40.14 o -4 2 4 429.64 537.84 15.40 o -3 2 4 252.16 271.13 8.26 o -2 2 4 912.69 869.58 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