#------------------------------------------------------------------------------ #$Date: 2016-11-09 04:25:35 +0200 (Wed, 09 Nov 2016) $ #$Revision: 188338 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/45/1544525.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1544525 _cell_angle_alpha 90.000 _cell_angle_beta 105.039 _cell_angle_gamma 90.000 _cell_length_a 8.0644 _cell_length_b 6.9410 _cell_length_c 8.6192 _exptl_crystal_F_000 228.00 _reflns_d_resolution_high 0.7354 _cod_data_source_file su4094Isup2.hkl _cod_data_source_block I _shelx_title ' SIR2014 run in space group P 21/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 122.21 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 500.86 501.32 2.94 o 3 0 0 280.43 307.10 2.64 o 4 0 0 1132.32 1276.32 20.60 o 5 0 0 77.70 88.04 3.29 o 6 0 0 1.12 1.22 0.66 o 7 0 0 50.14 43.52 3.27 o 8 0 0 2.71 5.81 1.56 o 9 0 0 25.35 25.43 2.98 o 1 1 0 4876.28 4646.16 24.76 o 2 1 0 466.48 462.11 6.67 o 3 1 0 1454.79 1461.64 10.25 o 4 1 0 174.49 194.55 1.86 o 5 1 0 278.39 262.92 3.00 o 6 1 0 40.91 33.46 1.18 o 7 1 0 25.46 31.09 1.25 o 8 1 0 1.04 0.61 0.51 o 9 1 0 4.37 6.11 1.08 o 0 2 0 14934.68 13419.51 56.45 o 1 2 0 210.28 223.49 0.94 o 2 2 0 0.37 3.13 0.22 o 3 2 0 210.26 222.97 2.16 o 4 2 0 917.19 932.80 8.22 o 5 2 0 30.22 23.64 0.97 o 6 2 0 67.75 68.01 1.96 o 7 2 0 94.53 87.05 2.15 o 8 2 0 69.37 72.36 2.12 o 9 2 0 7.20 8.19 1.06 o 1 3 0 569.68 550.33 2.15 o 2 3 0 803.50 808.59 4.31 o 3 3 0 363.59 387.37 2.41 o 4 3 0 44.22 39.66 0.86 o 5 3 0 400.95 383.73 3.02 o 6 3 0 143.96 135.65 2.65 o 7 3 0 148.86 147.48 2.97 o 8 3 0 0.08 0.32 0.39 o 9 3 0 35.19 36.34 2.07 o 10 3 0 1.39 1.33 0.82 o 0 4 0 4159.97 4192.07 16.19 o 1 4 0 88.83 103.64 0.94 o 2 4 0 44.35 37.90 0.73 o 3 4 0 106.53 110.32 1.24 o 4 4 0 562.05 571.03 2.71 o 5 4 0 0.94 1.09 0.22 o 6 4 0 50.16 49.02 1.51 o 7 4 0 47.36 47.18 1.57 o 8 4 0 43.23 42.62 1.59 o 9 4 0 3.82 0.98 0.85 o 1 5 0 1003.25 1008.94 3.70 o 2 5 0 15.83 17.24 0.85 o 3 5 0 420.28 428.12 4.28 o 4 5 0 54.28 52.77 1.43 o 5 5 0 123.33 127.56 2.63 o 6 5 0 6.73 7.52 0.63 o 7 5 0 18.79 18.22 0.97 o 8 5 0 0.17 0.00 0.49 o 0 6 0 2457.19 2423.68 14.37 o 1 6 0 154.50 157.93 2.49 o 2 6 0 165.18 161.26 2.81 o 3 6 0 3.79 3.27 0.46 o 4 6 0 246.00 251.30 3.71 o 5 6 0 30.51 28.87 1.50 o 6 6 0 1.58 2.96 0.96 o 7 6 0 17.70 20.96 2.69 o 1 7 0 311.59 307.11 3.81 o 2 7 0 9.63 10.71 0.84 o 3 7 0 205.84 202.82 3.52 o 4 7 0 10.90 8.53 0.92 o 5 7 0 53.61 58.14 4.55 o 6 7 0 6.93 11.43 2.32 o 0 8 0 588.57 558.04 8.71 o 1 8 0 48.86 43.96 2.11 o 2 8 0 13.36 14.28 1.56 o 3 8 0 25.06 26.14 2.13 o 4 8 0 111.05 112.90 6.11 o -9 0 1 40.87 39.73 3.59 o -8 0 1 4.23 2.76 0.96 o -7 0 1 183.82 167.86 6.16 o -6 0 1 158.62 176.79 2.49 o -5 0 1 335.27 294.61 3.54 o -4 0 1 604.83 690.39 3.28 o -3 0 1 559.49 559.81 3.26 o 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o -1 2 1 706.27 802.77 2.68 o 0 2 1 731.94 845.55 4.07 o 1 2 1 243.92 229.26 1.33 o 2 2 1 293.79 314.54 1.98 o 3 2 1 59.88 50.00 0.88 o 4 2 1 28.85 31.29 0.82 o 5 2 1 725.38 704.00 6.02 o 6 2 1 68.70 62.15 1.75 o 7 2 1 192.22 189.66 3.20 o 8 2 1 12.65 17.31 1.52 o 9 2 1 26.20 26.57 1.90 o 10 2 1 9.97 18.37 4.65 o -9 3 1 1.30 1.06 0.50 o -8 3 1 359.51 338.48 4.25 o -7 3 1 238.67 220.17 3.20 o -6 3 1 274.01 269.68 3.29 o -5 3 1 44.59 47.79 1.03 o -4 3 1 196.50 226.18 2.05 o -3 3 1 108.63 122.02 1.44 o -2 3 1 3.65 9.17 0.31 o -1 3 1 6.29 9.49 0.27 o 0 3 1 22.52 34.90 0.47 o 1 3 1 669.20 717.01 4.23 o 2 3 1 186.03 177.95 1.61 o 3 3 1 2.13 2.67 0.27 o 4 3 1 315.53 303.07 2.40 o 5 3 1 0.38 0.65 0.25 o 6 3 1 336.82 325.16 4.33 o 7 3 1 44.52 38.63 1.55 o 8 3 1 33.14 32.09 1.87 o 9 3 1 1.06 1.23 1.21 o -9 4 1 104.72 98.21 3.96 o -8 4 1 19.20 17.70 1.04 o -7 4 1 212.55 203.64 3.24 o -6 4 1 1.59 2.12 0.32 o -5 4 1 103.98 99.30 1.48 o -4 4 1 8.30 12.22 0.57 o -3 4 1 6.36 6.16 0.35 o -2 4 1 35.50 37.03 0.77 o -1 4 1 98.23 108.69 1.10 o 0 4 1 267.61 304.31 2.20 o 1 4 1 179.24 188.66 1.75 o 2 4 1 42.75 47.60 1.11 o 3 4 1 100.51 99.25 1.57 o 4 4 1 22.77 19.75 0.61 o 5 4 1 320.20 312.04 2.98 o 6 4 1 27.72 28.41 1.01 o 7 4 1 123.03 122.66 2.53 o 8 4 1 7.88 8.81 0.97 o -8 5 1 137.05 130.85 2.68 o -7 5 1 33.10 32.97 1.28 o -6 5 1 120.56 125.67 2.54 o -5 5 1 13.02 11.41 0.71 o -4 5 1 0.37 0.64 0.27 o -3 5 1 187.49 195.16 2.09 o -2 5 1 282.17 278.46 2.00 o -1 5 1 10.32 8.18 0.38 o 0 5 1 181.95 171.14 1.74 o 1 5 1 0.03 0.38 0.20 o 2 5 1 144.10 148.18 2.16 o 3 5 1 115.38 106.25 1.92 o 4 5 1 42.53 40.39 1.38 o 5 5 1 17.87 16.84 0.82 o 6 5 1 33.71 35.18 1.64 o 7 5 1 36.67 36.46 2.06 o -8 6 1 1.39 -1.70 1.55 o -7 6 1 60.72 64.71 2.35 o -6 6 1 14.05 14.26 1.23 o -5 6 1 79.13 80.94 2.67 o -4 6 1 68.22 65.12 1.73 o -3 6 1 142.77 145.65 3.22 o -2 6 1 7.77 9.23 0.66 o -1 6 1 37.65 38.33 1.05 o 0 6 1 11.64 14.17 0.69 o 1 6 1 213.49 215.40 2.63 o 2 6 1 33.17 30.79 1.10 o 3 6 1 23.08 25.38 1.15 o 4 6 1 43.62 41.77 1.88 o 5 6 1 38.02 40.64 1.70 o 6 6 1 16.21 19.03 1.50 o 7 6 1 27.41 34.48 3.79 o -7 7 1 31.88 40.82 3.93 o -6 7 1 39.13 44.08 3.83 o -5 7 1 0.05 0.23 0.87 o -4 7 1 0.48 0.93 0.47 o -3 7 1 71.48 71.52 2.46 o -2 7 1 92.21 95.08 2.73 o -1 7 1 0.02 0.25 0.30 o 0 7 1 52.11 53.98 1.61 o 1 7 1 4.73 5.19 0.54 o 2 7 1 74.44 77.34 2.63 o 3 7 1 19.33 18.51 1.35 o 4 7 1 25.17 24.81 1.58 o 5 7 1 1.34 0.88 0.55 o -3 8 1 7.66 7.71 1.16 o -2 8 1 7.27 8.54 0.94 o -1 8 1 10.47 7.96 1.43 o 0 8 1 62.19 59.95 2.19 o 1 8 1 43.43 41.00 1.81 o 2 8 1 9.74 11.43 1.16 o 3 8 1 28.40 32.98 1.91 o 4 8 1 1.22 1.17 1.10 o 1 9 1 30.73 28.49 3.10 o 2 9 1 36.71 40.66 3.77 o -10 0 2 112.77 132.55 6.89 o -9 0 2 0.01 -0.14 0.67 o -8 0 2 20.61 20.16 2.38 o -7 0 2 14.81 19.62 2.11 o -6 0 2 824.73 865.97 63.64 o -5 0 2 10.00 12.21 0.81 o -4 0 2 814.16 785.08 6.12 o -3 0 2 82.32 87.28 1.07 o -2 0 2 1796.04 1832.78 6.48 o -1 0 2 340.37 377.86 2.19 o 0 0 2 3451.45 3315.80 26.40 o 1 0 2 287.77 292.83 3.52 o 2 0 2 18.56 22.74 0.56 o 3 0 2 243.75 260.03 3.72 o 4 0 2 177.60 156.49 2.95 o 5 0 2 393.30 387.46 3.52 o 6 0 2 108.27 103.49 4.91 o 7 0 2 38.07 37.23 3.19 o 8 0 2 110.74 119.47 6.22 o -10 1 2 6.48 5.56 1.09 o -9 1 2 3.82 1.86 0.81 o -8 1 2 55.45 48.79 2.51 o -7 1 2 283.20 256.82 4.67 o -6 1 2 92.88 89.43 1.43 o -5 1 2 1084.89 1093.32 12.61 o -4 1 2 25.97 25.65 0.99 o -3 1 2 629.81 572.86 2.34 o -2 1 2 1845.09 1788.70 12.09 o -1 1 2 1799.99 1809.55 10.52 o 0 1 2 173.13 165.43 0.86 o 1 1 2 175.44 155.25 0.88 o 2 1 2 475.14 476.61 4.26 o 3 1 2 1.15 4.45 0.35 o 4 1 2 3.87 3.40 0.34 o 5 1 2 290.63 278.77 3.72 o 6 1 2 219.72 228.37 3.00 o 7 1 2 8.38 10.44 1.25 o 8 1 2 37.91 42.90 3.37 o -10 2 2 198.18 230.74 9.01 o -9 2 2 24.08 23.30 1.52 o -8 2 2 37.44 37.98 1.49 o -7 2 2 180.05 190.05 3.61 o -6 2 2 352.25 344.37 3.53 o -5 2 2 131.40 127.02 1.93 o -4 2 2 17.66 11.60 0.92 o -3 2 2 25.83 26.46 0.71 o -2 2 2 123.43 104.50 0.99 o -1 2 2 158.59 174.48 1.18 o 0 2 2 1370.79 1301.99 8.98 o 1 2 2 264.42 290.69 1.55 o 2 2 2 155.57 146.10 1.10 o 3 2 2 2.39 1.85 0.17 o 4 2 2 809.69 768.41 8.01 o 5 2 2 422.16 422.03 2.92 o 6 2 2 3.05 2.98 0.69 o 7 2 2 0.01 0.17 0.61 o 8 2 2 125.07 130.62 3.83 o 9 2 2 138.22 160.93 10.23 o -10 3 2 15.36 14.50 2.38 o -9 3 2 2.90 6.13 0.77 o -8 3 2 0.50 0.33 0.34 o -7 3 2 226.56 207.42 3.08 o -6 3 2 331.81 307.86 3.13 o -5 3 2 211.23 202.68 2.56 o -4 3 2 11.63 13.81 0.54 o -3 3 2 4.73 5.78 0.38 o -2 3 2 114.62 104.38 1.13 o -1 3 2 207.06 188.55 1.48 o 0 3 2 916.70 981.06 4.37 o 1 3 2 394.44 402.37 3.64 o 2 3 2 6.54 7.45 0.38 o 3 3 2 194.55 185.99 1.61 o 4 3 2 5.43 5.63 0.36 o 5 3 2 685.33 662.60 5.42 o 6 3 2 333.35 323.66 5.28 o 7 3 2 24.62 25.37 1.58 o 8 3 2 100.44 107.86 3.51 o -9 4 2 13.12 12.71 1.05 o -8 4 2 35.85 38.90 1.51 o -7 4 2 82.48 85.82 1.93 o -6 4 2 249.57 241.50 2.89 o -5 4 2 59.55 61.83 1.53 o -4 4 2 49.01 43.22 1.18 o -3 4 2 30.46 26.84 0.90 o -2 4 2 140.80 124.60 1.47 o -1 4 2 21.74 22.80 0.56 o 0 4 2 526.94 546.49 2.44 o 1 4 2 43.40 46.93 0.87 o 2 4 2 118.16 111.87 1.65 o 3 4 2 9.64 7.97 0.44 o 4 4 2 444.31 442.62 3.60 o 5 4 2 305.55 306.27 3.02 o 6 4 2 5.48 5.54 0.70 o 7 4 2 0.04 0.12 0.52 o 8 4 2 85.85 88.53 4.02 o -9 5 2 1.36 0.26 0.44 o -8 5 2 43.35 39.48 1.48 o -7 5 2 200.04 196.71 3.33 o -6 5 2 29.26 29.85 1.40 o -5 5 2 366.61 360.44 4.48 o -4 5 2 3.73 4.58 0.44 o -3 5 2 231.30 229.01 2.78 o -2 5 2 180.30 177.23 2.01 o -1 5 2 351.94 346.67 2.47 o 0 5 2 0.54 0.15 0.12 o 1 5 2 152.66 155.83 1.73 o 2 5 2 110.76 109.06 1.82 o 3 5 2 0.94 1.78 0.30 o 4 5 2 0.34 0.26 0.27 o 5 5 2 169.91 172.61 3.00 o 6 5 2 126.33 122.11 3.57 o 7 5 2 0.76 1.06 0.62 o -8 6 2 13.06 12.70 1.22 o -7 6 2 0.47 1.00 0.44 o -6 6 2 195.47 189.54 3.68 o -5 6 2 3.94 4.63 0.79 o -4 6 2 174.02 172.32 3.86 o -3 6 2 19.02 18.55 1.09 o -2 6 2 270.86 262.64 2.66 o -1 6 2 39.75 38.93 1.10 o 0 6 2 284.85 292.33 2.98 o 1 6 2 48.65 43.74 1.17 o 2 6 2 14.09 12.79 0.88 o 3 6 2 34.20 31.45 1.41 o 4 6 2 84.38 88.17 2.20 o 5 6 2 141.34 138.18 3.19 o 6 6 2 24.36 24.24 1.76 o -6 7 2 13.52 15.83 3.43 o -5 7 2 125.68 123.29 3.61 o -4 7 2 5.49 6.36 0.96 o -3 7 2 87.67 91.13 2.94 o -2 7 2 47.99 47.23 1.55 o -1 7 2 102.69 99.88 2.60 o 0 7 2 0.00 0.05 0.26 o 1 7 2 76.95 81.68 2.26 o 2 7 2 29.09 24.60 1.31 o 3 7 2 5.72 7.01 0.76 o 4 7 2 1.06 1.30 0.54 o 5 7 2 130.60 138.48 5.04 o -4 8 2 6.09 6.29 1.51 o -3 8 2 1.60 2.18 0.79 o -2 8 2 20.45 20.31 1.52 o -1 8 2 3.79 5.05 0.72 o 0 8 2 87.46 92.96 2.73 o 1 8 2 2.14 2.82 0.70 o 2 8 2 48.38 47.80 2.33 o 3 8 2 0.13 0.12 0.38 o 4 8 2 144.51 146.77 6.90 o -1 9 2 13.85 13.91 2.19 o 0 9 2 11.52 11.52 2.15 o 1 9 2 54.55 60.27 4.62 o -10 0 3 40.16 41.81 3.81 o -9 0 3 13.55 13.89 2.07 o -8 0 3 5.92 5.85 1.31 o -7 0 3 285.78 286.51 7.64 o -6 0 3 7.17 9.54 1.45 o -5 0 3 478.53 490.96 21.05 o -4 0 3 368.85 397.52 3.51 o -3 0 3 431.51 426.21 5.11 o -2 0 3 2930.11 3104.59 10.69 o -1 0 3 406.84 387.79 6.18 o 0 0 3 2074.32 2056.48 5.74 o 1 0 3 0.89 1.91 0.22 o 2 0 3 26.71 27.83 0.97 o 3 0 3 49.93 54.34 1.48 o 4 0 3 68.63 60.70 2.19 o 5 0 3 1115.42 1085.96 10.17 o 6 0 3 115.14 105.60 5.14 o 7 0 3 90.92 95.26 5.28 o 8 0 3 1.20 -0.64 0.74 o -10 1 3 22.77 22.04 2.00 o -9 1 3 6.70 5.82 1.00 o -8 1 3 99.51 102.35 3.60 o -7 1 3 38.39 37.85 1.47 o -6 1 3 195.66 190.87 2.96 o -5 1 3 34.85 32.69 0.89 o -4 1 3 113.78 120.98 3.31 o -3 1 3 872.55 893.80 3.82 o -2 1 3 2.23 2.07 0.25 o -1 1 3 820.76 837.91 3.16 o 0 1 3 787.38 763.81 3.53 o 1 1 3 207.73 251.57 1.23 o 2 1 3 891.74 963.34 5.58 o 3 1 3 513.71 518.08 2.79 o 4 1 3 291.03 301.34 2.85 o 5 1 3 345.24 331.61 3.65 o 6 1 3 543.75 531.66 5.93 o 7 1 3 0.00 0.36 0.53 o 8 1 3 55.84 58.09 3.18 o -10 2 3 1.77 2.83 0.84 o -9 2 3 11.96 12.70 1.15 o -8 2 3 91.05 88.48 2.57 o -7 2 3 60.68 57.25 1.71 o -6 2 3 6.09 6.56 0.58 o -5 2 3 14.31 15.41 0.53 o -4 2 3 61.61 59.41 1.14 o -3 2 3 0.33 0.07 0.16 o -2 2 3 383.80 398.84 2.10 o -1 2 3 361.99 323.56 2.03 o 0 2 3 47.05 32.07 0.49 o 1 2 3 415.92 418.97 1.99 o 2 2 3 88.49 103.39 1.01 o 3 2 3 703.80 722.99 3.73 o 4 2 3 0.80 0.87 0.26 o 5 2 3 1341.93 1289.94 8.46 o 6 2 3 2.93 1.74 0.57 o 7 2 3 75.62 77.12 2.84 o 8 2 3 6.68 8.59 1.18 o -10 3 3 37.81 35.17 2.44 o -9 3 3 61.01 57.53 1.88 o -8 3 3 39.60 40.78 1.32 o -7 3 3 139.99 136.19 2.24 o -6 3 3 1.14 1.31 0.29 o -5 3 3 28.21 26.83 0.80 o -4 3 3 30.05 31.30 0.74 o -3 3 3 19.75 20.31 0.56 o -2 3 3 1.29 2.21 0.22 o -1 3 3 0.63 1.80 0.18 o 0 3 3 978.20 927.57 3.49 o 1 3 3 359.15 413.67 2.18 o 2 3 3 1547.70 1559.26 10.10 o 3 3 3 318.96 324.02 3.49 o 4 3 3 537.76 522.71 4.64 o 5 3 3 66.65 67.69 1.82 o 6 3 3 516.33 492.14 5.88 o 7 3 3 27.78 28.15 1.74 o 8 3 3 19.97 22.11 2.69 o -9 4 3 17.17 17.13 1.24 o -8 4 3 52.87 52.99 1.61 o -7 4 3 56.48 53.49 1.37 o -6 4 3 10.44 10.53 1.19 o -5 4 3 40.51 39.55 1.11 o -4 4 3 58.13 55.74 1.35 o -3 4 3 12.96 12.93 0.68 o -2 4 3 255.11 239.02 2.15 o -1 4 3 168.99 152.85 1.50 o 0 4 3 13.03 10.22 0.37 o 1 4 3 217.85 232.81 3.07 o 2 4 3 15.24 21.98 0.63 o 3 4 3 418.81 421.59 3.32 o 4 4 3 1.24 1.72 0.41 o 5 4 3 749.92 740.73 6.24 o 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20.36 1.94 o 0 3 8 65.82 64.62 2.10 o 1 3 8 0.01 -0.49 0.68 o 2 3 8 100.57 93.65 3.28 o 3 3 8 9.82 12.45 1.37 o 4 3 8 3.95 7.25 2.90 o -7 4 8 29.53 31.19 2.37 o -6 4 8 32.11 31.98 1.62 o -5 4 8 158.18 161.73 3.14 o -4 4 8 4.54 4.59 0.57 o -3 4 8 84.18 85.60 2.18 o -2 4 8 0.02 0.09 0.32 o -1 4 8 52.77 54.73 1.88 o 0 4 8 0.47 0.85 0.50 o 1 4 8 16.15 15.45 1.32 o 2 4 8 27.14 29.77 1.86 o 3 4 8 55.73 59.12 2.67 o -7 5 8 4.63 3.33 1.27 o -6 5 8 15.60 15.08 1.32 o -5 5 8 15.77 12.69 1.07 o -4 5 8 9.52 10.76 0.86 o -3 5 8 15.51 15.65 1.15 o -2 5 8 66.37 69.15 2.35 o -1 5 8 1.91 1.96 0.55 o 0 5 8 0.50 1.02 0.49 o 1 5 8 36.90 37.40 2.09 o 2 5 8 53.77 60.58 4.63 o -5 6 8 57.31 51.84 4.27 o -4 6 8 31.20 29.03 2.31 o -3 6 8 2.59 2.90 0.85 o -2 6 8 0.13 0.00 0.60 o -1 6 8 0.15 1.02 1.21 o 1 6 8 4.06 6.76 1.70 o -8 0 9 27.29 22.83 2.88 o -7 0 9 64.01 63.90 3.28 o -6 0 9 11.07 12.60 1.48 o -5 0 9 0.98 1.41 0.64 o -4 0 9 21.76 20.80 1.71 o -3 0 9 245.62 240.13 6.02 o -2 0 9 5.77 5.50 0.87 o -1 0 9 90.90 92.75 3.20 o 0 0 9 31.07 33.82 3.10 o 1 0 9 120.07 120.47 5.92 o 2 0 9 237.55 263.30 9.01 o 3 0 9 18.08 18.19 2.43 o 4 0 9 64.48 69.13 4.91 o -8 1 9 28.70 25.15 2.94 o -7 1 9 37.68 35.27 1.75 o -6 1 9 98.34 92.56 2.66 o -5 1 9 85.11 86.50 2.47 o -4 1 9 16.06 14.88 1.02 o -3 1 9 96.13 94.10 3.52 o -2 1 9 121.18 116.27 3.18 o -1 1 9 1.29 0.74 0.43 o 0 1 9 27.44 27.66 1.57 o 1 1 9 149.05 156.67 3.70 o 2 1 9 51.15 51.33 2.82 o 3 1 9 12.90 13.35 1.51 o -8 2 9 12.76 8.51 1.80 o -7 2 9 220.68 227.55 4.39 o -6 2 9 71.97 69.04 2.78 o -5 2 9 33.16 29.09 1.77 o -4 2 9 184.75 184.45 4.27 o -3 2 9 146.76 142.88 3.66 o -2 2 9 95.78 100.51 3.02 o -1 2 9 3.23 3.02 0.64 o 0 2 9 43.98 42.46 1.99 o 1 2 9 14.20 17.41 1.13 o 2 2 9 120.43 134.82 4.47 o 3 2 9 2.42 0.06 1.17 o -6 3 9 217.34 211.67 4.95 o -5 3 9 234.84 227.97 4.23 o -4 3 9 23.82 25.06 1.41 o -3 3 9 282.81 281.88 5.56 o -2 3 9 15.91 15.07 1.24 o -1 3 9 10.38 9.70 1.01 o 0 3 9 3.17 3.25 0.84 o 1 3 9 69.37 67.08 3.35 o 2 3 9 6.82 9.95 2.22 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1.98 o -3 2 10 381.80 405.00 6.55 o -2 2 10 1.41 1.84 0.58 o -1 2 10 48.80 50.23 2.28 o 0 2 10 0.19 0.47 0.64 o -5 3 10 5.98 6.50 1.14 o -4 3 10 240.84 244.01 6.38 o -3 3 10 8.82 9.53 1.32 o -2 3 10 153.42 154.15 4.88 o -1 3 10 13.00 12.52 2.04 o 0 3 10 17.67 14.83 2.28 o 1 3 10 1.85 1.53 0.98 o -5 4 10 136.55 136.15 4.85 o -4 4 10 25.91 24.12 1.69 o -3 4 10 244.65 231.43 8.59 o -5 1 11 115.72 115.83 6.17 o -3 1 11 3.32 2.19 1.12 o -2 1 11 61.70 63.62 4.85 o -1 1 11 103.69 109.03 6.24 o 0 1 11 4.00 4.09 1.50 o -4 2 11 3.33 2.47 1.19 o -3 2 11 131.76 142.28 4.91 o -2 2 11 37.99 38.99 3.72 o -1 2 11 3.64 3.40 1.41 o -3 3 11 1.66 0.48 0.98 o