#------------------------------------------------------------------------------ #$Date: 2016-11-23 04:10:52 +0200 (Wed, 23 Nov 2016) $ #$Revision: 188631 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/46/1544650.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1544650 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.3620 _cell_length_b 17.7187 _cell_length_c 22.1796 _exptl_crystal_F_000 1560.00 _reflns_d_resolution_high 0.6984 _cod_data_source_file wm4029Isup2.hkl _cod_data_source_block I _shelx_title ' DAM008 OLEX2: imported from CIF' _shelx_refln_list_code 4 _shelx_f_calc_maximum 287.17 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1371.50 1308.50 15.94 o 4 0 0 2083.05 2133.01 30.01 o 6 0 0 5554.33 5294.06 57.22 o 8 0 0 1229.82 1145.30 31.89 o 10 0 0 3.80 10.32 35.64 o 12 0 0 218.45 395.83 92.86 o 1 1 0 2652.28 2670.49 22.51 o 2 1 0 17411.19 18343.48 116.31 o 3 1 0 254.17 249.51 6.57 o 4 1 0 10747.71 10715.70 74.11 o 5 1 0 1.58 16.89 6.57 o 6 1 0 2692.36 2625.46 25.33 o 7 1 0 56.40 65.66 10.32 o 8 1 0 912.33 876.09 20.64 o 9 1 0 4.05 -16.89 16.89 o 10 1 0 2622.19 2615.14 51.59 o 11 1 0 28.09 -3.75 44.08 o 12 1 0 422.39 415.54 66.60 o 13 1 0 7.47 -48.78 191.35 o 0 2 0 76359.38 81981.09 781.36 o 1 2 0 64.62 85.36 3.75 o 2 2 0 1677.32 1696.84 15.94 o 3 2 0 1567.42 1736.23 16.89 o 4 2 0 1140.55 1180.01 15.94 o 5 2 0 6972.11 7428.95 59.09 o 6 2 0 7992.98 7742.24 61.91 o 7 2 0 908.82 817.00 18.76 o 8 2 0 1500.53 1549.57 30.01 o 9 2 0 167.44 153.83 19.69 o 10 2 0 0.01 30.96 25.33 o 11 2 0 52.52 52.53 44.08 o 12 2 0 273.85 402.40 78.79 o 13 2 0 1.34 78.79 164.15 o 1 3 0 17957.00 19072.29 106.93 o 2 3 0 28026.12 29432.54 194.17 o 3 3 0 5014.36 4940.44 38.46 o 4 3 0 17611.22 18358.51 118.19 o 5 3 0 224.01 225.12 9.38 o 6 3 0 824.86 796.36 18.76 o 7 3 0 198.96 182.91 14.07 o 8 3 0 763.46 737.26 21.57 o 9 3 0 157.20 149.15 19.69 o 10 3 0 1568.28 1555.20 43.15 o 11 3 0 63.31 62.84 40.33 o 12 3 0 47.12 -58.15 73.16 o 13 3 0 24.62 -127.57 127.57 o 0 4 0 2318.90 2251.20 23.45 o 1 4 0 13532.95 14660.89 84.42 o 2 4 0 18391.02 19091.10 117.25 o 3 4 0 24.05 26.26 5.63 o 4 4 0 219.29 248.57 9.38 o 5 4 0 347.28 387.39 12.19 o 6 4 0 8939.23 9228.03 67.54 o 7 4 0 1224.80 1141.55 24.39 o 8 4 0 1261.60 1188.44 30.01 o 9 4 0 448.91 458.68 25.33 o 10 4 0 32.63 45.96 27.21 o 11 4 0 1.30 -40.33 40.33 o 12 4 0 215.54 272.02 69.41 o 13 4 0 37.82 78.79 138.83 o 1 5 0 2200.64 2186.48 16.89 o 2 5 0 3855.13 3635.68 29.08 o 3 5 0 5264.42 5464.78 43.15 o 4 5 0 27968.07 29856.46 206.37 o 5 5 0 698.58 605.95 16.89 o 6 5 0 173.29 178.22 13.14 o 7 5 0 8.65 -12.19 12.19 o 8 5 0 2367.06 2372.20 41.27 o 9 5 0 790.81 732.58 30.96 o 10 5 0 1635.95 1667.76 49.72 o 11 5 0 46.13 -43.15 43.15 o 12 5 0 15.49 88.18 74.11 o 13 5 0 3.45 484.01 146.33 o 0 6 0 2106.71 2281.21 29.08 o 1 6 0 4846.25 4940.44 34.71 o 2 6 0 7774.75 8261.90 55.34 o 3 6 0 75.47 89.11 6.57 o 4 6 0 316.03 323.61 11.25 o 5 6 0 1679.91 1649.94 26.26 o 6 6 0 4903.56 4786.61 46.90 o 7 6 0 108.92 99.43 15.01 o 8 6 0 2513.05 2550.42 45.96 o 9 6 0 311.07 330.18 29.08 o 10 6 0 81.41 67.54 34.71 o 11 6 0 38.30 47.83 46.90 o 12 6 0 238.35 210.12 78.79 o 13 6 0 24.40 -116.31 181.03 o 1 7 0 4632.80 4608.38 34.71 o 2 7 0 5772.96 5319.39 41.27 o 3 7 0 4821.78 4843.83 37.52 o 4 7 0 13620.58 13757.64 96.61 o 5 7 0 835.87 741.96 19.69 o 6 7 0 319.70 287.03 18.76 o 7 7 0 110.45 102.25 16.89 o 8 7 0 2125.33 2073.92 37.52 o 9 7 0 114.10 91.93 24.39 o 10 7 0 742.31 673.48 44.08 o 11 7 0 227.72 285.15 48.78 o 12 7 0 55.07 -75.04 78.79 o 0 8 0 1737.88 1613.35 27.21 o 1 8 0 2762.07 2748.33 24.39 o 2 8 0 179.15 161.34 8.44 o 3 8 0 1111.37 1112.47 16.89 o 4 8 0 5.29 2.82 8.44 o 5 8 0 5474.14 5298.76 44.08 o 6 8 0 5521.55 5293.13 57.22 o 7 8 0 1651.25 1731.54 36.58 o 8 8 0 1167.35 1150.92 34.71 o 9 8 0 0.19 19.69 29.08 o 10 8 0 51.60 39.40 38.46 o 11 8 0 79.43 90.98 47.83 o 12 8 0 305.41 332.05 98.49 o 1 9 0 45.26 50.65 6.57 o 2 9 0 7303.50 7485.23 55.34 o 3 9 0 1209.92 1259.73 19.69 o 4 9 0 7559.27 7386.74 60.97 o 5 9 0 2854.41 2822.44 31.89 o 6 9 0 1727.84 1721.22 33.76 o 7 9 0 0.07 3.75 17.82 o 8 9 0 151.05 133.19 21.57 o 9 9 0 218.71 199.80 30.96 o 10 9 0 413.42 419.29 45.96 o 11 9 0 310.43 327.36 51.59 o 12 9 0 60.91 135.08 97.55 o 0 10 0 9947.40 9939.97 100.37 o 1 10 0 9193.03 9416.57 69.41 o 2 10 0 851.71 782.29 16.89 o 3 10 0 1790.35 1849.73 24.39 o 4 10 0 2134.94 2131.13 29.08 o 5 10 0 2973.03 3139.48 37.52 o 6 10 0 4438.90 4422.67 60.03 o 7 10 0 1748.88 1712.79 45.03 o 8 10 0 1198.79 1160.30 39.40 o 9 10 0 0.37 -15.94 34.71 o 10 10 0 14.44 -15.94 42.21 o 11 10 0 35.82 72.22 57.22 o 12 10 0 260.74 330.18 100.37 o 1 11 0 86.43 100.37 9.38 o 2 11 0 1210.28 1170.62 21.57 o 3 11 0 2240.68 2268.08 29.08 o 4 11 0 1677.17 1680.89 29.08 o 5 11 0 2287.63 2295.28 38.46 o 6 11 0 16.08 15.94 17.82 o 7 11 0 2.40 -22.51 22.51 o 8 11 0 1.03 -0.94 28.14 o 9 11 0 305.40 254.20 38.46 o 10 11 0 638.61 536.53 50.65 o 11 11 0 264.51 417.41 63.79 o 12 11 0 195.43 253.26 107.87 o 0 12 0 10278.66 10252.28 106.93 o 1 12 0 4974.90 4878.53 44.08 o 2 12 0 1735.76 1646.18 26.26 o 3 12 0 1066.35 996.15 22.51 o 4 12 0 1713.26 1668.70 30.96 o 5 12 0 58.60 79.73 16.89 o 6 12 0 1165.41 1252.23 35.64 o 7 12 0 1211.80 1265.36 44.08 o 8 12 0 749.99 707.25 46.90 o 9 12 0 66.18 19.69 41.27 o 10 12 0 54.79 35.64 49.72 o 11 12 0 95.15 135.08 63.79 o 1 13 0 629.66 651.90 17.82 o 2 13 0 1042.77 962.39 23.45 o 3 13 0 6378.55 6527.54 60.97 o 4 13 0 1442.36 1393.86 31.89 o 5 13 0 311.95 320.79 22.51 o 6 13 0 743.04 743.83 30.01 o 7 13 0 318.11 327.36 30.96 o 8 13 0 173.07 221.37 41.27 o 9 13 0 450.72 526.21 49.72 o 10 13 0 269.25 312.35 60.03 o 11 13 0 163.43 180.09 73.16 o 0 14 0 911.30 901.42 33.76 o 1 14 0 1144.62 1097.46 25.33 o 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200.01 128.51 27.21 o 5 17 0 548.57 547.79 37.52 o 6 17 0 0.04 -15.01 35.64 o 7 17 0 105.16 77.86 50.65 o 8 17 0 386.86 523.41 62.84 o 9 17 0 246.46 312.35 75.98 o 0 18 0 589.33 623.77 42.21 o 1 18 0 1715.86 1848.80 46.90 o 2 18 0 225.18 238.25 27.21 o 3 18 0 32.55 -2.82 25.33 o 4 18 0 0.32 -1.88 30.01 o 5 18 0 894.61 831.06 46.90 o 6 18 0 11.58 18.76 42.21 o 7 18 0 675.94 624.71 62.84 o 8 18 0 11.61 12.19 60.97 o 9 18 0 62.43 142.58 79.73 o 1 19 0 544.96 525.28 33.76 o 2 19 0 237.58 214.80 29.08 o 3 19 0 1046.48 1020.54 41.27 o 4 19 0 213.02 222.31 35.64 o 5 19 0 727.10 800.11 51.59 o 6 19 0 2.23 -4.69 54.40 o 7 19 0 3.19 -60.03 60.03 o 8 19 0 113.18 23.45 75.98 o 0 20 0 174.82 223.24 49.72 o 1 20 0 1579.77 1576.77 51.59 o 2 20 0 14.60 -23.45 30.01 o 3 20 0 6.92 18.76 34.71 o 4 20 0 4.34 27.21 37.52 o 5 20 0 973.08 1001.78 57.22 o 6 20 0 1.49 3.75 60.03 o 7 20 0 762.50 630.33 75.04 o 8 20 0 3.54 -47.83 94.73 o 1 21 0 226.24 240.13 35.64 o 2 21 0 6.66 -21.57 34.71 o 3 21 0 418.32 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1 2915.84 2957.51 19.69 o 2 3 1 23334.94 24382.38 152.90 o 3 3 1 16302.40 16530.40 121.94 o 4 3 1 2025.15 2046.71 22.51 o 5 3 1 5219.49 5194.64 42.21 o 6 3 1 129.44 134.13 12.19 o 7 3 1 95.00 88.18 13.14 o 8 3 1 974.56 1001.78 24.39 o 9 3 1 2145.77 2075.79 37.52 o 10 3 1 100.11 106.93 26.26 o 11 3 1 658.74 708.19 48.78 o 12 3 1 65.17 200.73 79.73 o 13 3 1 0.05 60.03 136.95 o -13 4 1 406.02 727.89 146.33 o -12 4 1 35.88 63.79 72.22 o -11 4 1 62.62 31.89 40.33 o -10 4 1 112.42 106.93 29.08 o -9 4 1 692.35 715.69 29.08 o -8 4 1 804.36 823.56 26.26 o -7 4 1 4336.96 4216.30 47.83 o -6 4 1 279.80 266.39 12.19 o -5 4 1 4907.93 4914.17 41.27 o -4 4 1 845.43 894.85 16.89 o -3 4 1 54.49 50.65 5.63 o -2 4 1 1169.03 1080.58 12.19 o -1 4 1 37291.39 39368.77 238.25 o 0 4 1 29903.18 32431.29 191.35 o 1 4 1 36753.95 38788.12 221.37 o 2 4 1 1016.18 906.10 15.01 o 3 4 1 49.24 54.40 6.57 o 4 4 1 836.39 853.58 15.94 o 5 4 1 5061.43 5111.15 44.08 o 6 4 1 275.58 287.96 15.01 o 7 4 1 4724.36 4547.41 47.83 o 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