Crystallography Open Database

Information card for entry 1544710

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Structure parameters

Chemical name	Poly[di-μ~2~-acetato-κ^4^<i>O</i>:<i>O</i>'-μ~3~-thiourea-κ^3^<i>S</i>:<i>S</i>:<i>S</i>-lead(II)]
Formula	C5 H10 N2 O4 Pb S
Calculated formula	C5 H10 N2 O4 Pb S
Title of publication	Poly[di-μ~2~-acetato-κ^4^<i>O</i>:<i>O</i>'-μ~3~-thiourea-κ^3^<i>S</i>:<i>S</i>:<i>S</i>-lead(II)]: a redetermination
Authors of publication	Zouihri, Hafid; Ait Mouha, Mbark; Ba Mohamed, Bouchra; Yamni, Khalid; Tijani, Najib
Journal of publication	IUCrData
Year of publication	2016
Journal volume	1
Journal issue	12
Pages of publication	x161892
a	4.4865 ± 0.0002 Å
b	15.7001 ± 0.0005 Å
c	13.6313 ± 0.0005 Å
α	90°
β	91.481 ± 0.002°
γ	90°
Cell volume	959.85 ± 0.06 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0162
Residual factor for significantly intense reflections	0.0153
Weighted residual factors for significantly intense reflections	0.0368
Weighted residual factors for all reflections included in the refinement	0.0371
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

Version history

Revision	Date	Message	Files
189976 (current)	2017-01-06	cif/ Updating files of 1544710 Original log message: Adding full bibliography for 1544710.cif.	1544710.cif 1544710.hkl
188863	2016-12-03	cif/ hkl/ Adding structures of 1544710 via cif-deposit CGI script.	1544710.cif 1544710.hkl