#------------------------------------------------------------------------------ #$Date: 2017-01-11 04:26:44 +0200 (Wed, 11 Jan 2017) $ #$Revision: 190360 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/50/1545021.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1545021 _cell_angle_alpha 90.000 _cell_angle_beta 99.414 _cell_angle_gamma 90.000 _cell_length_a 8.3510 _cell_length_b 27.1560 _cell_length_c 8.5450 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.7688 _cod_data_source_file pk4010Isup2.hkl _cod_data_source_block I _shelx_title ' x599e' _shelx_refln_list_code 4 _shelx_f_calc_maximum 215.43 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2683.16 2771.63 72.88 o 4 0 0 2285.14 2377.01 138.89 o 6 0 0 13.62 35.31 7.68 o 8 0 0 599.90 588.79 58.67 o 10 0 0 878.69 881.16 92.82 o 1 1 0 301.78 329.68 11.46 o 2 1 0 7607.45 7284.86 78.71 o 3 1 0 7349.82 7439.66 112.85 o 4 1 0 2714.91 2752.07 45.13 o 5 1 0 627.35 574.90 23.28 o 6 1 0 4751.73 4901.74 91.33 o 7 1 0 610.11 572.80 29.81 o 8 1 0 1367.14 1528.12 66.12 o 9 1 0 44.85 46.01 11.71 o 10 1 0 217.98 167.19 28.33 o 1 2 0 22809.82 22805.53 246.60 o 2 2 0 2709.38 2834.54 40.18 o 3 2 0 706.45 698.16 15.63 o 4 2 0 2591.30 2491.54 46.88 o 5 2 0 6456.54 6298.85 140.29 o 6 2 0 84.95 89.32 11.94 o 7 2 0 67.09 76.81 13.14 o 8 2 0 3.10 15.98 6.10 o 9 2 0 2462.55 2804.49 116.18 o 10 2 0 80.59 58.17 29.80 o 1 3 0 3193.26 3136.43 43.91 o 2 3 0 27017.12 27740.03 273.89 o 3 3 0 18426.09 18565.80 182.86 o 4 3 0 1629.43 1490.64 47.51 o 5 3 0 394.34 392.22 20.71 o 6 3 0 2041.59 2017.42 42.35 o 7 3 0 22.23 30.10 6.57 o 8 3 0 1343.10 1388.85 59.92 o 9 3 0 88.37 82.40 17.07 o 10 3 0 25.73 19.54 22.50 o 0 4 0 26093.96 25188.36 424.87 o 1 4 0 132.14 102.43 5.33 o 2 4 0 6193.82 6020.17 70.53 o 3 4 0 878.82 989.91 23.05 o 4 4 0 9508.69 9110.88 133.09 o 5 4 0 870.83 929.63 30.29 o 6 4 0 4.90 7.63 3.31 o 7 4 0 993.48 1027.05 47.72 o 8 4 0 81.35 87.47 10.63 o 9 4 0 377.55 357.76 36.43 o 10 4 0 562.82 599.01 46.37 o 1 5 0 925.20 903.02 13.89 o 2 5 0 10477.98 10580.79 90.79 o 3 5 0 197.72 204.81 11.46 o 4 5 0 7078.78 7200.78 106.13 o 5 5 0 353.91 372.42 17.52 o 6 5 0 1119.60 1173.64 44.68 o 7 5 0 484.11 517.03 38.63 o 8 5 0 1920.00 2059.62 66.62 o 9 5 0 11.33 25.94 7.56 o 10 5 0 548.92 589.51 45.83 o 0 6 0 6822.67 7457.78 98.09 o 1 6 0 171.31 192.58 10.97 o 2 6 0 46.92 64.16 7.74 o 3 6 0 159.64 162.71 10.89 o 4 6 0 6115.04 6336.42 103.21 o 5 6 0 11534.94 11646.07 313.69 o 6 6 0 200.97 209.54 14.46 o 7 6 0 722.99 854.75 53.15 o 8 6 0 236.31 228.57 28.84 o 9 6 0 1357.24 1498.44 60.62 o 10 6 0 137.75 131.54 24.52 o 1 7 0 3378.33 3138.99 47.76 o 2 7 0 106.51 77.37 7.34 o 3 7 0 57.74 103.15 8.37 o 4 7 0 415.57 395.00 28.89 o 5 7 0 877.92 806.29 31.95 o 6 7 0 1412.59 1334.70 56.70 o 7 7 0 1063.15 1183.29 54.17 o 8 7 0 211.63 235.51 27.30 o 9 7 0 242.57 261.98 23.48 o 10 7 0 37.40 31.82 8.18 o 0 8 0 30007.32 30176.08 389.49 o 1 8 0 2896.56 3075.15 47.05 o 2 8 0 5280.23 5219.58 49.56 o 3 8 0 585.77 592.90 20.21 o 4 8 0 11293.00 11692.56 257.73 o 5 8 0 6242.25 6500.51 134.98 o 6 8 0 41.15 47.00 7.72 o 7 8 0 171.18 185.70 16.61 o 8 8 0 760.05 999.41 92.53 o 9 8 0 189.66 221.87 23.30 o 10 8 0 440.66 413.12 38.89 o 1 9 0 937.96 1019.29 17.42 o 2 9 0 3930.22 4109.80 67.12 o 3 9 0 1306.43 1322.31 42.99 o 4 9 0 3729.41 3477.42 87.02 o 5 9 0 1.76 15.72 4.05 o 6 9 0 1280.17 1229.76 50.07 o 7 9 0 192.35 195.76 18.70 o 8 9 0 5475.67 5879.31 329.36 o 9 9 0 0.37 4.66 7.75 o 10 9 0 405.36 401.95 36.27 o 0 10 0 219.38 376.48 26.80 o 1 10 0 973.78 936.02 19.21 o 2 10 0 835.96 739.92 19.72 o 3 10 0 1115.95 1292.32 44.54 o 4 10 0 3295.40 3410.89 77.96 o 5 10 0 2617.19 2529.71 54.71 o 6 10 0 33.46 32.92 6.23 o 7 10 0 45.63 55.06 13.13 o 8 10 0 167.77 148.39 28.67 o 9 10 0 2440.39 2704.20 128.40 o 10 10 0 101.46 89.99 21.11 o 1 11 0 4945.33 5049.68 48.85 o 2 11 0 2750.03 3070.10 47.66 o 3 11 0 6176.20 6061.12 89.17 o 4 11 0 770.78 830.59 34.63 o 5 11 0 948.59 1035.05 39.91 o 6 11 0 152.02 164.24 13.85 o 7 11 0 11.01 11.72 7.34 o 8 11 0 79.76 70.89 16.37 o 9 11 0 488.40 464.02 35.25 o 10 11 0 67.68 55.77 26.49 o 0 12 0 31827.02 33374.71 738.90 o 1 12 0 317.34 236.42 18.09 o 2 12 0 1261.76 1276.41 43.00 o 3 12 0 30.26 14.43 4.95 o 4 12 0 2926.21 2851.72 63.36 o 5 12 0 2068.84 2144.03 45.84 o 6 12 0 48.85 59.10 11.46 o 7 12 0 1175.55 1217.75 52.83 o 8 12 0 702.26 585.99 73.89 o 9 12 0 420.14 428.26 37.30 o 10 12 0 792.30 760.81 63.72 o 1 13 0 3203.87 3782.95 61.63 o 2 13 0 279.74 305.55 23.12 o 3 13 0 121.74 93.88 8.83 o 4 13 0 2748.73 2608.35 55.71 o 5 13 0 115.55 124.22 17.21 o 6 13 0 2277.91 2413.79 78.83 o 7 13 0 4.28 5.31 18.45 o 8 13 0 2113.73 2242.57 103.83 o 9 13 0 31.56 19.67 9.59 o 0 14 0 6038.51 5752.42 120.40 o 1 14 0 1397.69 1498.46 55.37 o 2 14 0 2564.88 2730.33 55.81 o 3 14 0 95.76 95.20 8.23 o 4 14 0 1272.41 1115.41 44.28 o 5 14 0 1520.87 1632.52 58.49 o 6 14 0 123.72 124.61 16.35 o 7 14 0 449.86 444.40 33.98 o 8 14 0 20.26 14.81 16.42 o 9 14 0 501.06 576.98 46.91 o 1 15 0 6948.35 7010.90 144.81 o 2 15 0 274.62 277.69 22.74 o 3 15 0 3579.30 3501.02 68.19 o 4 15 0 43.91 33.35 10.74 o 5 15 0 299.72 322.10 28.13 o 6 15 0 6.56 6.50 10.03 o 7 15 0 94.52 96.92 13.40 o 8 15 0 22.32 32.32 8.83 o 9 15 0 253.90 233.17 35.49 o 0 16 0 158.40 113.94 12.66 o 1 16 0 1624.04 1547.32 58.61 o 2 16 0 2116.30 2039.85 47.69 o 3 16 0 252.73 226.38 22.73 o 4 16 0 2985.77 2945.45 74.22 o 5 16 0 2447.13 2451.58 80.39 o 6 16 0 158.84 148.53 15.54 o 7 16 0 1020.13 981.97 36.19 o 8 16 0 14.37 18.70 10.14 o 9 16 0 589.23 544.57 46.25 o 1 17 0 349.67 330.97 21.92 o 2 17 0 3719.38 4079.31 87.65 o 3 17 0 1161.62 1166.49 23.98 o 4 17 0 5189.70 5092.83 149.39 o 5 17 0 17.39 19.30 4.84 o 6 17 0 751.40 710.90 48.19 o 7 17 0 40.26 41.19 8.79 o 8 17 0 1406.13 1448.94 74.28 o 9 17 0 13.98 0.92 7.41 o 0 18 0 9190.56 9384.48 250.43 o 1 18 0 0.77 34.51 17.24 o 2 18 0 115.83 115.46 11.06 o 3 18 0 217.57 249.70 14.84 o 4 18 0 5237.89 5157.88 141.61 o 5 18 0 917.10 935.29 47.17 o 6 18 0 59.19 48.46 11.13 o 7 18 0 392.01 362.95 27.75 o 8 18 0 27.33 26.13 10.02 o 9 18 0 206.66 229.10 31.56 o 1 19 0 5007.65 5457.90 113.61 o 2 19 0 56.70 56.60 12.24 o 3 19 0 656.94 588.27 29.98 o 4 19 0 24.10 11.63 10.66 o 5 19 0 26.90 17.01 5.60 o 6 19 0 10.27 8.17 7.57 o 7 19 0 7.39 0.15 5.13 o 8 19 0 32.50 9.54 12.68 o 9 19 0 83.08 12.22 23.86 o 0 20 0 3386.88 3743.30 98.90 o 1 20 0 902.69 834.28 45.57 o 2 20 0 318.01 325.73 25.17 o 3 20 0 252.53 271.65 26.62 o 4 20 0 2231.84 2200.09 69.06 o 5 20 0 4839.86 4714.68 185.62 o 6 20 0 10.30 3.67 5.03 o 7 20 0 303.06 300.61 23.31 o 8 20 0 59.35 49.04 6.13 o 1 21 0 392.39 430.00 32.74 o 2 21 0 1003.80 1094.85 53.63 o 3 21 0 2174.30 2232.99 69.76 o 4 21 0 777.99 702.75 39.67 o 5 21 0 22.52 33.04 4.28 o 6 21 0 889.74 917.02 47.27 o 7 21 0 145.83 75.31 22.65 o 8 21 0 1294.42 1324.29 77.97 o 0 22 0 5685.11 5603.44 199.19 o 1 22 0 43.62 78.58 13.86 o 2 22 0 1140.42 1185.26 51.38 o 3 22 0 240.85 218.98 27.43 o 4 22 0 344.66 369.32 23.07 o 5 22 0 394.86 371.44 28.02 o 6 22 0 2.86 -0.11 3.83 o 7 22 0 9.86 9.47 9.58 o 8 22 0 75.97 63.64 15.56 o 1 23 0 1574.19 1731.19 58.36 o 2 23 0 263.82 229.20 19.47 o 3 23 0 2822.93 2985.69 102.27 o 4 23 0 55.16 50.11 11.82 o 5 23 0 49.98 52.14 10.04 o 6 23 0 229.91 215.68 22.72 o 7 23 0 146.11 131.30 26.89 o 8 23 0 452.04 436.83 40.93 o 0 24 0 3.25 14.17 6.90 o 1 24 0 327.69 332.76 25.53 o 2 24 0 149.21 110.15 13.00 o 3 24 0 1018.18 1004.00 62.76 o 4 24 0 41.46 48.21 10.00 o 5 24 0 2244.52 2280.39 91.11 o 6 24 0 119.04 112.32 21.47 o 7 24 0 110.88 111.16 21.63 o 1 25 0 806.92 879.14 34.49 o 2 25 0 476.29 436.18 22.03 o 3 25 0 295.83 285.80 27.80 o 4 25 0 541.93 590.06 45.95 o 5 25 0 186.06 146.09 18.76 o 6 25 0 113.70 126.06 20.99 o 7 25 0 23.29 31.86 14.12 o 0 26 0 3498.15 3696.38 327.81 o 1 26 0 200.29 191.38 20.38 o 2 26 0 582.97 550.62 30.61 o 3 26 0 30.09 51.49 8.73 o 4 26 0 2783.52 2829.28 125.39 o 5 26 0 49.59 47.99 13.88 o 6 26 0 5.42 -10.06 10.06 o 7 26 0 0.94 -1.31 8.38 o 1 27 0 527.27 531.72 38.80 o 2 27 0 270.23 260.91 26.21 o 3 27 0 516.27 510.99 39.19 o 4 27 0 312.65 295.44 31.47 o 5 27 0 5.80 29.02 15.37 o 6 27 0 60.88 57.28 14.58 o 0 28 0 358.73 340.01 32.37 o 1 28 0 702.14 676.88 57.71 o 2 28 0 119.02 137.95 16.60 o 3 28 0 23.83 40.21 13.46 o 4 28 0 110.39 87.64 16.36 o 5 28 0 2041.16 2103.16 131.05 o 6 28 0 85.53 40.30 12.69 o 1 29 0 1802.84 1777.99 69.43 o 2 29 0 39.15 21.23 6.61 o 3 29 0 644.33 669.24 50.49 o 4 29 0 311.35 301.85 28.17 o 5 29 0 183.21 133.70 30.01 o 6 29 0 70.58 77.12 19.75 o 0 30 0 3652.81 3511.05 292.02 o 1 30 0 36.80 37.26 7.39 o 2 30 0 141.76 160.14 17.90 o 3 30 0 19.64 35.84 8.91 o 4 30 0 733.03 786.25 70.83 o 5 30 0 219.27 226.56 27.89 o 1 31 0 191.69 190.85 19.53 o 2 31 0 2.37 17.52 7.08 o 3 31 0 516.76 477.93 45.14 o 4 31 0 63.82 43.44 19.01 o 5 31 0 1.36 7.75 12.73 o 0 32 0 471.18 394.72 44.32 o 1 32 0 950.94 889.97 43.40 o 2 32 0 6.85 23.24 7.22 o 3 32 0 55.83 37.07 8.63 o 4 32 0 27.15 14.88 13.87 o 1 33 0 423.20 427.33 35.21 o 2 33 0 111.62 98.18 24.29 o 3 33 0 773.20 768.30 65.24 o 0 34 0 1451.40 1517.80 90.97 o 1 34 0 241.15 239.16 28.64 o 2 34 0 80.14 94.32 19.64 o 1 35 0 34.08 30.98 12.80 o -9 0 1 59.80 84.72 26.39 o -7 0 1 3059.88 3039.64 214.86 o -5 0 1 4681.23 5078.45 177.43 o -3 0 1 9671.17 9852.93 148.59 o -1 0 1 147.28 200.12 9.54 o 1 0 1 1250.33 1217.41 22.87 o 3 0 1 1421.15 1335.56 30.17 o 5 0 1 927.83 859.45 39.93 o 7 0 1 186.82 192.56 21.94 o 9 0 1 636.29 707.82 60.02 o -10 1 1 100.58 99.59 21.72 o -9 1 1 1640.74 1797.53 89.27 o -8 1 1 1358.20 1418.55 69.03 o -7 1 1 47.82 43.43 15.82 o -6 1 1 44.44 38.25 8.71 o -5 1 1 1466.15 1215.98 42.22 o -4 1 1 4897.00 4838.43 93.28 o -3 1 1 1.81 7.37 1.69 o -2 1 1 570.86 615.52 15.04 o -1 1 1 5687.69 5487.30 59.99 o 0 1 1 17060.25 16373.60 121.91 o 1 1 1 9280.52 8849.49 75.77 o 2 1 1 14.50 18.99 3.42 o 3 1 1 3505.62 3408.19 52.95 o 4 1 1 9636.22 9818.93 147.20 o 5 1 1 8111.16 8264.33 167.62 o 6 1 1 1588.94 1485.91 30.67 o 7 1 1 1301.03 1321.19 41.55 o 8 1 1 3.93 7.59 9.39 o 9 1 1 1163.72 1284.59 61.94 o 10 1 1 248.92 254.17 27.68 o -10 2 1 541.01 585.48 42.85 o -9 2 1 77.23 70.69 11.14 o -8 2 1 6137.22 6854.86 274.61 o -7 2 1 36.43 38.48 6.60 o -6 2 1 2114.23 2103.99 45.55 o -5 2 1 99.18 123.23 11.17 o -4 2 1 6747.39 6946.90 111.60 o -3 2 1 3555.55 3584.82 60.22 o -2 2 1 551.77 505.31 23.00 o -1 2 1 96.43 101.66 4.49 o 0 2 1 93.99 126.29 5.39 o 1 2 1 635.84 647.64 20.97 o 2 2 1 2442.18 2380.17 36.52 o 3 2 1 27.40 37.93 3.20 o 4 2 1 5277.74 4972.65 73.78 o 5 2 1 57.41 73.87 8.27 o 6 2 1 2866.01 2912.57 55.66 o 7 2 1 55.16 68.58 11.20 o 8 2 1 1116.28 1219.13 42.16 o 9 2 1 5.30 22.00 10.39 o 10 2 1 451.28 499.03 39.07 o -10 3 1 350.08 358.98 33.46 o -9 3 1 896.51 925.59 55.20 o -8 3 1 101.39 75.50 33.83 o -7 3 1 436.06 523.20 44.49 o -6 3 1 1063.68 1109.10 39.03 o -5 3 1 1639.29 1648.00 56.65 o -4 3 1 8267.06 8145.55 130.73 o -3 3 1 2661.76 2751.88 144.24 o -2 3 1 983.64 966.46 15.26 o -1 3 1 183.29 185.05 10.02 o 0 3 1 7761.27 7531.57 98.55 o 1 3 1 38.24 73.91 5.56 o 2 3 1 5658.12 5607.58 64.15 o 3 3 1 16.39 14.97 4.13 o 4 3 1 768.11 638.00 27.81 o 5 3 1 4606.92 4801.72 92.09 o 6 3 1 44.85 42.84 6.46 o 7 3 1 624.19 662.32 32.21 o 8 3 1 2.53 5.16 4.24 o 9 3 1 1020.66 1092.26 68.34 o 10 3 1 364.19 358.06 44.11 o -10 4 1 6.22 8.80 9.21 o -9 4 1 0.35 18.25 9.20 o -8 4 1 144.33 154.25 17.66 o -7 4 1 5324.52 5731.22 354.32 o -6 4 1 1113.22 1127.69 27.69 o -5 4 1 954.04 926.18 31.19 o -4 4 1 3576.24 3682.83 55.29 o -3 4 1 9241.05 8962.20 83.10 o -2 4 1 251.40 296.20 13.32 o -1 4 1 5257.83 5157.70 44.59 o 0 4 1 32.70 42.06 2.17 o 1 4 1 25698.23 25690.45 218.52 o 2 4 1 3874.37 3929.14 73.09 o 3 4 1 1165.43 1110.08 19.75 o 4 4 1 1239.54 1437.90 50.59 o 5 4 1 157.68 171.50 15.32 o 6 4 1 175.94 201.75 18.61 o 7 4 1 36.70 39.50 14.63 o 8 4 1 3.77 2.90 5.90 o 9 4 1 1055.52 1097.61 56.83 o 10 4 1 2.64 -1.02 6.73 o -10 5 1 5.27 13.74 7.42 o -9 5 1 1232.70 1378.47 58.28 o -8 5 1 78.13 94.83 11.93 o -7 5 1 607.75 648.96 42.81 o -6 5 1 756.65 794.86 34.47 o -5 5 1 2275.94 2197.49 52.73 o -4 5 1 2335.60 2237.96 81.72 o -3 5 1 187.43 161.92 11.48 o -2 5 1 13747.36 13885.96 127.32 o -1 5 1 1836.38 1917.02 55.34 o 0 5 1 310.66 282.37 12.48 o 1 5 1 25557.48 25199.17 220.65 o 2 5 1 3943.28 3904.17 59.56 o 3 5 1 379.01 334.94 16.61 o 4 5 1 2193.22 2442.93 52.36 o 5 5 1 6570.12 6383.06 132.70 o 6 5 1 159.01 151.52 12.98 o 7 5 1 2548.73 2657.97 87.63 o 8 5 1 80.48 85.42 11.30 o 9 5 1 1198.94 1307.91 84.80 o 10 5 1 120.28 95.35 17.70 o -10 6 1 425.48 447.78 44.48 o -9 6 1 0.55 -5.10 5.10 o -8 6 1 7216.67 7557.02 707.63 o -7 6 1 123.36 124.39 12.54 o -6 6 1 1932.32 1873.47 40.51 o -5 6 1 10.69 24.59 9.41 o -4 6 1 36.01 69.62 6.37 o -3 6 1 832.09 831.21 15.53 o -2 6 1 522.28 598.70 12.96 o -1 6 1 13660.93 14188.51 129.97 o 0 6 1 8394.99 8800.19 90.56 o 1 6 1 147.44 142.79 10.64 o 2 6 1 8115.26 8510.98 100.72 o 3 6 1 333.34 295.49 20.01 o 4 6 1 3737.95 3495.68 52.51 o 5 6 1 0.18 11.45 2.84 o 6 6 1 1108.88 1081.91 43.48 o 7 6 1 356.93 383.19 35.18 o 8 6 1 198.23 256.92 25.67 o 9 6 1 21.78 17.29 11.58 o 10 6 1 286.30 310.42 38.76 o -10 7 1 79.13 90.54 21.17 o -9 7 1 22.41 18.88 7.73 o -8 7 1 8.63 9.39 6.71 o -7 7 1 278.48 279.14 24.60 o -6 7 1 113.28 112.74 16.57 o -5 7 1 264.97 246.24 27.98 o -4 7 1 20593.18 20852.44 420.82 o -3 7 1 99.53 100.62 9.70 o -2 7 1 10169.47 10355.19 108.32 o -1 7 1 2793.36 2900.99 44.75 o 0 7 1 46411.55 45522.06 581.80 o 1 7 1 1165.00 1088.33 17.82 o 2 7 1 422.80 457.36 20.83 o 3 7 1 14.49 21.50 2.68 o 4 7 1 2230.03 2085.82 44.26 o 5 7 1 1912.47 1965.59 45.60 o 6 7 1 623.26 664.03 39.11 o 7 7 1 1770.94 1856.74 69.71 o 8 7 1 13.71 20.85 7.34 o 9 7 1 171.48 176.13 25.00 o 10 7 1 868.87 931.91 80.13 o -10 8 1 124.86 116.10 21.52 o -9 8 1 18.14 17.19 6.66 o -8 8 1 164.38 204.98 27.70 o 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8 2 71.51 90.34 12.42 o -6 8 2 697.01 747.91 48.69 o -5 8 2 1150.15 1084.78 40.40 o -4 8 2 4550.35 4179.27 84.90 o -3 8 2 336.18 321.30 21.55 o -2 8 2 2332.90 2310.01 36.22 o -1 8 2 518.18 531.71 28.43 o 0 8 2 796.74 602.39 15.01 o 1 8 2 3533.20 3388.75 52.56 o 2 8 2 1359.26 1357.62 47.69 o 3 8 2 140.09 115.43 8.42 o 4 8 2 382.03 353.31 21.60 o 5 8 2 1916.31 1912.17 43.71 o 6 8 2 1453.88 1385.58 58.09 o 7 8 2 8.12 23.78 4.67 o 8 8 2 68.40 86.66 11.57 o 9 8 2 690.36 680.50 45.49 o -10 9 2 244.22 270.55 33.75 o -9 9 2 12.02 25.54 7.88 o -8 9 2 1186.60 1229.08 53.00 o -7 9 2 501.76 485.23 38.43 o -6 9 2 131.78 132.01 17.18 o -5 9 2 329.22 319.42 24.69 o -4 9 2 225.75 235.78 20.62 o -3 9 2 993.03 1070.87 35.21 o -2 9 2 1923.32 1792.17 56.27 o -1 9 2 628.04 609.15 32.12 o 0 9 2 2343.44 2244.73 37.88 o 1 9 2 1318.01 1226.47 29.21 o 2 9 2 5065.46 5136.69 76.44 o 3 9 2 458.23 476.14 22.39 o 4 9 2 5319.88 5274.78 106.25 o 5 9 2 148.39 170.15 19.18 o 6 9 2 2227.09 2330.21 77.96 o 7 9 2 42.90 38.06 3.97 o 8 9 2 605.64 542.97 45.23 o 9 9 2 82.19 95.75 17.83 o -10 10 2 24.40 35.10 11.97 o -9 10 2 2539.85 2639.57 122.10 o -8 10 2 950.09 951.28 33.53 o -7 10 2 31.47 36.90 10.33 o -6 10 2 61.72 41.88 7.61 o -5 10 2 1272.85 1221.42 45.25 o -4 10 2 4483.69 4424.06 98.42 o -3 10 2 912.22 872.16 29.08 o -2 10 2 315.34 315.50 20.12 o -1 10 2 35.45 33.15 3.78 o 0 10 2 7305.12 7486.17 92.77 o 1 10 2 4664.71 4283.24 64.46 o 2 10 2 16.09 17.70 3.08 o 3 10 2 2241.11 2213.50 50.60 o 4 10 2 550.74 532.26 28.78 o 5 10 2 7393.13 7549.42 187.83 o 6 10 2 693.18 667.16 38.87 o 7 10 2 106.12 107.97 12.76 o 8 10 2 9.26 -1.08 6.69 o 9 10 2 940.26 952.20 72.83 o -10 11 2 36.23 33.93 9.36 o -9 11 2 56.60 32.40 18.72 o -8 11 2 11.51 16.08 7.55 o -7 11 2 2845.02 2952.96 110.03 o -6 11 2 314.85 308.54 26.33 o -5 11 2 2214.51 2202.26 46.46 o -4 11 2 30.26 50.71 7.79 o -3 11 2 5268.54 4948.20 100.03 o -2 11 2 761.48 855.41 28.01 o -1 11 2 7196.68 7306.28 106.71 o 0 11 2 344.47 314.86 23.75 o 1 11 2 8344.15 8302.57 124.88 o 2 11 2 3.12 4.22 2.28 o 3 11 2 917.18 880.15 29.16 o 4 11 2 26.05 21.13 6.39 o 5 11 2 38.90 27.72 5.86 o 6 11 2 289.49 264.81 23.33 o 7 11 2 64.84 89.33 12.50 o 8 11 2 87.51 91.61 18.82 o 9 11 2 1283.19 1460.41 91.51 o -10 12 2 1.92 9.27 8.82 o -9 12 2 908.87 936.82 54.64 o -8 12 2 853.51 835.89 46.26 o -7 12 2 77.18 79.57 11.61 o -6 12 2 225.41 236.07 19.78 o -5 12 2 446.87 413.50 22.32 o -4 12 2 6019.49 5797.88 121.73 o -3 12 2 243.09 262.53 22.13 o -2 12 2 969.93 853.27 27.87 o -1 12 2 440.13 505.11 26.21 o 0 12 2 1339.96 1245.21 43.51 o 1 12 2 9658.38 9965.57 146.58 o 2 12 2 9.61 12.53 3.60 o 3 12 2 1594.10 1497.93 47.77 o 4 12 2 1268.03 1241.72 40.48 o 5 12 2 2466.52 2475.21 77.08 o 6 12 2 2582.40 2474.25 93.51 o 7 12 2 119.30 116.86 15.70 o 8 12 2 272.83 297.04 27.32 o 9 12 2 156.24 162.60 28.63 o -10 13 2 185.12 203.81 32.36 o -9 13 2 50.34 51.05 10.95 o -8 13 2 1337.22 1352.77 63.20 o -7 13 2 215.52 194.39 23.29 o -6 13 2 251.58 242.67 21.73 o -5 13 2 114.83 124.65 15.94 o -4 13 2 79.55 89.48 9.97 o -3 13 2 1.76 7.34 2.91 o -2 13 2 133.71 70.64 6.43 o -1 13 2 1894.19 1952.04 61.26 o 0 13 2 1289.44 1115.81 41.57 o 1 13 2 164.23 89.32 34.10 o 2 13 2 7524.58 7666.06 154.95 o 3 13 2 31.61 47.03 5.22 o 4 13 2 2409.37 2213.38 43.88 o 5 13 2 118.87 130.17 14.99 o 6 13 2 1797.50 1777.85 75.83 o 7 13 2 240.37 193.33 29.70 o 8 13 2 392.19 402.40 36.99 o 9 13 2 2.54 5.08 9.15 o -9 14 2 393.00 398.69 33.26 o -8 14 2 591.14 612.94 47.75 o -7 14 2 98.80 113.16 14.38 o -6 14 2 101.08 112.03 15.89 o -5 14 2 92.07 78.72 13.90 o -4 14 2 4805.66 4863.95 98.94 o -3 14 2 346.58 283.70 23.09 o -2 14 2 3302.54 3493.65 71.76 o -1 14 2 373.51 395.98 23.54 o 0 14 2 7451.68 7861.88 173.10 o 1 14 2 1647.47 1514.33 51.78 o 2 14 2 54.72 65.15 8.39 o 3 14 2 767.81 820.27 29.42 o 4 14 2 218.58 188.05 16.07 o 5 14 2 4372.66 4270.18 138.51 o 6 14 2 499.17 560.51 42.69 o 7 14 2 459.71 511.26 43.08 o 8 14 2 139.70 148.03 30.49 o 9 14 2 403.73 400.13 40.41 o -9 15 2 34.38 27.13 17.48 o -8 15 2 31.81 26.56 7.69 o -7 15 2 2635.33 2723.64 87.81 o -6 15 2 25.19 23.99 11.49 o -5 15 2 1861.71 1973.20 66.14 o -4 15 2 76.41 65.86 10.63 o -3 15 2 7185.34 7183.74 136.89 o -2 15 2 132.48 131.30 10.67 o -1 15 2 3737.47 3692.26 75.32 o 0 15 2 4.48 8.08 5.47 o 1 15 2 11526.06 11753.34 237.94 o 2 15 2 105.41 78.25 7.82 o 3 15 2 152.19 172.32 16.61 o 4 15 2 99.83 97.74 13.44 o 5 15 2 658.46 631.10 47.35 o 6 15 2 47.79 41.05 7.66 o 7 15 2 878.15 894.25 60.48 o 8 15 2 77.80 42.32 12.23 o 9 15 2 279.54 285.87 32.93 o -9 16 2 829.69 918.32 63.80 o -8 16 2 148.88 131.31 21.27 o -7 16 2 120.90 96.47 14.24 o -6 16 2 431.32 478.43 25.15 o -5 16 2 2951.51 2920.58 95.42 o -4 16 2 2268.03 2209.58 62.14 o -3 16 2 1610.22 1638.37 55.93 o -2 16 2 1016.16 969.03 35.38 o -1 16 2 52.96 46.78 9.05 o 0 16 2 1657.77 1574.50 50.81 o 1 16 2 7086.80 7108.53 135.11 o 2 16 2 155.72 150.20 16.55 o 3 16 2 66.08 46.07 7.04 o 4 16 2 54.25 56.38 8.51 o 5 16 2 1893.07 1904.58 71.27 o 6 16 2 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1719.09 62.22 o 4 18 2 655.82 604.60 36.20 o 5 18 2 940.53 978.50 77.14 o 6 18 2 973.02 946.75 52.14 o 7 18 2 5.62 3.65 8.53 o 8 18 2 11.12 30.94 8.38 o -9 19 2 101.26 63.63 12.20 o -8 19 2 38.22 28.53 13.19 o -7 19 2 1067.93 1132.32 56.06 o -6 19 2 83.36 74.19 14.40 o -5 19 2 3178.17 3181.01 118.43 o -4 19 2 242.26 204.43 19.75 o -3 19 2 3208.32 3123.77 81.32 o -2 19 2 315.73 275.74 16.82 o -1 19 2 2449.72 2568.21 49.07 o 0 19 2 270.31 256.17 18.95 o 1 19 2 1844.11 1805.25 54.82 o 2 19 2 198.06 179.53 27.29 o 3 19 2 1260.19 1259.44 50.67 o 4 19 2 555.86 540.80 48.55 o 5 19 2 2.66 -0.46 10.07 o 6 19 2 180.03 144.36 22.08 o 7 19 2 350.48 377.61 36.17 o 8 19 2 53.27 41.42 11.55 o -8 20 2 84.40 55.90 12.98 o -7 20 2 233.13 211.08 25.97 o -6 20 2 33.36 26.01 9.58 o -5 20 2 298.60 314.62 29.22 o -4 20 2 780.77 788.25 41.50 o -3 20 2 1127.06 1071.03 57.98 o -2 20 2 28.94 30.98 11.87 o -1 20 2 302.13 291.06 25.06 o 0 20 2 1271.87 1339.23 57.37 o 1 20 2 10848.26 11038.93 299.54 o 2 20 2 1623.74 1667.97 47.28 o 3 20 2 358.32 331.82 25.58 o 4 20 2 22.83 16.33 9.11 o 5 20 2 2178.04 2274.71 90.71 o 6 20 2 425.35 370.44 32.90 o 7 20 2 43.31 27.82 9.53 o 8 20 2 2.62 11.03 8.04 o -8 21 2 597.34 570.63 50.38 o -7 21 2 155.24 159.16 29.24 o -6 21 2 588.86 593.94 48.65 o -5 21 2 87.02 104.56 12.86 o -4 21 2 115.43 127.52 16.31 o -3 21 2 1803.71 1756.07 62.81 o -2 21 2 1116.19 1009.49 38.91 o -1 21 2 54.41 63.53 10.10 o 0 21 2 1223.81 1323.13 67.27 o 1 21 2 322.10 271.58 25.43 o 2 21 2 881.60 868.92 35.40 o 3 21 2 283.87 270.88 23.36 o 4 21 2 2101.87 2149.94 97.46 o 5 21 2 3.43 3.73 10.55 o 6 21 2 1076.41 1071.25 52.07 o 7 21 2 3.03 -2.78 7.37 o 8 21 2 96.93 67.47 11.97 o -8 22 2 1724.69 1809.49 93.33 o -7 22 2 0.93 -4.29 8.72 o -6 22 2 254.69 271.09 27.61 o -5 22 2 294.56 269.42 33.99 o -4 22 2 2791.52 2933.82 116.46 o -3 22 2 135.17 126.99 17.53 o -2 22 2 562.46 573.58 33.04 o -1 22 2 1.19 6.47 7.19 o 0 22 2 2891.91 3063.56 101.87 o 1 22 2 1572.08 1626.55 60.92 o 2 22 2 354.94 365.50 27.19 o 3 22 2 2.60 14.12 8.20 o 4 22 2 915.97 899.31 82.40 o 5 22 2 371.53 373.86 34.35 o 6 22 2 387.31 371.67 34.81 o 7 22 2 2.21 8.11 10.78 o -8 23 2 355.96 375.63 33.73 o -7 23 2 905.00 875.87 60.75 o -6 23 2 63.87 43.80 11.50 o -5 23 2 1121.28 1162.90 45.21 o -4 23 2 442.71 471.09 36.07 o -3 23 2 2362.77 2364.35 80.39 o -2 23 2 915.97 826.74 40.88 o -1 23 2 536.78 563.88 31.45 o 0 23 2 436.89 435.66 42.26 o 1 23 2 770.57 739.68 44.21 o 2 23 2 474.84 458.43 21.60 o 3 23 2 18.42 24.20 11.10 o 4 23 2 405.85 438.27 37.50 o 5 23 2 22.99 20.62 9.70 o 6 23 2 217.82 207.98 25.47 o 7 23 2 66.13 35.15 16.28 o -7 24 2 111.16 77.21 15.69 o -6 24 2 1.70 -11.42 11.42 o -5 24 2 212.93 246.46 26.58 o -4 24 2 630.65 563.36 48.37 o -3 24 2 599.74 588.69 64.79 o -2 24 2 105.10 100.97 15.01 o -1 24 2 19.95 16.87 7.80 o 0 24 2 6.89 26.38 6.20 o 1 24 2 3036.67 3184.36 108.21 o 2 24 2 0.97 4.64 8.88 o 3 24 2 480.26 496.30 37.59 o 4 24 2 7.22 24.24 9.29 o 5 24 2 1789.31 1942.88 83.31 o 6 24 2 51.08 35.80 10.10 o 7 24 2 23.12 -3.59 8.97 o -7 25 2 323.24 286.09 33.04 o -6 25 2 6.10 9.15 11.97 o -5 25 2 639.27 650.83 59.12 o -4 25 2 203.89 222.37 26.33 o -3 25 2 1055.42 1027.44 47.49 o -2 25 2 1083.95 960.09 99.78 o -1 25 2 374.38 361.27 24.34 o 0 25 2 474.65 462.90 25.49 o 1 25 2 61.44 39.90 12.84 o 2 25 2 159.03 167.31 17.82 o 3 25 2 33.67 22.82 8.47 o 4 25 2 374.98 342.55 31.17 o 5 25 2 0.31 -0.72 6.27 o 6 25 2 431.48 386.65 43.10 o -7 26 2 8.94 -0.18 5.83 o -6 26 2 141.45 166.43 19.79 o -5 26 2 156.94 167.63 40.24 o -4 26 2 1919.44 2153.58 93.96 o -3 26 2 18.57 58.91 16.71 o -2 26 2 393.15 438.19 37.48 o -1 26 2 39.90 26.57 6.66 o 0 26 2 2550.11 2606.36 104.88 o 1 26 2 1.73 11.39 4.61 o 2 26 2 11.07 11.78 5.89 o 3 26 2 4.15 -4.52 4.52 o 4 26 2 484.09 518.73 75.70 o 5 26 2 3.07 -7.55 7.55 o 6 26 2 894.82 914.67 58.84 o -6 27 2 10.64 19.57 13.83 o -5 27 2 1156.55 1184.94 72.24 o -4 27 2 4.31 -0.34 8.10 o -3 27 2 1852.66 1958.85 90.58 o -2 27 2 8.06 10.57 6.83 o -1 27 2 753.23 755.86 29.66 o 0 27 2 231.67 225.46 24.26 o 1 27 2 127.14 200.39 33.93 o 2 27 2 854.72 904.71 48.54 o 3 27 2 102.97 98.14 20.25 o 4 27 2 345.48 344.13 29.88 o 5 27 2 0.22 2.88 5.54 o 6 27 2 335.32 299.45 36.19 o -6 28 2 3.58 11.07 11.93 o -5 28 2 714.45 672.57 54.54 o -4 28 2 177.45 155.46 27.99 o -3 28 2 774.44 790.68 45.58 o -2 28 2 63.68 70.01 9.78 o -1 28 2 18.41 30.81 8.95 o 0 28 2 122.53 91.59 11.51 o 1 28 2 2028.46 2186.36 77.40 o 2 28 2 288.27 281.97 29.42 o 3 28 2 68.73 53.92 16.64 o 4 28 2 7.01 23.61 10.54 o 5 28 2 1621.76 1794.49 118.76 o -6 29 2 1.00 28.28 21.00 o -5 29 2 222.20 230.61 27.04 o -4 29 2 7.27 10.03 10.62 o -3 29 2 941.31 948.11 67.06 o -2 29 2 389.14 328.80 35.28 o -1 29 2 593.62 610.52 41.20 o 0 29 2 213.59 268.66 34.49 o 1 29 2 453.68 442.20 46.74 o 2 29 2 71.16 71.06 13.04 o 3 29 2 136.84 139.09 23.91 o 4 29 2 490.51 510.74 54.05 o 5 29 2 353.61 325.67 36.49 o -5 30 2 4.18 1.60 8.06 o -4 30 2 2135.60 2364.78 174.64 o -3 30 2 0.16 11.13 19.49 o -2 30 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