#------------------------------------------------------------------------------
#$Date: 2017-03-02 08:08:30 +0200 (Thu, 02 Mar 2017) $
#$Revision: 192762 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/54/53/1545377.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_1545377
loop_
_publ_author_name
'Mayr, Tobias'
'Grassl, Tobias'
'Korber, Nikolaus'
'Christoffel, Volker'
'Bodensteiner, Michael'
_publ_section_title
;
Cannabidiol revisited
;
_journal_coeditor_code SU4129
_journal_issue 2
_journal_name_full IUCrData
_journal_page_first x170276
_journal_paper_doi 10.1107/S2414314617002760
_journal_volume 2
_journal_year 2017
_chemical_formula_iupac 'C21 H30 O2'
_chemical_formula_moiety 'C21 H30 O2'
_chemical_formula_sum 'C21 H30 O2'
_chemical_formula_weight 314.45
_chemical_melting_point_gt 339
_chemical_melting_point_lt 340
_chemical_name_common Cannabidiol
_chemical_name_systematic
2-[(1R,6R)-3-Methyl-6-(prop-1-en-2-yl)cyclohex-2-enyl]-5-pentylbenzene-1,3-diol
_space_group_crystal_system monoclinic
_space_group_IT_number 4
_space_group_name_Hall 'P 2yb'
_space_group_name_H-M_alt 'P 1 21 1'
_symmetry_space_group_name_Hall 'P 2yb'
_symmetry_space_group_name_H-M 'P 1 21 1'
_atom_sites_solution_hydrogens difmap
_atom_sites_solution_primary dual
_audit_creation_method
;
Olex2 1.2-alpha
(compiled 2016.09.09 svn.r3337 for OlexSys, GUI svn.r5227)
;
_cell_angle_alpha 90
_cell_angle_beta 95.4480(10)
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 10.43950(10)
_cell_length_b 10.87390(10)
_cell_length_c 16.7853(2)
_cell_measurement_reflns_used 54306
_cell_measurement_temperature 123
_cell_measurement_theta_max 74.7560
_cell_measurement_theta_min 3.5940
_cell_volume 1896.83(3)
_computing_cell_refinement
;
CrysAlis Pro (Rigaku OD, 2015)
;
_computing_data_collection
;
CrysAlis Pro (Rigaku OD, 2015)
;
_computing_data_reduction
;
CrysAlis Pro (Rigaku OD, 2015)
;
_computing_molecular_graphics
;
Mercury (Macrae et al., 2008)
;
_computing_publication_material
;
OLEX2 (Dolomanov et al., 2009)
;
_computing_structure_refinement
;
SHELXL (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 123
_diffrn_detector_area_resol_mean 4.1818
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device 'four-circle diffractometer'
_diffrn_measurement_device_type 'Agilent GV1000, TitanS2'
_diffrn_measurement_method '\w scans'
_diffrn_radiation_monochromator mirror
_diffrn_radiation_type 'Cu K\b'
_diffrn_radiation_wavelength 1.39222
_diffrn_reflns_av_R_equivalents 0.0442
_diffrn_reflns_limit_h_max 14
_diffrn_reflns_limit_h_min -14
_diffrn_reflns_limit_k_max 14
_diffrn_reflns_limit_k_min -15
_diffrn_reflns_limit_l_max 23
_diffrn_reflns_limit_l_min -23
_diffrn_reflns_number 85198
_diffrn_reflns_theta_full 74.500
_diffrn_reflns_theta_max 75.273
_diffrn_reflns_theta_min 2.388
_exptl_absorpt_coefficient_mu 0.386
_exptl_absorpt_correction_T_max 0.997
_exptl_absorpt_correction_T_min 0.996
_exptl_absorpt_correction_type gaussian
_exptl_absorpt_process_details
;
(CrysAlisPro; Rigaku OD, 2015)
;
_exptl_crystal_colour 'clear colourless'
_exptl_crystal_density_diffrn 1.101
_exptl_crystal_description prism
_exptl_crystal_F_000 688
_exptl_crystal_size_max 0.276
_exptl_crystal_size_mid 0.158
_exptl_crystal_size_min 0.152
_refine_diff_density_max 0.232
_refine_diff_density_min -0.126
_refine_ls_abs_structure_details
;
Flack x determined using 4335 quotients
[(I^+^)-(I^-^)]/[(I^+^)+(I^-^)]
(Parsons et al., 2013
;
_refine_ls_abs_structure_Flack -0.03(6)
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.027
_refine_ls_hydrogen_treatment refall
_refine_ls_matrix_type full
_refine_ls_number_parameters 655
_refine_ls_number_reflns 10203
_refine_ls_number_restraints 1
_refine_ls_restrained_S_all 1.027
_refine_ls_R_factor_all 0.0336
_refine_ls_R_factor_gt 0.0322
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0493P)^2^+0.1553P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0861
_refine_ls_wR_factor_ref 0.0881
_reflns_number_gt 9859
_reflns_number_total 10203
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file su4129sup1.cif
_cod_data_source_block I
_cod_database_code 1545377
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_hkl_file
;
0 -15 1 24.46 1.62
0 -14 0 52.17 3.02
0 -14 0 43.40 2.48
0 -14 0 52.04 3.24
0 -14 -1 9.90 1.31
0 -14 1 13.04 1.68
0 -14 -1 13.92 1.66
0 -14 -1 10.05 1.29
0 -14 1 10.91 1.52
0 -14 -1 12.61 1.66
0 -14 -2 5.28 1.06
0 -14 -2 5.52 1.09
0 -14 -2 3.08 0.95
0 -14 2 4.97 1.07
0 -14 -2 5.18 0.97
0 -14 2 4.89 1.08
0 -14 3 1.37 0.69
0 -14 -3 1.37 0.79
0 -14 -3 0.63 0.56
0 -14 3 -0.01 0.58
0 -14 -3 0.94 0.56
0 -14 -3 0.80 0.66
0 -14 4 41.85 2.59
0 -14 -4 40.19 2.37
0 -14 -4 45.00 2.54
0 -14 -4 37.70 2.65
0 -14 -5 1.28 0.73
0 -14 5 1.41 0.63
0 -14 -5 1.05 0.57
0 -14 5 0.39 0.49
0 -14 6 42.78 2.43
0 -14 -6 45.45 2.36
0 -14 -6 41.71 2.68
0 -14 7 1.04 0.50
0 -14 7 0.41 0.42
0 -14 -7 1.01 0.63
0 -14 -7 0.64 0.38
0 -14 -8 6.77 0.98
0 -13 0 -0.32 0.89
0 -13 0 -0.52 0.70
0 -13 0 -0.11 0.85
0 -13 -1 8.90 1.80
0 -13 1 4.88 1.20
0 -13 -1 9.75 1.74
0 -13 1 7.69 1.66
0 -13 1 7.76 1.67
0 -13 1 6.68 1.27
0 -13 -1 5.81 1.29
0 -13 -2 10.44 1.64
0 -13 -2 9.30 1.54
0 -13 -2 12.38 1.87
0 -13 2 7.52 1.68
0 -13 2 10.51 1.55
0 -13 -2 11.36 1.76
0 -13 -2 11.75 2.04
0 -13 2 12.48 1.93
0 -13 -3 5.32 1.27
0 -13 -3 5.33 1.46
0 -13 3 2.96 0.92
0 -13 -3 8.13 2.04
0 -13 -3 4.81 1.35
0 -13 -3 4.23 1.36
0 -13 3 3.34 1.34
0 -13 3 2.52 1.02
0 -13 4 4.74 1.25
0 -13 -4 7.32 1.43
0 -13 4 6.33 1.15
0 -13 -4 6.89 1.44
0 -13 -4 7.04 1.41
0 -13 -4 4.88 1.23
0 -13 4 5.59 1.30
0 -13 -4 5.85 1.68
0 -13 -5 24.24 2.43
0 -13 -5 25.64 2.77
0 -13 5 19.66 1.80
0 -13 5 21.38 2.30
0 -13 5 15.62 2.07
0 -13 -5 20.02 2.21
0 -13 -5 19.29 2.17
0 -13 -5 22.89 2.29
0 -13 -6 35.44 2.70
0 -13 -6 30.90 2.60
0 -13 6 28.10 2.58
0 -13 -6 31.24 2.71
0 -13 -6 31.78 2.42
0 -13 -7 24.28 2.24
0 -13 -7 23.73 2.29
0 -13 -7 24.59 2.27
0 -13 7 19.89 2.02
0 -13 8 7.64 1.15
0 -13 -8 15.61 1.79
0 -13 8 11.44 1.50
0 -13 8 5.20 1.12
0 -13 -8 13.61 1.62
0 -13 -8 12.31 1.67
0 -13 9 4.62 1.02
0 -13 9 9.46 1.30
0 -13 -9 12.87 1.52
0 -13 9 6.12 0.97
0 -13 -9 12.40 1.56
0 -13 -9 14.10 1.57
0 -13 -10 29.95 2.11
0 -13 -10 30.06 2.05
0 -13 -10 25.71 2.11
0 -13 10 26.42 1.84
0 -13 -10 26.56 2.18
0 -13 -11 0.54 0.47
0 -13 -11 2.54 0.78
0 -13 -11 1.69 0.53
0 -13 -11 1.35 0.62
0 -12 0 5.94 1.39
0 -12 0 7.06 1.63
0 -12 0 4.63 1.31
0 -12 0 6.95 1.63
0 -12 0 7.99 1.69
0 -12 0 6.01 1.89
0 -12 1 9.30 1.58
0 -12 1 12.30 2.13
0 -12 -1 12.87 2.25
0 -12 -1 12.94 2.00
0 -12 -1 11.27 1.93
0 -12 1 12.93 2.13
0 -12 -1 13.97 2.05
0 -12 -1 12.09 1.99
0 -12 -1 13.65 2.19
0 -12 -1 15.05 2.43
0 -12 1 11.10 1.72
0 -12 -2 62.38 4.54
0 -12 -2 51.00 3.82
0 -12 -2 59.34 4.50
0 -12 2 50.07 3.40
0 -12 2 52.19 3.76
0 -12 -2 65.67 4.40
0 -12 -2 55.12 3.90
0 -12 -2 56.17 4.04
0 -12 2 58.98 4.34
0 -12 -2 52.81 3.86
0 -12 2 66.12 4.57
0 -12 2 56.99 4.86
0 -12 3 20.55 2.60
0 -12 -3 23.42 2.95
0 -12 3 15.01 2.06
0 -12 -3 21.17 2.56
0 -12 3 31.73 3.84
0 -12 -3 19.00 2.41
0 -12 3 16.93 1.92
0 -12 3 25.51 3.04
0 -12 -3 19.66 2.46
0 -12 -3 21.55 2.52
0 -12 -3 22.58 2.93
0 -12 4 79.11 4.82
0 -12 -4 76.13 4.77
0 -12 4 56.60 4.02
0 -12 -4 79.17 5.21
0 -12 -4 81.77 5.23
0 -12 -4 79.30 4.66
0 -12 4 79.53 4.75
0 -12 -4 78.78 4.77
0 -12 -4 79.54 4.73
0 -12 -4 75.70 4.89
0 -12 4 67.77 4.10
0 -12 4 76.12 5.45
0 -12 5 29.68 3.27
0 -12 -5 27.27 3.04
0 -12 -5 31.32 3.08
0 -12 -5 29.95 2.85
0 -12 5 33.92 4.35
0 -12 5 21.64 2.51
0 -12 -5 27.90 2.93
0 -12 -5 28.42 2.99
0 -12 5 28.89 2.59
0 -12 5 32.30 3.18
0 -12 -5 27.04 3.39
0 -12 -5 31.62 3.48
0 -12 -6 15.33 2.29
0 -12 6 16.44 1.96
0 -12 -6 13.03 2.26
0 -12 6 13.40 2.22
0 -12 6 14.40 2.12
0 -12 -6 15.31 2.16
0 -12 -6 12.36 2.34
0 -12 -6 15.98 2.33
0 -12 6 15.50 2.22
0 -12 -6 17.47 2.74
0 -12 -6 15.69 1.98
0 -12 -7 30.25 2.85
0 -12 7 25.68 2.88
0 -12 7 28.49 2.45
0 -12 7 27.58 2.79
0 -12 -7 32.53 3.50
0 -12 -7 28.71 2.42
0 -12 -7 30.72 2.87
0 -12 7 27.00 2.58
0 -12 -7 29.42 2.95
0 -12 -7 29.51 3.14
0 -12 -8 78.19 4.91
0 -12 -8 76.18 4.25
0 -12 8 68.73 4.12
0 -12 -8 80.03 4.53
0 -12 8 54.32 4.10
0 -12 8 63.08 3.78
0 -12 -8 86.85 4.85
0 -12 -8 87.14 5.03
0 -12 8 70.13 3.54
0 -12 -9 33.61 2.65
0 -12 9 35.99 2.84
0 -12 -9 38.08 3.09
0 -12 9 23.51 2.26
0 -12 -9 38.63 3.38
0 -12 -9 40.27 3.13
0 -12 9 25.96 2.84
0 -12 10 8.30 1.28
0 -12 -10 13.87 1.94
0 -12 -10 13.86 2.08
0 -12 10 12.01 1.59
0 -12 10 9.99 1.88
0 -12 -10 13.60 1.84
0 -12 -11 2.87 1.10
0 -12 11 1.24 0.74
0 -12 11 1.14 0.53
0 -12 11 4.22 1.61
0 -12 -11 3.46 1.04
0 -12 -11 2.16 0.84
0 -12 -12 13.10 1.48
0 -12 12 11.13 1.26
0 -12 -12 11.33 1.45
0 -12 -12 13.53 1.73
0 -12 -12 9.56 1.38
0 -12 12 11.01 1.65
0 -12 -13 10.22 1.23
0 -12 -13 12.59 1.34
0 -12 -13 10.41 1.40
0 -12 13 11.25 1.11
0 -12 -14 -0.13 0.44
0 -11 0 -0.42 0.91
0 -11 0 -0.98 1.09
0 -11 0 -1.62 1.62
0 -11 0 -1.76 1.54
0 -11 0 -0.35 1.13
0 -11 0 -1.49 1.30
0 -11 0 0.82 0.98
0 -11 1 23.43 2.88
0 -11 -1 24.58 2.86
0 -11 1 22.50 2.92
0 -11 -1 21.19 2.60
0 -11 -1 26.33 2.99
0 -11 -1 24.46 2.91
0 -11 -1 21.64 2.87
0 -11 1 24.37 3.05
0 -11 1 28.45 3.27
0 -11 -1 23.46 2.70
0 -11 1 25.16 2.83
0 -11 1 27.42 3.84
0 -11 1 23.01 2.57
0 -11 -1 23.10 3.05
0 -11 -2 134.74 6.83
0 -11 2 152.35 7.17
0 -11 -2 141.08 7.07
0 -11 2 127.03 6.17
0 -11 -2 146.68 6.83
0 -11 2 127.83 5.66
0 -11 -2 131.42 6.53
0 -11 -2 142.16 6.91
0 -11 2 127.68 7.03
0 -11 -2 120.01 6.12
0 -11 -2 130.68 6.24
0 -11 -2 146.21 6.66
0 -11 2 142.42 6.90
0 -11 2 131.31 6.23
0 -11 3 8.33 1.46
0 -11 -3 13.92 2.63
0 -11 -3 11.25 2.22
0 -11 -3 10.80 2.20
0 -11 -3 10.37 1.96
0 -11 -3 9.34 2.13
0 -11 -3 7.05 2.01
0 -11 3 13.02 2.36
0 -11 3 9.15 1.80
0 -11 3 9.15 1.76
0 -11 -3 12.73 2.46
0 -11 -3 11.54 2.21
0 -11 3 13.86 3.21
0 -11 3 12.83 2.33
0 -11 -3 11.15 2.02
0 -11 -4 111.84 6.01
0 -11 -4 122.27 6.29
0 -11 -4 111.75 6.35
0 -11 -4 123.25 6.86
0 -11 -4 120.61 6.03
0 -11 4 110.99 6.02
0 -11 -4 114.13 6.03
0 -11 -4 120.96 6.61
0 -11 4 99.95 4.81
0 -11 -4 116.19 6.00
0 -11 4 111.31 5.57
0 -11 4 95.59 5.92
0 -11 -4 119.90 6.32
0 -11 4 115.45 7.07
0 -11 4 121.10 6.37
0 -11 -5 117.97 6.53
0 -11 5 106.45 6.38
0 -11 -5 129.16 6.10
0 -11 5 125.56 6.44
0 -11 -5 120.73 6.76
0 -11 5 119.57 5.70
0 -11 5 114.60 6.13
0 -11 -5 119.95 6.18
0 -11 -5 130.57 6.86
0 -11 -5 122.03 6.19
0 -11 -5 128.31 6.43
0 -11 5 126.86 7.75
0 -11 -5 129.51 6.47
0 -11 -6 22.47 2.89
0 -11 6 29.66 4.25
0 -11 6 23.45 2.60
0 -11 -6 23.75 2.99
0 -11 -6 22.35 2.89
0 -11 -6 25.60 3.40
0 -11 -6 24.83 3.18
0 -11 -6 24.94 2.80
0 -11 6 22.12 3.22
0 -11 -6 25.57 2.90
0 -11 6 23.35 2.92
0 -11 6 23.93 3.00
0 -11 -6 22.63 3.13
0 -11 -7 -0.66 1.26
0 -11 -7 1.16 1.40
0 -11 7 0.36 0.86
0 -11 -7 0.05 1.32
0 -11 7 0.02 1.38
0 -11 7 0.40 1.13
0 -11 -7 1.66 1.01
0 -11 -7 1.86 1.34
0 -11 -7 -0.47 1.33
0 -11 -7 -1.08 1.18
0 -11 7 0.15 0.84
0 -11 8 28.50 3.01
0 -11 -8 29.39 3.52
0 -11 8 26.87 3.60
0 -11 8 42.06 4.99
0 -11 -8 25.95 3.01
0 -11 -8 38.11 3.44
0 -11 8 33.70 3.14
0 -11 -8 29.84 3.04
0 -11 8 30.35 2.71
0 -11 -8 33.30 3.63
0 -11 -9 36.76 3.43
0 -11 9 35.63 3.74
0 -11 9 38.99 2.87
0 -11 9 50.77 5.47
0 -11 -9 42.51 3.90
0 -11 -9 40.98 3.55
0 -11 -9 38.71 3.97
0 -11 9 30.09 2.93
0 -11 9 38.41 3.27
0 -11 -9 43.65 3.59
0 -11 -10 7.03 1.86
0 -11 10 2.76 1.51
0 -11 -10 4.92 1.69
0 -11 10 6.33 1.43
0 -11 10 3.63 1.02
0 -11 10 4.73 1.21
0 -11 -10 6.99 1.71
0 -11 -10 3.70 1.37
0 -11 10 4.09 0.96
0 -11 -11 1.50 1.19
0 -11 -11 -0.45 1.03
0 -11 11 0.11 0.72
0 -11 11 0.50 1.35
0 -11 11 1.56 0.98
0 -11 11 -0.53 0.80
0 -11 -11 1.06 0.97
0 -11 -11 1.74 1.40
0 -11 12 84.32 4.96
0 -11 12 82.41 4.12
0 -11 -12 95.87 4.73
0 -11 -12 82.35 4.12
0 -11 -12 91.68 4.65
0 -11 -12 88.46 5.05
0 -11 -13 10.02 1.54
0 -11 13 7.00 1.22
0 -11 -13 5.69 1.36
0 -11 13 5.69 1.68
0 -11 -13 8.37 1.51
0 -11 14 22.73 2.34
0 -11 14 20.60 1.76
0 -11 -14 18.37 1.88
0 -11 -14 22.67 2.03
0 -11 -14 20.05 2.07
0 -11 15 3.34 0.68
0 -11 -15 4.03 0.79
0 -11 15 4.13 1.00
0 -11 -15 2.46 0.77
0 -11 -15 3.43 0.86
0 -10 0 16.26 2.16
0 -10 0 18.72 2.62
0 -10 0 21.38 3.16
0 -10 0 19.71 3.27
0 -10 0 18.14 2.49
0 -10 0 20.76 2.55
0 -10 0 19.50 2.82
0 -10 0 18.10 2.81
0 -10 0 18.67 2.59
0 -10 0 19.76 2.50
0 -10 1 62.96 4.13
0 -10 -1 71.50 5.01
0 -10 -1 70.83 4.72
0 -10 -1 72.25 4.68
0 -10 1 68.16 4.43
0 -10 1 66.72 5.42
0 -10 1 76.42 4.77
0 -10 -1 62.56 4.84
0 -10 -1 74.87 4.64
0 -10 -1 62.66 4.24
0 -10 -1 76.97 5.06
0 -10 -1 77.80 4.95
0 -10 1 76.82 4.76
0 -10 1 67.67 4.68
0 -10 -1 72.76 5.19
0 -10 1 77.83 4.99
0 -10 1 79.74 5.23
0 -10 2 76.95 4.81
0 -10 -2 77.38 4.94
0 -10 2 75.54 4.77
0 -10 -2 64.62 4.57
0 -10 -2 74.06 5.34
0 -10 -2 77.01 4.87
0 -10 -2 72.42 4.63
0 -10 2 77.80 5.23
0 -10 2 73.60 4.42
0 -10 2 74.80 4.98
0 -10 2 74.11 4.75
0 -10 -2 73.03 4.93
0 -10 -2 68.95 4.81
0 -10 -2 81.19 5.38
0 -10 2 76.36 5.78
0 -10 -2 79.49 5.32
0 -10 -3 123.05 6.62
0 -10 3 110.77 5.64
0 -10 3 127.56 5.64
0 -10 -3 133.09 7.18
0 -10 3 125.75 6.48
0 -10 3 126.21 6.12
0 -10 3 127.02 7.41
0 -10 -3 134.47 6.40
0 -10 -3 119.07 6.54
0 -10 3 103.74 6.42
0 -10 3 120.99 6.27
0 -10 -3 125.77 6.24
0 -10 -3 128.79 6.61
0 -10 -3 119.14 6.09
0 -10 -3 115.81 5.96
0 -10 -3 120.98 6.45
0 -10 -4 83.01 5.35
0 -10 -4 86.31 5.77
0 -10 4 80.02 4.35
0 -10 -4 85.53 5.61
0 -10 -4 81.27 5.09
0 -10 4 83.09 5.30
0 -10 4 86.63 4.95
0 -10 4 75.33 5.38
0 -10 -4 85.74 5.08
0 -10 -4 80.79 5.10
0 -10 4 80.38 5.13
0 -10 -4 71.80 4.30
0 -10 -4 83.36 5.11
0 -10 -4 82.25 5.51
0 -10 4 85.22 6.45
0 -10 -4 87.41 5.40
0 -10 -5 5.70 1.75
0 -10 -5 2.37 1.29
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10 2 11 20.02 2.32
10 2 11 19.24 2.35
10 2 11 17.51 2.33
-10 2 -11 15.59 2.22
10 2 11 19.91 2.18
-10 2 -11 15.99 2.13
-10 2 -11 19.41 2.51
10 2 11 18.90 2.23
10 2 11 18.32 2.15
10 2 11 19.22 2.09
10 2 12 3.40 1.06
10 2 12 3.35 0.94
10 2 12 4.25 1.14
10 2 12 4.70 1.25
-10 2 -12 2.77 1.00
-10 2 -12 3.45 1.16
10 2 12 3.94 1.03
-10 2 -12 6.82 1.42
10 2 12 3.28 0.92
10 2 13 15.78 1.73
10 2 13 17.16 1.80
10 2 13 16.60 1.67
-10 2 -13 16.02 1.78
-10 2 -13 12.57 1.70
10 2 13 17.83 1.84
10 2 14 29.13 2.03
10 2 14 30.04 2.07
10 2 14 27.23 1.88
-10 2 -14 26.44 1.80
-10 2 -14 30.93 2.13
10 2 14 31.14 2.08
10 3 -17 2.04 0.78
10 3 -17 1.10 0.62
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10 3 -16 2.14 0.92
10 3 -16 1.29 0.78
10 3 -16 1.14 0.86
10 3 -16 1.36 0.91
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10 3 -15 3.44 1.06
10 3 -15 4.78 1.08
10 3 -15 7.23 1.57
10 3 -15 5.11 1.33
10 3 -15 4.35 1.45
10 3 -15 5.99 1.41
-10 3 15 6.09 1.22
-10 3 15 6.58 1.17
-10 3 15 5.82 1.01
10 3 -14 21.84 2.34
10 3 -14 24.68 2.76
10 3 -14 24.51 2.79
10 3 -14 23.14 2.60
10 3 -14 23.02 2.86
-10 3 14 26.33 2.49
10 3 -14 22.50 2.39
-10 3 14 22.00 2.17
10 3 -14 25.37 2.97
10 3 -13 2.39 1.25
10 3 -13 3.71 1.39
10 3 -13 2.39 1.44
10 3 -13 4.21 1.63
10 3 -13 3.90 1.63
10 3 -13 1.75 1.22
-10 3 13 2.99 1.16
10 3 -13 3.34 1.11
-10 3 13 2.80 0.97
10 3 -12 14.32 2.72
10 3 -12 16.67 2.44
10 3 -12 16.58 2.68
10 3 -12 16.64 2.74
10 3 -12 17.05 2.83
10 3 -12 15.05 2.33
-10 3 12 16.36 2.31
10 3 -12 12.32 1.97
10 3 -12 16.41 2.05
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10 3 -11 7.30 2.42
10 3 -11 7.60 1.94
10 3 -11 7.78 2.25
10 3 -11 3.80 1.81
10 3 -11 5.89 2.21
10 3 -11 5.13 1.70
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10 3 -11 4.31 1.28
-10 3 11 3.77 1.09
10 3 -10 149.83 7.48
10 3 -10 151.55 7.79
10 3 -10 138.13 7.63
10 3 -10 128.29 6.54
10 3 -10 152.94 8.26
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10 3 -10 141.18 6.55
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10 3 -10 155.81 8.70
10 3 -9 58.19 4.95
10 3 -9 63.66 5.18
10 3 -9 59.21 5.09
10 3 -9 55.22 4.35
10 3 -9 64.99 5.55
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10 3 -9 59.76 4.53
10 3 -9 57.77 5.67
10 3 -8 46.02 4.49
10 3 -8 48.91 4.72
10 3 -8 47.65 3.99
10 3 -8 51.91 4.81
10 3 -8 48.91 4.15
10 3 -8 50.72 4.90
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10 3 -8 50.07 4.23
10 3 -8 55.21 5.62
10 3 -7 105.62 5.65
10 3 -7 105.28 6.72
10 3 -7 99.88 6.50
10 3 -7 104.76 6.16
10 3 -7 101.44 6.76
10 3 -7 90.99 5.45
10 3 -7 99.64 6.81
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10 3 -7 102.46 6.11
10 3 -7 110.50 7.79
10 3 -6 34.27 3.28
10 3 -6 35.59 3.98
10 3 -6 34.56 3.96
10 3 -6 28.99 3.53
10 3 -6 33.32 4.02
10 3 -6 28.77 3.02
10 3 -6 29.07 3.89
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10 3 -6 32.33 3.62
10 3 -6 37.01 4.62
10 3 -5 45.17 3.84
10 3 -5 42.49 4.35
10 3 -5 42.87 4.45
10 3 -5 44.78 4.27
10 3 -5 47.58 4.57
10 3 -5 44.24 4.60
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10 3 -5 48.39 4.38
10 3 -5 42.55 4.95
10 3 -4 33.61 3.39
10 3 -4 33.06 3.88
10 3 -4 32.16 3.80
10 3 -4 29.04 2.82
10 3 -4 33.86 3.82
10 3 -4 35.65 4.04
10 3 -4 32.42 3.98
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10 3 -4 35.17 3.95
10 3 -4 35.25 4.50
10 3 -3 80.89 5.23
10 3 -3 79.45 5.91
10 3 -3 87.42 5.93
10 3 -3 80.92 11.84
10 3 -3 87.36 4.84
10 3 -3 85.36 6.14
10 3 -3 84.68 5.93
10 3 -3 78.96 6.02
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10 3 -3 88.86 5.97
10 3 -3 92.37 6.96
10 3 -2 11.58 2.88
10 3 -2 9.95 2.09
10 3 -2 9.58 2.39
10 3 -2 11.06 2.50
10 3 -2 11.45 1.99
10 3 -2 12.69 2.80
10 3 -2 8.13 4.48
10 3 -2 13.38 2.70
10 3 -2 10.72 2.49
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10 3 -2 9.92 1.66
10 3 -2 9.37 2.47
10 3 -1 159.49 7.38
10 3 -1 164.41 8.43
10 3 -1 163.11 7.99
10 3 -1 184.27 17.99
10 3 -1 158.63 6.77
10 3 -1 170.74 8.86
10 3 -1 171.92 8.21
10 3 -1 162.25 8.20
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-10 3 1 187.91 7.99
10 3 -1 153.86 6.32
-10 3 1 160.91 14.17
10 3 -1 178.92 8.37
10 3 -1 159.79 8.96
10 3 0 56.96 4.46
10 3 0 64.93 5.34
10 3 0 66.33 10.73
10 3 0 58.72 4.18
10 3 0 65.65 5.68
10 3 0 63.20 4.93
10 3 0 61.90 4.97
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10 3 0 62.42 4.07
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-10 3 0 52.15 8.33
10 3 0 60.21 4.88
10 3 0 67.33 5.77
10 3 1 47.47 3.87
10 3 1 49.10 3.60
10 3 1 50.40 4.22
10 3 1 49.54 4.66
10 3 1 55.36 4.11
10 3 1 54.82 5.11
10 3 1 53.00 4.46
10 3 1 49.55 4.42
-10 3 -1 62.75 4.70
-10 3 -1 53.35 4.21
10 3 1 53.65 3.82
-10 3 -1 55.66 4.19
10 3 1 56.22 4.80
10 3 1 48.58 4.64
10 3 2 3.18 1.26
10 3 2 4.36 1.29
10 3 2 1.97 1.22
10 3 2 2.00 1.61
10 3 2 2.69 0.96
10 3 2 4.04 1.28
10 3 2 2.83 1.96
10 3 2 2.65 1.18
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10 3 2 3.50 1.09
10 3 2 4.91 1.71
10 3 2 2.38 1.53
10 3 3 19.29 2.52
10 3 3 20.41 2.45
10 3 3 20.53 2.42
10 3 3 19.61 2.71
10 3 3 20.24 3.24
10 3 3 24.83 2.90
10 3 3 19.97 3.21
10 3 3 22.88 2.85
10 3 3 19.65 2.71
-10 3 -3 20.99 2.75
-10 3 -3 20.89 2.58
10 3 3 21.18 2.54
10 3 3 22.99 3.18
10 3 3 18.25 2.80
10 3 4 23.71 2.79
10 3 4 26.58 2.85
10 3 4 27.90 2.88
10 3 4 24.80 3.11
10 3 4 22.47 2.70
10 3 4 22.44 3.32
10 3 4 24.74 2.84
10 3 4 22.99 2.83
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10 3 4 23.50 2.72
10 3 4 24.53 3.19
10 3 4 23.19 3.03
10 3 5 15.94 2.41
10 3 5 12.26 2.02
10 3 5 15.25 2.53
10 3 5 14.02 2.07
10 3 5 15.81 2.33
10 3 5 11.14 2.42
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-10 3 -5 11.40 1.90
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10 3 5 12.39 2.31
10 3 5 13.90 2.53
10 3 6 1.40 1.11
10 3 6 1.09 1.05
10 3 6 3.76 1.62
10 3 6 2.44 0.94
10 3 6 1.59 1.14
10 3 6 4.40 1.92
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10 3 6 2.39 1.01
10 3 6 1.05 1.11
10 3 6 3.29 1.33
10 3 7 20.08 2.53
10 3 7 19.22 2.47
10 3 7 24.57 3.16
10 3 7 20.98 2.73
10 3 7 22.25 3.26
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10 3 7 23.05 2.75
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10 3 8 0.80 0.88
10 3 8 1.53 1.45
10 3 8 1.04 1.00
10 3 8 -0.05 1.13
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10 3 9 49.97 3.69
10 3 9 50.71 3.78
10 3 9 58.87 4.21
10 3 9 53.72 3.89
10 3 9 50.17 4.20
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10 3 9 55.75 3.79
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10 3 9 51.28 3.82
10 3 9 59.13 3.96
10 3 10 13.95 2.06
10 3 10 13.83 1.94
10 3 10 14.27 2.02
10 3 10 14.88 2.14
10 3 10 12.75 2.06
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10 3 10 12.49 1.90
10 3 11 24.15 2.42
10 3 11 23.45 2.43
10 3 11 23.23 2.39
-10 3 -11 21.34 2.20
10 3 11 26.91 2.48
-10 3 -11 21.36 2.33
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10 3 11 26.10 2.43
10 3 11 22.76 2.39
10 3 11 26.27 2.42
10 3 12 14.92 1.80
10 3 12 15.51 1.80
10 3 12 16.45 1.80
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10 3 12 20.26 1.98
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10 3 13 11.96 1.52
10 3 13 13.71 1.59
10 3 13 15.98 1.62
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-10 3 -13 11.98 1.42
10 3 13 15.64 1.69
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10 3 14 29.72 1.93
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10 4 -16 2.22 0.89
10 4 -16 3.10 0.92
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10 4 -15 2.85 1.06
10 4 -15 3.05 1.06
10 4 -15 1.96 1.17
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10 4 -14 8.75 1.69
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10 4 -10 27.79 3.38
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10 4 -6 7.20 2.16
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10 4 -6 6.47 2.21
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10 4 -5 75.39 5.54
10 4 -5 74.14 4.44
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10 4 -5 73.51 5.68
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10 5 -15 10.39 1.41
10 5 -15 10.12 1.52
10 5 -15 9.37 1.48
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10 5 -15 9.03 1.24
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10 5 -13 15.56 2.23
10 5 -13 15.58 2.23
10 5 -13 14.80 2.13
10 5 -13 12.20 2.20
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10 5 -12 0.41 1.26
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10 5 -11 16.77 2.55
10 5 -11 15.87 2.47
10 5 -11 11.44 2.23
10 5 -11 14.15 2.02
10 5 -11 17.31 2.73
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10 5 -11 19.55 2.48
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10 5 -10 32.60 3.52
10 5 -10 30.64 2.95
10 5 -10 31.91 3.43
10 5 -10 25.80 2.60
10 5 -10 31.53 3.64
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10 5 -10 31.83 3.25
10 5 -10 31.21 3.96
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10 5 -9 24.13 3.22
10 5 -9 22.98 3.05
10 5 -9 23.76 2.86
10 5 -9 20.76 3.01
10 5 -9 21.22 3.15
10 5 -9 23.09 2.85
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10 5 -8 3.43 1.72
10 5 -8 4.30 1.82
10 5 -8 2.54 1.56
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13 6 -1 10.52 1.28
13 6 0 23.29 1.53
13 6 0 22.44 1.65
13 6 0 21.94 1.89
-13 6 0 29.83 1.97
-13 6 0 22.34 1.71
13 6 0 25.01 1.88
13 6 1 6.53 0.90
13 6 1 9.22 1.23
-13 6 -1 8.44 1.07
-13 6 -1 4.96 0.94
13 6 1 9.15 1.12
13 6 2 5.46 0.94
-13 6 -2 5.07 0.90
14 -3 -5 7.18 1.11
-14 -3 5 7.37 1.00
14 -3 -4 5.94 1.11
-14 -3 4 5.99 0.91
14 -3 -4 5.33 1.00
14 -3 -3 18.34 1.76
14 -3 -3 19.26 1.58
-14 -3 3 19.58 1.60
14 -3 -3 18.03 1.61
14 -3 -3 18.35 1.79
14 -3 -2 5.63 1.07
14 -3 -2 5.91 0.95
14 -3 -2 3.19 0.92
-14 -3 2 8.07 1.06
-14 -3 2 6.06 0.84
14 -3 -2 5.53 0.97
14 -3 -2 6.12 1.16
14 -3 -1 1.28 0.61
14 -3 -1 0.59 0.53
-14 -3 1 0.52 0.44
-14 -3 1 1.78 0.61
14 -3 -1 1.33 0.60
14 -3 -1 0.37 0.64
14 -3 0 6.02 1.03
-14 -3 0 8.08 1.03
-14 -3 0 6.88 0.98
14 -3 0 6.77 1.05
14 -3 0 6.44 1.10
14 -3 1 17.22 1.56
-14 -3 -1 19.99 1.52
14 -3 1 20.90 1.67
14 -3 1 19.30 1.76
14 -2 -6 7.90 1.17
14 -2 -6 7.38 1.04
-14 -2 6 9.70 1.13
14 -2 -5 2.70 1.05
14 -2 -5 5.03 1.11
14 -2 -5 5.63 0.95
14 -2 -5 3.42 0.82
-14 -2 5 4.01 0.81
14 -2 -5 4.28 0.97
14 -2 -4 5.23 1.41
14 -2 -4 5.31 1.16
14 -2 -4 6.86 1.15
14 -2 -4 5.01 0.99
-14 -2 4 6.14 1.00
14 -2 -4 4.13 0.93
14 -2 -4 5.46 1.11
14 -2 -3 66.68 3.95
14 -2 -3 71.15 3.58
14 -2 -3 75.49 3.41
14 -2 -3 68.94 3.40
-14 -2 3 78.82 3.32
14 -2 -3 60.15 3.16
14 -2 -3 73.30 3.69
14 -2 -2 8.32 1.64
14 -2 -2 9.33 1.39
14 -2 -2 10.16 1.33
14 -2 -2 8.10 1.25
-14 -2 2 11.19 1.30
14 -2 -2 8.53 1.33
14 -2 -2 9.13 1.46
14 -2 -1 6.28 1.32
14 -2 -1 7.36 1.19
14 -2 -1 6.81 1.10
14 -2 -1 6.67 1.23
-14 -2 1 8.80 1.13
14 -2 -1 7.75 1.27
14 -2 -1 8.56 1.41
14 -2 0 54.90 2.88
14 -2 0 57.44 2.98
14 -2 0 51.22 2.87
14 -2 0 56.71 3.11
14 -2 0 57.93 3.26
14 -2 1 27.99 2.06
-14 -2 -1 33.57 2.07
14 -2 1 28.76 2.17
14 -2 1 29.93 2.30
14 -2 2 15.56 1.51
-14 -2 -2 18.81 1.45
-14 -2 -2 16.67 1.41
14 -2 2 17.88 1.63
14 -2 2 14.63 1.48
14 -1 -7 16.08 1.63
14 -1 -7 17.35 1.52
-14 -1 7 18.42 1.45
14 -1 -6 15.86 1.84
14 -1 -6 15.51 1.70
14 -1 -6 18.00 1.60
14 -1 -6 18.85 1.73
-14 -1 6 18.33 1.54
14 -1 -6 15.86 1.70
14 -1 -5 13.56 1.94
14 -1 -5 14.72 1.71
14 -1 -5 14.89 1.57
14 -1 -5 14.88 1.60
-14 -1 5 13.15 1.43
14 -1 -5 14.05 1.69
14 -1 -4 37.04 3.09
14 -1 -4 39.30 2.80
14 -1 -4 37.85 2.54
14 -1 -4 40.76 2.71
-14 -1 4 40.97 2.43
14 -1 -4 39.99 2.84
14 -1 -3 11.79 1.89
14 -1 -3 13.24 1.73
14 -1 -3 13.33 1.66
14 -1 -3 13.64 1.66
-14 -1 3 13.56 1.50
14 -1 -3 10.24 1.48
14 -1 -3 14.05 1.79
14 -1 -2 10.31 1.89
14 -1 -2 10.47 1.45
14 -1 -2 10.10 1.45
14 -1 -2 10.53 1.48
-14 -1 2 12.37 1.37
14 -1 -2 9.13 1.47
14 -1 -2 11.76 1.67
14 -1 -1 9.26 1.80
14 -1 -1 10.38 1.41
14 -1 -1 9.45 1.36
14 -1 -1 8.43 1.30
-14 -1 1 11.62 1.33
14 -1 -1 9.90 1.45
14 -1 -1 9.51 1.46
14 -1 0 1.83 0.96
14 -1 0 3.03 0.87
14 -1 0 2.21 0.85
14 -1 0 2.57 0.86
14 -1 0 2.47 0.79
-14 -1 0 2.92 0.75
14 -1 0 1.91 0.81
14 -1 0 2.79 0.91
14 -1 1 43.70 3.05
14 -1 1 45.56 2.83
14 -1 1 47.41 2.69
-14 -1 -1 47.20 2.43
14 -1 1 43.75 2.77
14 -1 1 46.62 2.83
14 -1 2 13.85 1.59
14 -1 2 9.82 1.41
-14 -1 -2 15.97 1.36
14 -1 2 15.24 1.60
14 -1 2 12.16 1.39
-14 -1 -3 17.45 1.45
14 -1 3 20.99 1.72
14 0 -7 17.19 1.73
14 0 -7 19.21 1.62
14 0 -7 17.94 1.68
-14 0 7 16.91 1.38
14 0 -7 18.04 1.69
14 0 -6 4.30 1.19
14 0 -6 2.84 0.94
14 0 -6 4.54 1.02
14 0 -6 3.16 0.89
-14 0 6 4.32 0.81
14 0 -6 3.78 0.98
14 0 -5 23.74 2.49
14 0 -5 27.45 2.33
14 0 -5 30.74 2.26
14 0 -5 27.17 2.24
14 0 -5 28.87 2.54
14 0 -4 25.46 2.61
14 0 -4 22.81 2.20
14 0 -4 32.18 2.38
14 0 -4 28.42 2.32
-14 0 4 32.57 2.12
14 0 -4 29.37 2.52
14 0 -3 29.29 2.86
14 0 -3 30.16 2.45
14 0 -3 32.49 2.41
14 0 -3 32.66 2.50
-14 0 3 30.57 2.08
14 0 -3 30.99 2.59
14 0 -2 21.80 2.57
14 0 -2 27.34 2.26
14 0 -2 31.31 2.34
14 0 -2 33.02 2.54
-14 0 2 35.38 2.20
14 0 -2 26.93 2.31
14 0 -2 31.75 2.59
14 0 -1 1.33 0.92
14 0 -1 1.26 0.69
14 0 -1 -0.27 0.64
14 0 -1 0.29 0.54
14 0 -1 0.66 0.63
-14 0 1 0.11 0.46
14 0 -1 -0.59 0.91
14 0 -1 0.00 0.44
14 0 -1 1.41 0.64
14 0 0 19.95 2.29
14 0 0 19.34 1.72
14 0 0 17.50 1.83
14 0 0 21.95 1.86
14 0 0 19.79 1.83
-14 0 0 21.26 1.66
14 0 0 19.18 1.56
14 0 0 21.32 1.99
14 0 0 23.40 2.18
14 0 1 27.36 2.48
14 0 1 21.71 2.08
14 0 1 26.25 1.94
-14 0 -1 28.61 1.78
14 0 1 26.90 1.83
14 0 1 25.81 2.11
14 0 1 25.92 2.11
14 0 2 -0.18 0.64
14 0 2 0.02 0.48
14 0 2 0.46 0.62
14 0 2 0.43 0.47
14 0 3 0.47 0.68
14 1 -7 15.22 1.68
14 1 -7 19.64 1.63
14 1 -7 17.60 1.64
-14 1 7 16.81 1.40
14 1 -7 16.68 1.69
14 1 -6 13.38 1.76
14 1 -6 15.78 1.75
14 1 -6 16.85 1.61
14 1 -6 15.30 1.60
-14 1 6 17.35 1.48
14 1 -6 16.19 1.77
14 1 -5 11.71 1.86
14 1 -5 14.89 1.73
14 1 -5 14.03 1.55
14 1 -5 14.14 1.62
-14 1 5 12.14 1.22
14 1 -5 19.00 2.00
14 1 -4 32.98 3.02
14 1 -4 39.57 2.69
14 1 -4 41.39 2.62
14 1 -4 40.13 2.65
-14 1 4 35.67 1.99
14 1 -4 42.55 2.93
14 1 -3 10.07 1.91
14 1 -3 11.98 1.55
14 1 -3 14.80 1.64
14 1 -3 12.59 1.59
-14 1 3 12.61 1.32
14 1 -3 13.49 1.76
14 1 -2 9.98 1.83
14 1 -2 10.11 1.42
14 1 -2 9.29 1.28
14 1 -2 9.23 1.42
-14 1 2 10.03 1.16
14 1 -2 10.47 1.21
14 1 -2 7.70 1.27
14 1 -2 13.43 1.78
14 1 -1 9.66 1.75
14 1 -1 9.22 1.30
14 1 -1 8.47 1.31
14 1 -1 10.62 1.34
14 1 -1 10.58 1.38
14 1 -1 9.96 1.18
14 1 -1 7.15 1.17
14 1 -1 10.88 1.51
14 1 0 -0.34 0.82
14 1 0 0.55 0.80
14 1 0 2.12 0.78
14 1 0 2.89 0.93
-14 1 0 1.84 0.61
14 1 0 2.87 0.92
14 1 0 1.90 0.71
14 1 0 2.09 0.78
14 1 1 39.90 2.86
14 1 1 45.11 2.47
14 1 1 46.78 3.03
14 1 1 42.07 2.31
-14 1 -1 43.89 2.20
14 1 1 47.17 2.51
14 1 1 41.04 2.44
14 1 1 41.51 2.48
14 1 2 14.41 1.40
14 1 2 14.55 1.73
-14 1 -2 11.89 1.21
14 1 2 16.33 1.46
14 1 3 18.14 1.83
14 1 3 21.79 1.63
14 2 -7 3.58 0.84
14 2 -7 2.87 0.71
14 2 -7 2.10 0.69
-14 2 7 2.83 0.66
14 2 -7 3.07 0.87
14 2 -6 9.00 1.52
14 2 -6 8.29 1.14
14 2 -6 9.57 1.20
14 2 -6 8.83 1.18
-14 2 6 8.44 1.07
14 2 -6 9.28 1.36
14 2 -5 2.08 0.91
14 2 -5 2.96 0.88
14 2 -5 3.25 0.78
14 2 -5 4.35 0.97
-14 2 5 2.50 0.70
14 2 -5 3.88 0.99
14 2 -4 4.71 1.33
14 2 -4 4.55 0.99
14 2 -4 5.88 1.02
14 2 -4 7.00 1.16
14 2 -4 6.13 1.23
14 2 -3 59.54 3.85
14 2 -3 61.36 3.12
14 2 -3 72.29 3.28
14 2 -3 67.97 3.29
14 2 -3 64.58 2.73
14 2 -3 58.55 2.95
14 2 -3 67.62 3.56
14 2 -2 6.86 1.47
14 2 -2 10.26 1.27
14 2 -2 7.17 1.13
14 2 -2 9.45 1.13
14 2 -2 7.93 1.15
14 2 -2 8.89 1.35
14 2 -1 7.38 1.56
14 2 -1 8.29 1.10
14 2 -1 6.05 0.99
-14 2 1 6.80 0.98
14 2 -1 5.90 1.06
14 2 -1 7.04 1.01
14 2 -1 7.49 1.22
14 2 0 50.96 3.30
-14 2 0 54.57 2.47
14 2 0 57.43 2.74
14 2 1 27.20 2.25
14 2 1 28.40 1.96
-14 2 -1 30.32 1.84
14 2 1 32.16 2.05
14 2 2 14.82 1.67
-14 2 -2 16.08 1.40
14 2 2 17.40 1.48
14 3 -5 4.32 1.03
-14 3 5 6.42 0.88
14 3 -5 5.80 1.06
14 3 -4 5.78 1.24
-14 3 4 6.49 0.93
14 3 -4 7.26 1.16
14 3 -3 19.61 2.14
14 3 -2 4.81 1.24
14 3 -2 5.85 0.89
14 3 -1 0.69 0.75
14 3 -1 0.94 0.52
-14 3 0 6.96 0.92
14 3 0 8.77 1.07
14 3 1 23.24 1.66
0 0 0 0.00 0.00
TITL Cannabidiol_GV50_old_beta6 in P2(1)
REM P2(1) (#4 in standard setting)
CELL 1.39222 10.439513 10.873877 16.785318 90.0000 95.4480 90.0000
ZERR 4.00 0.000105 0.000143 0.000172 0.0000 0.0010 0.0000
LATT -1
SYMM -x, y+1/2,-z
SFAC C H O
UNIT 84.00 104.00 8.00
TREF
HKLF 4
END
_computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)'
;
_shelx_hkl_checksum 24986
_shelx_res_file
;
cannabidiol_gv50_old_beta6.res created by SHELXL-2014/7
TITL cannabidiol_gv50_old_beta6_a.res in P2(1)
REM Old TITL cannabidiol_gv50_old_beta6_a.res in P2(1)
REM SHELXT solution in P2(1)
REM R1 0.105, Rweak 0.029, Alpha 0.002, Orientation as input
REM Flack x = 0.242 ( 0.047 ) from Parsons' quotients
REM Formula found by SHELXT: C39 O6
CELL 1.39222 10.4395 10.8739 16.7853 90 95.448 90
ZERR 4 0.0001 0.0001 0.0002 0 0.001 0
LATT -1
SYMM -X,0.5+Y,-Z
SFAC C H O
DISP C 0.016 0.008 65.263
DISP H -0 0 0.65
DISP O 0.044 0.027 219.64
UNIT 84 120 8
L.S. 10
PLAN 20
TEMP -150.15
BOND $H
list 4
MORE -1
CONF
fmap 2
acta 149
REM
REM
REM
WGHT 0.049300 0.155300
FVAR 0.92683
O2 3 0.458733 0.271126 0.688014 11.00000 0.02889 0.03369 =
0.04376 -0.01099 0.01019 -0.00525
O3 3 0.229104 0.319092 0.756791 11.00000 0.03489 0.03426 =
0.04088 -0.00040 0.01210 0.00563
O4 3 -0.010068 0.649516 0.856980 11.00000 0.04157 0.03296 =
0.03799 -0.00377 0.01126 0.00460
O1 3 0.890371 0.391861 0.654742 11.00000 0.02766 0.04542 =
0.04809 -0.00587 0.00743 -0.00635
C7 1 0.561911 0.350493 0.702501 11.00000 0.02757 0.02800 =
0.02812 -0.00026 0.00164 -0.00183
C27 1 0.111987 0.478987 0.810280 11.00000 0.02559 0.03020 =
0.02708 -0.00125 0.00269 -0.00140
C28 1 0.062198 0.598240 0.801421 11.00000 0.02726 0.03130 =
0.03089 -0.00280 0.00336 -0.00085
C26 1 0.182349 0.435605 0.749011 11.00000 0.02373 0.03163 =
0.03023 -0.00265 0.00274 -0.00033
C6 1 0.680357 0.324281 0.673149 11.00000 0.02770 0.02790 =
0.02578 0.00074 0.00176 -0.00004
C5 1 0.774974 0.415108 0.685139 11.00000 0.02642 0.03310 =
0.02923 0.00278 0.00027 -0.00106
C29 1 0.082403 0.671948 0.735946 11.00000 0.03117 0.03108 =
0.03862 0.00246 0.00283 -0.00081
C41 1 -0.102034 0.401263 0.962934 11.00000 0.03355 0.03916 =
0.03613 0.00296 0.00770 -0.00192
C37 1 0.091702 0.399985 0.882712 11.00000 0.02973 0.03013 =
0.02724 -0.00024 0.00322 -0.00064
C9 1 0.638104 0.543750 0.758035 11.00000 0.03321 0.02898 =
0.03138 -0.00269 -0.00525 0.00174
C16 1 0.705336 0.204473 0.631810 11.00000 0.02999 0.02993 =
0.03124 -0.00160 0.00747 0.00068
C8 1 0.541431 0.454995 0.746502 11.00000 0.02944 0.03154 =
0.03145 -0.00370 0.00142 0.00196
C10 1 0.753831 0.523785 0.725190 11.00000 0.03000 0.03063 =
0.03614 -0.00033 -0.00491 -0.00327
C38 1 0.169261 0.448008 0.960004 11.00000 0.03114 0.03302 =
0.02818 -0.00038 0.00159 -0.00035
C31 1 0.201565 0.508121 0.682461 11.00000 0.02770 0.04152 =
0.02944 -0.00214 0.00609 -0.00336
C42 1 -0.050711 0.390381 0.893324 11.00000 0.03137 0.03577 =
0.03148 0.00162 0.00262 -0.00421
C30 1 0.153321 0.626966 0.675831 11.00000 0.02955 0.03944 =
0.03107 0.00417 0.00149 -0.00557
C17 1 0.611902 0.186095 0.557970 11.00000 0.04089 0.03920 =
0.02853 -0.00526 0.00838 -0.00052
C18 1 0.562730 0.077929 0.533145 11.00000 0.05028 0.04646 =
0.03420 -0.01287 0.01117 -0.00557
C44 1 0.313087 0.435482 0.957075 11.00000 0.03308 0.04734 =
0.03321 -0.00116 -0.00078 0.00201
C21 1 0.702716 0.092143 0.688488 11.00000 0.03563 0.03009 =
0.04050 0.00110 0.00695 0.00121
C22 1 0.801321 0.103495 0.760242 11.00000 0.03975 0.03568 =
0.05133 0.01027 -0.00134 0.00278
C11 1 0.616572 0.660187 0.803609 11.00000 0.04027 0.03194 =
0.04261 -0.00980 -0.00694 0.00321
C39 1 0.120602 0.382002 1.032361 11.00000 0.04137 0.04352 =
0.02713 0.00307 0.00199 0.00164
C32 1 0.177216 0.707130 0.604828 11.00000 0.04292 0.04821 =
0.03934 0.01122 0.00509 -0.00945
C12 1 0.498743 0.731866 0.770386 11.00000 0.04933 0.03486 =
0.04233 -0.00790 -0.00732 0.00817
C33 1 0.055780 0.746563 0.552801 11.00000 0.05723 0.04418 =
0.04033 0.01111 0.00108 -0.00473
C40 1 -0.018848 0.416771 1.040745 11.00000 0.04331 0.04907 =
0.03108 0.00144 0.00927 -0.00032
C13 1 0.478571 0.850210 0.814374 11.00000 0.05014 0.03063 =
0.04271 -0.00457 0.00062 0.00490
C23 1 0.764074 0.123715 0.832280 11.00000 0.05901 0.04353 =
0.04478 0.00683 -0.00652 -0.00218
C20 1 0.715238 -0.024820 0.638911 11.00000 0.05745 0.03000 =
0.06205 -0.00404 0.01285 0.00520
C43 1 -0.245374 0.397382 0.967031 11.00000 0.03546 0.06895 =
0.04840 0.00414 0.01364 -0.00371
C34 1 -0.014766 0.640815 0.509154 11.00000 0.04880 0.04260 =
0.04291 0.00681 0.00217 -0.00068
C14 1 0.359742 0.919937 0.782140 11.00000 0.06414 0.04515 =
0.07558 -0.01668 -0.01412 0.01813
C25 1 0.472138 0.067773 0.458073 11.00000 0.07314 0.06852 =
0.04009 -0.02362 0.00366 -0.01551
C45 1 0.368709 0.308956 0.955612 11.00000 0.04135 0.05578 =
0.05914 -0.00743 -0.00630 0.01446
C46 1 0.386845 0.534410 0.957360 11.00000 0.03655 0.06128 =
0.08325 0.00002 0.00703 -0.00798
C19 1 0.599405 -0.039214 0.576706 11.00000 0.06857 0.03691 =
0.05769 -0.01561 0.01216 -0.00877
C15 1 0.340097 1.040081 0.824096 11.00000 0.06802 0.03843 =
0.05805 -0.00064 0.01426 0.01335
C35 1 -0.133840 0.681950 0.455762 11.00000 0.05988 0.05113 =
0.05926 0.00519 -0.01124 0.00420
C24 1 0.941481 0.094287 0.746236 11.00000 0.03964 0.07829 =
0.07944 0.02256 -0.00156 0.01082
C36 1 -0.199512 0.575730 0.409736 11.00000 0.05836 0.06066 =
0.06923 0.00058 -0.00704 0.00055
H40A 2 -0.025275 0.503690 1.060925 11.00000 0.04306
H38 2 0.148818 0.537980 0.965043 11.00000 0.02720
H8 2 0.458807 0.465722 0.768792 11.00000 0.04167
H33A 2 -0.005200 0.789077 0.585975 11.00000 0.06195
H39A 2 0.176764 0.401222 1.081277 11.00000 0.04054
H21 2 0.616939 0.089172 0.708434 11.00000 0.03295
H33B 2 0.085204 0.807235 0.514783 11.00000 0.06288
H19A 2 0.527117 -0.070645 0.600845 11.00000 0.05951
H42 2 -0.106742 0.373800 0.846133 11.00000 0.03466
H32A 2 0.235369 0.665397 0.567737 11.00000 0.05464
H37 2 0.124911 0.315388 0.871242 11.00000 0.02957
H16 2 0.791676 0.210162 0.612056 11.00000 0.03002
H39B 2 0.127046 0.289541 1.024661 11.00000 0.04636
H40B 2 -0.055005 0.365273 1.083493 11.00000 0.05040
H17 2 0.590673 0.264268 0.527238 11.00000 0.04701
H31 2 0.250965 0.475942 0.640825 11.00000 0.04309
H45A 2 0.356480 0.255929 1.003860 11.00000 0.09222
H20A 2 0.797958 -0.017605 0.613212 11.00000 0.05979
H34A 2 -0.041582 0.578202 0.549781 11.00000 0.05009
H10 2 0.822787 0.585134 0.731097 11.00000 0.03884
H11A 2 0.607687 0.638695 0.861547 11.00000 0.04960
H13A 2 0.550148 0.902173 0.811747 11.00000 0.06863
H1 2 0.943238 0.444106 0.672682 11.00000 0.05387
H13B 2 0.473048 0.835021 0.872300 11.00000 0.05808
H29 2 0.048826 0.756395 0.732736 11.00000 0.04325
H24A 2 0.960841 0.150427 0.704647 11.00000 0.06970
H24B 2 0.992866 0.105522 0.792821 11.00000 0.07736
H3 2 0.289876 0.306581 0.728410 11.00000 0.04607
H35A 2 -0.111183 0.745976 0.419269 11.00000 0.06343
H35B 2 -0.189621 0.721111 0.488834 11.00000 0.06800
H46A 2 0.483499 0.524437 0.961634 11.00000 0.07090
H43A 2 -0.282880 0.468771 0.989806 11.00000 0.07407
H12A 2 0.416210 0.679337 0.768584 11.00000 0.07327
H46B 2 0.344016 0.613134 0.958187 11.00000 0.09033
H12B 2 0.499312 0.749935 0.715287 11.00000 0.06978
H15A 2 0.342196 1.030891 0.883321 11.00000 0.07987
H19B 2 0.616510 -0.103929 0.537338 11.00000 0.07376
H32B 2 0.223491 0.780713 0.625732 11.00000 0.06443
H14A 2 0.365126 0.934759 0.719932 11.00000 0.11313
H34B 2 0.048344 0.596309 0.474456 11.00000 0.05165
H20B 2 0.720891 -0.098142 0.674693 11.00000 0.05750
H43B 2 -0.292889 0.386072 0.914619 11.00000 0.06015
H23A 2 0.675850 0.131820 0.840328 11.00000 0.05899
H23B 2 0.818374 0.130224 0.878366 11.00000 0.06122
H2 2 0.475054 0.222611 0.649562 11.00000 0.04386
H4 2 -0.035564 0.592761 0.886431 11.00000 0.05426
H43C 2 -0.263650 0.331386 1.003034 11.00000 0.07336
H25A 2 0.442548 0.155641 0.437713 11.00000 0.07546
H15B 2 0.415357 1.097227 0.814839 11.00000 0.08191
H36A 2 -0.142252 0.537871 0.371974 11.00000 0.06292
H25B 2 0.512102 0.019797 0.420703 11.00000 0.06872
H25C 2 0.401125 0.024402 0.468415 11.00000 0.07304
H45B 2 0.463286 0.312013 0.951464 11.00000 0.06755
H11B 2 0.692467 0.713480 0.805691 11.00000 0.07180
H45C 2 0.331074 0.263514 0.914175 11.00000 0.07837
H36B 2 -0.221830 0.515157 0.447802 11.00000 0.07569
H14B 2 0.280092 0.876771 0.787594 11.00000 0.12525
H36C 2 -0.284239 0.610552 0.376590 11.00000 0.08776
H24C 2 0.954524 0.002563 0.722834 11.00000 0.09344
H15C 2 0.261224 1.085302 0.807986 11.00000 0.09772
HKLF 4
REM cannabidiol_gv50_old_beta6_a.res in P2(1)
REM R1 = 0.0322 for 9859 Fo > 4sig(Fo) and 0.0336 for all 10203 data
REM 655 parameters refined using 1 restraints
END
WGHT 0.0493 0.1553
REM Highest difference peak 0.232, deepest hole -0.126, 1-sigma level 0.027
Q1 1 -0.0619 0.7168 0.5466 11.00000 0.05 0.23
Q2 1 0.0705 0.6763 0.5317 11.00000 0.05 0.19
Q3 1 -0.0735 0.4217 0.9295 11.00000 0.05 0.16
Q4 1 0.0290 0.3978 0.8912 11.00000 0.05 0.16
Q5 1 0.6256 0.3379 0.6845 11.00000 0.05 0.15
Q6 1 0.1245 0.4236 0.9187 11.00000 0.05 0.15
Q7 1 0.6856 0.2745 0.6507 11.00000 0.05 0.15
Q8 1 0.6980 0.5379 0.7412 11.00000 0.05 0.14
Q9 1 0.1900 0.4838 0.7156 11.00000 0.05 0.14
Q10 1 0.7524 0.1020 0.7195 11.00000 0.05 0.14
Q11 1 0.2946 0.9561 0.8044 11.00000 0.05 0.14
Q12 1 0.2450 0.4456 0.9571 11.00000 0.05 0.14
Q13 1 -0.1720 0.3996 0.9673 11.00000 0.05 0.13
Q14 1 0.0490 0.4076 1.0372 11.00000 0.05 0.13
Q15 1 0.1438 0.4069 0.9989 11.00000 0.05 0.13
Q16 1 0.1018 0.4381 0.8515 11.00000 0.05 0.13
Q17 1 0.8038 0.1533 0.7967 11.00000 0.05 0.12
Q18 1 0.0821 0.5354 0.8048 11.00000 0.05 0.12
Q19 1 0.6263 0.6047 0.7780 11.00000 0.05 0.12
Q20 1 0.5524 0.4075 0.7279 11.00000 0.05 0.12
;
_shelx_res_checksum 83494
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
O O2 0.45873(9) 0.27113(11) 0.68801(7) 0.0350(2) Uani d 1
O O3 0.22910(10) 0.31909(11) 0.75679(7) 0.0361(2) Uani d 1
O O4 -0.01007(11) 0.64952(12) 0.85698(7) 0.0370(2) Uani d 1
O O1 0.89037(10) 0.39186(12) 0.65474(7) 0.0401(2) Uani d 1
C C7 0.56191(12) 0.35049(13) 0.70250(8) 0.0280(2) Uani d 1
C C27 0.11199(12) 0.47899(13) 0.81028(7) 0.0276(2) Uani d 1
C C28 0.06220(12) 0.59824(14) 0.80142(8) 0.0298(2) Uani d 1
C C26 0.18235(11) 0.43560(13) 0.74901(7) 0.0285(2) Uani d 1
C C6 0.68036(12) 0.32428(13) 0.67315(7) 0.0272(2) Uani d 1
C C5 0.77497(12) 0.41511(14) 0.68514(8) 0.0297(2) Uani d 1
C C29 0.08240(13) 0.67195(14) 0.73595(9) 0.0337(3) Uani d 1
C C41 -0.10203(14) 0.40126(16) 0.96293(9) 0.0360(3) Uani d 1
C C37 0.09170(12) 0.39998(14) 0.88271(7) 0.0290(2) Uani d 1
C C9 0.63810(13) 0.54375(14) 0.75803(8) 0.0317(3) Uani d 1
C C16 0.70534(12) 0.20447(14) 0.63181(8) 0.0301(2) Uani d 1
C C8 0.54143(13) 0.45499(14) 0.74650(8) 0.0309(2) Uani d 1
C C10 0.75383(13) 0.52378(14) 0.72519(8) 0.0328(3) Uani d 1
C C38 0.16926(12) 0.44801(14) 0.96000(8) 0.0309(3) Uani d 1
C C31 0.20157(13) 0.50812(15) 0.68246(8) 0.0327(3) Uani d 1
C C42 -0.05071(13) 0.39038(15) 0.89332(8) 0.0329(3) Uani d 1
C C30 0.15332(13) 0.62697(15) 0.67583(8) 0.0334(3) Uani d 1
C C17 0.61190(15) 0.18610(16) 0.55797(8) 0.0359(3) Uani d 1
C C18 0.56273(18) 0.07793(18) 0.53315(9) 0.0432(4) Uani d 1
C C44 0.31309(14) 0.43548(17) 0.95708(9) 0.0381(3) Uani d 1
C C21 0.70272(14) 0.09214(15) 0.68849(9) 0.0352(3) Uani d 1
C C22 0.80132(16) 0.10349(17) 0.76024(11) 0.0426(3) Uani d 1
C C11 0.61657(16) 0.66019(16) 0.80361(10) 0.0390(3) Uani d 1
C C39 0.12060(15) 0.38200(17) 1.03236(8) 0.0374(3) Uani d 1
C C32 0.17722(17) 0.70713(19) 0.60483(10) 0.0434(4) Uani d 1
C C12 0.49874(18) 0.73187(17) 0.77039(10) 0.0429(3) Uani d 1
C C33 0.0558(2) 0.74656(19) 0.55280(11) 0.0475(4) Uani d 1
C C40 -0.01885(16) 0.41677(18) 1.04074(9) 0.0408(3) Uani d 1
C C13 0.47857(18) 0.85021(16) 0.81437(10) 0.0414(3) Uani d 1
C C23 0.7641(2) 0.12371(19) 0.83228(11) 0.0498(4) Uani d 1
C C20 0.7152(2) -0.02482(18) 0.63891(13) 0.0494(4) Uani d 1
C C43 -0.24537(17) 0.3974(2) 0.96703(12) 0.0503(4) Uani d 1
C C34 -0.01477(18) 0.64082(19) 0.50915(11) 0.0449(4) Uani d 1
C C14 0.3597(2) 0.9199(2) 0.78214(16) 0.0630(6) Uani d 1
C C25 0.4721(3) 0.0678(3) 0.45807(12) 0.0607(6) Uani d 1
C C45 0.36871(18) 0.3090(2) 0.95561(14) 0.0528(5) Uani d 1
C C46 0.38685(19) 0.5344(3) 0.95736(16) 0.0603(5) Uani d 1
C C19 0.5994(2) -0.03921(19) 0.57671(13) 0.0540(4) Uani d 1
C C15 0.3401(2) 1.0401(2) 0.82410(13) 0.0543(5) Uani d 1
C C35 -0.1338(2) 0.6820(2) 0.45576(15) 0.0578(5) Uani d 1
C C24 0.9415(2) 0.0943(3) 0.74624(18) 0.0663(6) Uani d 1
C C36 -0.1995(2) 0.5757(3) 0.40974(17) 0.0636(6) Uani d 1
H H40A -0.025(2) 0.504(2) 1.0609(14) 0.043(5) Uiso d 1
H H38 0.1488(18) 0.538(2) 0.9650(11) 0.027(4) Uiso d 1
H H8 0.459(2) 0.466(2) 0.7688(13) 0.042(5) Uiso d 1
H H33A -0.005(3) 0.789(3) 0.5860(17) 0.062(7) Uiso d 1
H H39A 0.177(2) 0.401(2) 1.0813(13) 0.041(5) Uiso d 1
H H21 0.617(2) 0.089(2) 0.7084(12) 0.033(5) Uiso d 1
H H33B 0.085(3) 0.807(3) 0.5148(17) 0.063(8) Uiso d 1
H H19A 0.527(3) -0.071(3) 0.6008(16) 0.060(7) Uiso d 1
H H42 -0.107(2) 0.374(2) 0.8461(12) 0.035(5) Uiso d 1
H H32A 0.235(3) 0.665(3) 0.5677(16) 0.055(7) Uiso d 1
H H37 0.1249(18) 0.315(2) 0.8712(11) 0.030(4) Uiso d 1
H H16 0.7917(18) 0.210(2) 0.6121(11) 0.030(4) Uiso d 1
H H39B 0.127(2) 0.290(3) 1.0247(14) 0.046(6) Uiso d 1
H H40B -0.055(2) 0.365(3) 1.0835(15) 0.050(6) Uiso d 1
H H17 0.591(2) 0.264(3) 0.5272(15) 0.047(6) Uiso d 1
H H31 0.251(2) 0.476(2) 0.6408(13) 0.043(5) Uiso d 1
H H45A 0.356(4) 0.256(4) 1.004(2) 0.092(11) Uiso d 1
H H20A 0.798(3) -0.018(3) 0.6132(16) 0.060(7) Uiso d 1
H H34A -0.042(2) 0.578(3) 0.5498(15) 0.050(6) Uiso d 1
H H10 0.823(2) 0.585(2) 0.7311(13) 0.039(5) Uiso d 1
H H11A 0.608(2) 0.639(3) 0.8615(15) 0.050(6) Uiso d 1
H H13A 0.550(3) 0.902(3) 0.8117(18) 0.069(8) Uiso d 1
H H1 0.943(3) 0.444(3) 0.6727(15) 0.054(7) Uiso d 1
H H13B 0.473(3) 0.835(3) 0.8723(17) 0.058(7) Uiso d 1
H H29 0.049(2) 0.756(2) 0.7327(13) 0.043(6) Uiso d 1
H H24A 0.961(3) 0.150(3) 0.7046(19) 0.070(8) Uiso d 1
H H24B 0.993(3) 0.106(3) 0.793(2) 0.077(9) Uiso d 1
H H3 0.290(2) 0.307(2) 0.7284(14) 0.046(6) Uiso d 1
H H35A -0.111(3) 0.746(3) 0.4193(18) 0.063(8) Uiso d 1
H H35B -0.190(3) 0.721(3) 0.4888(19) 0.068(8) Uiso d 1
H H46A 0.483(3) 0.524(3) 0.9616(18) 0.071(9) Uiso d 1
H H43A -0.283(3) 0.469(3) 0.9898(19) 0.074(9) Uiso d 1
H H12A 0.416(3) 0.679(3) 0.7686(19) 0.073(9) Uiso d 1
H H46B 0.344(4) 0.613(4) 0.958(2) 0.090(11) Uiso d 1
H H12B 0.499(3) 0.750(3) 0.7153(19) 0.070(8) Uiso d 1
H H15A 0.342(3) 1.031(3) 0.883(2) 0.080(10) Uiso d 1
H H19B 0.617(3) -0.104(3) 0.537(2) 0.074(9) Uiso d 1
H H32B 0.223(3) 0.781(3) 0.6257(17) 0.064(8) Uiso d 1
H H14A 0.365(4) 0.935(4) 0.720(3) 0.113(14) Uiso d 1
H H34B 0.048(2) 0.596(3) 0.4745(15) 0.052(6) Uiso d 1
H H20B 0.721(3) -0.098(3) 0.6747(16) 0.057(7) Uiso d 1
H H43B -0.293(3) 0.386(3) 0.9146(17) 0.060(7) Uiso d 1
H H23A 0.676(3) 0.132(3) 0.8403(16) 0.059(7) Uiso d 1
H H23B 0.818(3) 0.130(3) 0.8784(17) 0.061(7) Uiso d 1
H H2 0.475(2) 0.223(2) 0.6496(14) 0.044(5) Uiso d 1
H H4 -0.036(3) 0.593(3) 0.8864(16) 0.054(7) Uiso d 1
H H43C -0.264(3) 0.331(3) 1.0030(19) 0.073(9) Uiso d 1
H H25A 0.443(3) 0.156(4) 0.438(2) 0.075(9) Uiso d 1
H H15B 0.415(3) 1.097(4) 0.815(2) 0.082(10) Uiso d 1
H H36A -0.142(3) 0.538(3) 0.3720(17) 0.063(8) Uiso d 1
H H25B 0.512(3) 0.020(3) 0.4207(19) 0.069(8) Uiso d 1
H H25C 0.401(3) 0.024(3) 0.4684(19) 0.073(9) Uiso d 1
H H45B 0.463(3) 0.312(3) 0.9515(18) 0.068(8) Uiso d 1
H H11B 0.692(3) 0.713(3) 0.8057(18) 0.072(8) Uiso d 1
H H45C 0.331(3) 0.264(3) 0.914(2) 0.078(9) Uiso d 1
H H36B -0.222(3) 0.515(4) 0.448(2) 0.076(9) Uiso d 1
H H14B 0.280(5) 0.877(5) 0.788(3) 0.125(16) Uiso d 1
H H36C -0.284(4) 0.611(4) 0.377(2) 0.088(11) Uiso d 1
H H24C 0.955(4) 0.003(4) 0.723(2) 0.093(11) Uiso d 1
H H15C 0.261(4) 1.085(4) 0.808(2) 0.098(12) Uiso d 1
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
O2 0.0289(4) 0.0337(5) 0.0438(5) -0.0053(4) 0.0102(4) -0.0110(4)
O3 0.0349(5) 0.0343(6) 0.0409(5) 0.0056(4) 0.0121(4) -0.0004(4)
O4 0.0416(5) 0.0330(6) 0.0380(5) 0.0046(4) 0.0113(4) -0.0038(4)
O1 0.0277(4) 0.0454(7) 0.0481(6) -0.0063(4) 0.0074(4) -0.0059(5)
C7 0.0276(5) 0.0280(6) 0.0281(5) -0.0018(4) 0.0016(4) -0.0003(4)
C27 0.0256(5) 0.0302(6) 0.0271(5) -0.0014(4) 0.0027(4) -0.0013(4)
C28 0.0273(5) 0.0313(7) 0.0309(5) -0.0008(5) 0.0034(4) -0.0028(5)
C26 0.0237(5) 0.0316(7) 0.0302(5) -0.0003(4) 0.0027(4) -0.0026(5)
C6 0.0277(5) 0.0279(6) 0.0258(5) 0.0000(4) 0.0018(4) 0.0007(4)
C5 0.0264(5) 0.0331(7) 0.0292(5) -0.0011(5) 0.0003(4) 0.0028(5)
C29 0.0312(6) 0.0311(7) 0.0386(6) -0.0008(5) 0.0028(5) 0.0025(5)
C41 0.0335(6) 0.0392(8) 0.0361(6) -0.0019(5) 0.0077(5) 0.0030(6)
C37 0.0297(5) 0.0301(7) 0.0272(5) -0.0006(5) 0.0032(4) -0.0002(4)
C9 0.0332(6) 0.0290(7) 0.0314(6) 0.0017(5) -0.0052(5) -0.0027(5)
C16 0.0300(6) 0.0299(7) 0.0312(5) 0.0007(5) 0.0075(4) -0.0016(5)
C8 0.0294(5) 0.0315(7) 0.0315(5) 0.0020(5) 0.0014(4) -0.0037(5)
C10 0.0300(6) 0.0306(7) 0.0361(6) -0.0033(5) -0.0049(5) -0.0003(5)
C38 0.0311(6) 0.0330(7) 0.0282(5) -0.0004(5) 0.0016(4) -0.0004(5)
C31 0.0277(5) 0.0415(8) 0.0294(5) -0.0034(5) 0.0061(4) -0.0021(5)
C42 0.0314(6) 0.0358(7) 0.0315(6) -0.0042(5) 0.0026(5) 0.0016(5)
C30 0.0295(6) 0.0394(8) 0.0311(6) -0.0056(5) 0.0015(4) 0.0042(5)
C17 0.0409(7) 0.0392(8) 0.0285(6) -0.0005(6) 0.0084(5) -0.0053(5)
C18 0.0503(8) 0.0465(10) 0.0342(6) -0.0056(7) 0.0112(6) -0.0129(6)
C44 0.0331(6) 0.0473(9) 0.0332(6) 0.0020(6) -0.0008(5) -0.0012(6)
C21 0.0356(6) 0.0301(7) 0.0405(7) 0.0012(5) 0.0070(5) 0.0011(5)
C22 0.0397(7) 0.0357(8) 0.0513(8) 0.0028(6) -0.0013(6) 0.0103(7)
C11 0.0403(7) 0.0319(8) 0.0426(7) 0.0032(6) -0.0069(6) -0.0098(6)
C39 0.0414(7) 0.0435(9) 0.0271(5) 0.0016(6) 0.0020(5) 0.0031(5)
C32 0.0429(7) 0.0482(10) 0.0393(7) -0.0094(7) 0.0051(6) 0.0112(7)
C12 0.0493(8) 0.0349(8) 0.0423(8) 0.0082(6) -0.0073(6) -0.0079(6)
C33 0.0572(9) 0.0442(10) 0.0403(8) -0.0047(7) 0.0011(7) 0.0111(7)
C40 0.0433(7) 0.0491(10) 0.0311(6) -0.0003(6) 0.0093(5) 0.0014(6)
C13 0.0501(8) 0.0306(8) 0.0427(7) 0.0049(6) 0.0006(6) -0.0046(6)
C23 0.0590(10) 0.0435(10) 0.0448(8) -0.0022(8) -0.0065(7) 0.0068(7)
C20 0.0574(10) 0.0300(8) 0.0621(10) 0.0052(7) 0.0128(8) -0.0040(7)
C43 0.0355(7) 0.0689(13) 0.0484(8) -0.0037(8) 0.0136(6) 0.0041(9)
C34 0.0488(8) 0.0426(9) 0.0429(8) -0.0007(7) 0.0022(6) 0.0068(7)
C14 0.0641(12) 0.0452(12) 0.0756(14) 0.0181(9) -0.0141(10) -0.0167(10)
C25 0.0731(13) 0.0685(15) 0.0401(8) -0.0155(11) 0.0037(9) -0.0236(9)
C45 0.0413(8) 0.0558(12) 0.0591(10) 0.0145(8) -0.0063(7) -0.0074(9)
C46 0.0366(8) 0.0613(14) 0.0833(15) -0.0080(8) 0.0070(9) 0.0000(11)
C19 0.0686(12) 0.0369(10) 0.0577(10) -0.0088(8) 0.0122(9) -0.0156(8)
C15 0.0680(12) 0.0384(10) 0.0581(10) 0.0133(9) 0.0143(9) -0.0006(8)
C35 0.0599(11) 0.0511(12) 0.0593(11) 0.0042(9) -0.0112(9) 0.0052(9)
C24 0.0396(9) 0.0783(17) 0.0794(15) 0.0108(10) -0.0016(9) 0.0226(14)
C36 0.0584(12) 0.0607(14) 0.0692(13) 0.0005(10) -0.0070(10) 0.0006(11)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0160 0.0080 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0440 0.0270 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
0 6 7 0.0893
-1 1 12 0.0936
0 -7 6 0.0734
3 -4 -9 0.0577
0 8 -2 0.0799
-7 -1 4 0.1062
7 0 -5 0.0730
0 -8 0 0.0688
-2 -7 -6 0.0777
1 -1 -12 0.0643
-1 6 7 0.0802
-2 5 -9 0.1101
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
C7 O2 H2 107.9(16)
C26 O3 H3 112.3(18)
C28 O4 H4 108.9(19)
C5 O1 H1 108.4(18)
O2 C7 C6 120.59(12)
C8 C7 O2 116.69(12)
C8 C7 C6 122.72(12)
C28 C27 C26 116.69(12)
C28 C27 C37 122.01(11)
C26 C27 C37 121.29(13)
O4 C28 C27 121.79(13)
O4 C28 C29 115.90(13)
C29 C28 C27 122.32(12)
O3 C26 C27 116.85(12)
O3 C26 C31 121.68(12)
C31 C26 C27 121.46(13)
C7 C6 C16 122.20(12)
C5 C6 C7 116.12(12)
C5 C6 C16 121.68(11)
O1 C5 C6 116.65(13)
O1 C5 C10 121.43(13)
C10 C5 C6 121.92(12)
C28 C29 C30 119.97(14)
C28 C29 H29 120.1(13)
C30 C29 H29 119.9(13)
C42 C41 C40 121.44(13)
C42 C41 C43 121.36(14)
C43 C41 C40 117.19(13)
C27 C37 C38 112.15(11)
C27 C37 H37 106.6(11)
C38 C37 H37 107.8(11)
C42 C37 C27 110.20(11)
C42 C37 C38 111.34(10)
C42 C37 H37 108.5(11)
C8 C9 C11 120.68(13)
C10 C9 C8 118.71(13)
C10 C9 C11 120.60(14)
C6 C16 C17 111.32(12)
C6 C16 C21 112.57(11)
C6 C16 H16 107.6(12)
C17 C16 C21 110.52(12)
C17 C16 H16 105.6(11)
C21 C16 H16 108.9(12)
C7 C8 C9 119.71(12)
C7 C8 H8 119.2(14)
C9 C8 H8 121.1(14)
C5 C10 C9 120.58(13)
C5 C10 H10 118.7(13)
C9 C10 H10 120.7(13)
C37 C38 H38 107.4(11)
C44 C38 C37 112.51(11)
C44 C38 C39 112.76(12)
C44 C38 H38 108.0(11)
C39 C38 C37 108.52(11)
C39 C38 H38 107.4(11)
C26 C31 H31 119.9(15)
C30 C31 C26 120.74(12)
C30 C31 H31 119.4(15)
C41 C42 C37 125.11(12)
C41 C42 H42 118.5(13)
C37 C42 H42 116.4(12)
C29 C30 C32 120.33(15)
C31 C30 C29 118.81(13)
C31 C30 C32 120.86(14)
C16 C17 H17 113.6(14)
C18 C17 C16 124.76(16)
C18 C17 H17 121.6(14)
C17 C18 C25 121.23(19)
C17 C18 C19 121.57(16)
C19 C18 C25 117.16(18)
C45 C44 C38 118.15(15)
C46 C44 C38 120.39(17)
C46 C44 C45 121.46(17)
C16 C21 H21 107.7(13)
C22 C21 C16 111.96(13)
C22 C21 C20 114.41(15)
C22 C21 H21 107.7(12)
C20 C21 C16 108.26(13)
C20 C21 H21 106.5(13)
C23 C22 C21 120.27(16)
C23 C22 C24 121.83(19)
C24 C22 C21 117.87(18)
C9 C11 C12 113.57(12)
C9 C11 H11A 109.0(16)
C9 C11 H11B 110.9(19)
C12 C11 H11A 109.1(14)
C12 C11 H11B 110(2)
H11A C11 H11B 104(2)
C38 C39 H39A 110.1(14)
C38 C39 H39B 109.3(14)
C40 C39 C38 110.32(12)
C40 C39 H39A 111.6(13)
C40 C39 H39B 109.4(14)
H39A C39 H39B 105.9(19)
C30 C32 C33 114.85(14)
C30 C32 H32A 112.2(16)
C30 C32 H32B 107.4(17)
C33 C32 H32A 106.6(15)
C33 C32 H32B 109.2(18)
H32A C32 H32B 106(2)
C11 C12 H12A 111.8(19)
C11 C12 H12B 112.7(19)
C13 C12 C11 113.86(13)
C13 C12 H12A 109.4(18)
C13 C12 H12B 108(2)
H12A C12 H12B 100(3)
C32 C33 H33A 110.4(16)
C32 C33 H33B 105.3(17)
C34 C33 C32 113.65(17)
C34 C33 H33A 108.3(18)
C34 C33 H33B 111.2(17)
H33A C33 H33B 108(2)
C41 C40 C39 111.66(12)
C41 C40 H40A 110.2(13)
C41 C40 H40B 109.2(14)
C39 C40 H40A 111.0(13)
C39 C40 H40B 110.6(14)
H40A C40 H40B 103.9(19)
C12 C13 C14 113.65(15)
C12 C13 H13A 109.9(19)
C12 C13 H13B 111.2(18)
C14 C13 H13A 108(2)
C14 C13 H13B 108.2(17)
H13A C13 H13B 105(2)
C22 C23 H23A 121.3(17)
C22 C23 H23B 124.9(18)
H23A C23 H23B 114(2)
C21 C20 H20A 106.8(18)
C21 C20 H20B 109.9(16)
C19 C20 C21 110.68(15)
C19 C20 H20A 111.8(16)
C19 C20 H20B 109.1(16)
H20A C20 H20B 108(2)
C41 C43 H43A 116(2)
C41 C43 H43B 112.6(16)
C41 C43 H43C 107.7(19)
H43A C43 H43B 106(3)
H43A C43 H43C 104(3)
H43B C43 H43C 111(3)
C33 C34 C35 113.08(17)
C33 C34 H34A 109.5(14)
C33 C34 H34B 108.6(15)
C35 C34 H34A 109.1(14)
C35 C34 H34B 109.3(14)
H34A C34 H34B 107(2)
C13 C14 H14A 108(2)
C13 C14 H14B 114(3)
C15 C14 C13 114.30(18)
C15 C14 H14A 110(3)
C15 C14 H14B 103(3)
H14A C14 H14B 107(4)
C18 C25 H25A 110.3(18)
C18 C25 H25B 108.3(19)
C18 C25 H25C 110(2)
H25A C25 H25B 115(3)
H25A C25 H25C 108(3)
H25B C25 H25C 105(3)
C44 C45 H45A 116(2)
C44 C45 H45B 111(2)
C44 C45 H45C 112(2)
H45A C45 H45B 106(3)
H45A C45 H45C 103(3)
H45B C45 H45C 109(3)
C44 C46 H46A 119(2)
C44 C46 H46B 117(2)
H46A C46 H46B 124(3)
C18 C19 C20 113.24(16)
C18 C19 H19A 109.6(18)
C18 C19 H19B 109(2)
C20 C19 H19A 110.7(16)
C20 C19 H19B 110.3(19)
H19A C19 H19B 103(3)
C14 C15 H15A 113(2)
C14 C15 H15B 108(2)
C14 C15 H15C 117(3)
H15A C15 H15B 105(3)
H15A C15 H15C 105(3)
H15B C15 H15C 107(3)
C34 C35 H35A 110.3(17)
C34 C35 H35B 107.5(19)
C36 C35 C34 112.3(2)
C36 C35 H35A 110.5(18)
C36 C35 H35B 112(2)
H35A C35 H35B 104(3)
C22 C24 H24A 110.2(18)
C22 C24 H24B 111(2)
C22 C24 H24C 106(2)
H24A C24 H24B 113(3)
H24A C24 H24C 106(3)
H24B C24 H24C 110(3)
C35 C36 H36A 111.6(18)
C35 C36 H36B 108(2)
C35 C36 H36C 108(2)
H36A C36 H36B 110(3)
H36A C36 H36C 109(3)
H36B C36 H36C 110(3)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
O2 C7 1.3836(16)
O2 H2 0.86(3)
O3 C26 1.3595(18)
O3 H3 0.84(3)
O4 C28 1.3723(16)
O4 H4 0.85(3)
O1 C5 1.3756(17)
O1 H1 0.83(3)
C7 C6 1.4031(18)
C7 C8 1.3829(19)
C27 C28 1.400(2)
C27 C26 1.4011(17)
C27 C37 1.5198(18)
C28 C29 1.392(2)
C26 C31 1.3973(19)
C6 C5 1.3978(18)
C6 C16 1.510(2)
C5 C10 1.388(2)
C29 C30 1.395(2)
C29 H29 0.98(3)
C41 C42 1.3361(19)
C41 C40 1.508(2)
C41 C43 1.505(2)
C37 C38 1.5530(17)
C37 C42 1.5176(18)
C37 H37 1.01(2)
C9 C8 1.397(2)
C9 C10 1.392(2)
C9 C11 1.507(2)
C16 C17 1.516(2)
C16 C21 1.550(2)
C16 H16 0.991(19)
C8 H8 0.98(2)
C10 H10 0.98(2)
C38 C44 1.5131(19)
C38 C39 1.5380(19)
C38 H38 1.01(2)
C31 C30 1.388(2)
C31 H31 0.97(2)
C42 H42 0.96(2)
C30 C32 1.516(2)
C17 C18 1.334(2)
C17 H17 1.01(3)
C18 C25 1.506(3)
C18 C19 1.500(3)
C44 C45 1.494(3)
C44 C46 1.323(3)
C21 C22 1.513(2)
C21 C20 1.532(2)
C21 H21 0.99(2)
C22 C23 1.323(3)
C22 C24 1.507(3)
C11 C12 1.517(2)
C11 H11A 1.01(3)
C11 H11B 0.98(3)
C39 C40 1.523(2)
C39 H39A 0.98(2)
C39 H39B 1.02(3)
C32 C33 1.531(3)
C32 H32A 1.02(3)
C32 H32B 0.98(3)
C12 C13 1.508(2)
C12 H12A 1.03(3)
C12 H12B 0.95(3)
C33 C34 1.516(3)
C33 H33A 1.00(3)
C33 H33B 0.99(3)
C40 H40A 1.01(3)
C40 H40B 1.01(3)
C13 C14 1.510(3)
C13 H13A 0.94(3)
C13 H13B 0.99(3)
C23 H23A 0.95(3)
C23 H23B 0.92(3)
C20 C19 1.529(3)
C20 H20A 1.00(3)
C20 H20B 1.00(3)
C43 H43A 0.96(4)
C43 H43B 0.98(3)
C43 H43C 0.97(4)
C34 C35 1.529(3)
C34 H34A 1.02(3)
C34 H34B 1.04(3)
C14 C15 1.507(3)
C14 H14A 1.06(4)
C14 H14B 0.97(5)
C25 H25A 1.05(4)
C25 H25B 0.94(3)
C25 H25C 0.91(4)
C45 H45A 1.01(4)
C45 H45B 1.00(3)
C45 H45C 0.91(4)
C46 H46A 1.01(3)
C46 H46B 0.97(4)
C19 H19A 0.95(3)
C19 H19B 0.99(3)
C15 H15A 1.00(3)
C15 H15B 1.03(4)
C15 H15C 0.97(4)
C35 C36 1.517(4)
C35 H35A 0.97(3)
C35 H35B 0.94(3)
C24 H24A 0.96(3)
C24 H24B 0.91(4)
C24 H24C 1.09(4)
C36 H36A 1.00(3)
C36 H36B 0.96(4)
C36 H36C 1.07(4)
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
O2 C7 C6 C5 174.74(12)
O2 C7 C6 C16 -5.95(19)
O2 C7 C8 C9 -175.02(12)
O3 C26 C31 C30 -179.81(12)
O4 C28 C29 C30 -179.15(13)
O1 C5 C10 C9 -177.67(13)
C7 C6 C5 O1 -178.32(12)
C7 C6 C5 C10 1.27(18)
C7 C6 C16 C17 59.51(16)
C7 C6 C16 C21 -65.22(16)
C27 C28 C29 C30 0.7(2)
C27 C26 C31 C30 1.3(2)
C27 C37 C38 C44 -67.06(16)
C27 C37 C38 C39 167.46(12)
C27 C37 C42 C41 -135.63(17)
C28 C27 C26 O3 -178.98(11)
C28 C27 C26 C31 -0.02(18)
C28 C27 C37 C38 -70.38(15)
C28 C27 C37 C42 54.26(16)
C28 C29 C30 C31 0.6(2)
C28 C29 C30 C32 -179.24(13)
C26 C27 C28 O4 178.87(12)
C26 C27 C28 C29 -0.96(18)
C26 C27 C37 C38 109.37(14)
C26 C27 C37 C42 -125.99(13)
C26 C31 C30 C29 -1.5(2)
C26 C31 C30 C32 178.27(13)
C6 C7 C8 C9 4.8(2)
C6 C5 C10 C9 2.8(2)
C6 C16 C17 C18 -143.92(15)
C6 C16 C21 C22 -58.66(16)
C6 C16 C21 C20 174.31(13)
C5 C6 C16 C17 -121.22(13)
C5 C6 C16 C21 114.05(13)
C29 C30 C32 C33 -62.2(2)
C37 C27 C28 O4 -1.37(19)
C37 C27 C28 C29 178.80(12)
C37 C27 C26 O3 1.26(18)
C37 C27 C26 C31 -179.78(11)
C37 C38 C44 C45 -66.00(18)
C37 C38 C44 C46 115.25(19)
C37 C38 C39 C40 -64.94(16)
C9 C11 C12 C13 -178.47(15)
C16 C6 C5 O1 2.37(18)
C16 C6 C5 C10 -178.04(12)
C16 C17 C18 C25 -178.89(16)
C16 C17 C18 C19 -1.5(3)
C16 C21 C22 C23 109.34(19)
C16 C21 C22 C24 -69.1(2)
C16 C21 C20 C19 -63.94(19)
C8 C7 C6 C5 -5.08(19)
C8 C7 C6 C16 174.22(12)
C8 C9 C10 C5 -3.1(2)
C8 C9 C11 C12 -55.2(2)
C10 C9 C8 C7 -0.6(2)
C10 C9 C11 C12 123.46(16)
C38 C37 C42 C41 -10.5(2)
C38 C39 C40 C41 50.55(19)
C31 C30 C32 C33 118.00(18)
C42 C41 C40 C39 -16.2(2)
C42 C37 C38 C44 168.94(13)
C42 C37 C38 C39 43.46(16)
C30 C32 C33 C34 -66.3(2)
C17 C16 C21 C22 176.17(13)
C17 C16 C21 C20 49.14(16)
C17 C18 C19 C20 -11.9(3)
C44 C38 C39 C40 169.73(14)
C21 C16 C17 C18 -18.05(19)
C21 C20 C19 C18 44.8(2)
C22 C21 C20 C19 170.46(16)
C11 C9 C8 C7 178.12(13)
C11 C9 C10 C5 178.21(13)
C11 C12 C13 C14 -178.8(2)
C39 C38 C44 C45 57.14(19)
C39 C38 C44 C46 -121.6(2)
C32 C33 C34 C35 -178.50(17)
C12 C13 C14 C15 -178.5(2)
C33 C34 C35 C36 177.4(2)
C40 C41 C42 C37 -4.0(3)
C20 C21 C22 C23 -127.02(19)
C20 C21 C22 C24 54.5(2)
C43 C41 C42 C37 176.55(17)
C43 C41 C40 C39 163.23(17)
C25 C18 C19 C20 165.63(17)
_cod_database_fobs_code 1545377