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Information card for entry 1545903
Preview
| Coordinates | 1545903.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C20 H19 Br N2 O4 |
|---|---|
| Calculated formula | C20 H19 Br N2 O4 |
| Title of publication | Catalytic Annulation of Diethyl Methylenecyclopropane-1,1-dicarboxylate with 1,1-Dicyanoalkenes. |
| Authors of publication | Suzuki, Itaru; Tsunoi, Shinji; Shibata, Ikuya |
| Journal of publication | Organic letters |
| Year of publication | 2017 |
| Journal volume | 19 |
| Journal issue | 10 |
| Pages of publication | 2690 - 2693 |
| a | 28.3676 ± 0.0005 Å |
| b | 12.0527 ± 0.0002 Å |
| c | 11.4928 ± 0.0002 Å |
| α | 90° |
| β | 91.5907 ± 0.001° |
| γ | 90° |
| Cell volume | 3927.94 ± 0.12 Å3 |
| Cell temperature | 123 K |
| Ambient diffraction temperature | 123 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for significantly intense reflections | 0.0613 |
| Weighted residual factors for all reflections included in the refinement | 0.1498 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.007 |
| Diffraction radiation wavelength | 1.54187 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 197479 (current) | 2017-06-05 | cif/ Updating files of 1545903 Original log message: Adding full bibliography for 1545903.cif. |
1545903.cif |
| 195885 | 2017-05-02 | cif/ Adding structures of 1545903 via cif-deposit CGI script. |
1545903.cif |
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