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Information card for entry 1545905
Preview
| Coordinates | 1545905.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C126 H183 Cl6 O3 W1.5 |
|---|---|
| Calculated formula | C126 H183 Cl6 O3 W1.5 |
| Title of publication | Synthesis of 2,6-Hexa-tert-butylterphenyl Derivatives, 2,6-(2,4,6-t-Bu3C6H2)2C6H3X, where X = I, Li, OH, SH, N3, or NH2 |
| Authors of publication | Bukhryakov, Konstantin V.; Schrock, Richard R.; Hoveyda, Amir H.; Müller, Peter; Becker, Jonathan |
| Journal of publication | Organic Letters |
| Year of publication | 2017 |
| a | 19.931 ± 0.004 Å |
| b | 65.396 ± 0.014 Å |
| c | 18.862 ± 0.004 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 24585 ± 9 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.1796 |
| Residual factor for significantly intense reflections | 0.1707 |
| Weighted residual factors for significantly intense reflections | 0.4547 |
| Weighted residual factors for all reflections included in the refinement | 0.4625 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.274 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 195886 (current) | 2017-05-02 | cif/ Adding structures of 1545904, 1545905 via cif-deposit CGI script. |
1545905.cif |
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