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Information card for entry 1546246
Preview
| Coordinates | 1546246.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C123 H254 K2 N2 O32 Si8 U2 |
|---|---|
| Calculated formula | C123 H254 K2 N2 O32 Si8 U2 |
| Title of publication | Metathesis of a UV imido complex: a route to a terminal UV sulfide |
| Authors of publication | Kelly, Rory P.; Falcone, Marta; Lamsfus, Carlos Alvarez; Scopelliti, Rosario; Maron, Laurent; Meyer, Karsten; Mazzanti, Marinella |
| Journal of publication | Chem. Sci. |
| Year of publication | 2017 |
| a | 92.6284 ± 0.0008 Å |
| b | 24.32104 ± 0.00017 Å |
| c | 13.71515 ± 0.00011 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 30897.8 ± 0.4 Å3 |
| Cell temperature | 100.01 ± 0.1 K |
| Ambient diffraction temperature | 100.01 ± 0.1 K |
| Number of distinct elements | 7 |
| Space group number | 43 |
| Hermann-Mauguin space group symbol | F d d 2 |
| Hall space group symbol | F 2 -2d |
| Residual factor for all reflections | 0.0255 |
| Residual factor for significantly intense reflections | 0.0252 |
| Weighted residual factors for significantly intense reflections | 0.0639 |
| Weighted residual factors for all reflections included in the refinement | 0.0642 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 197542 (current) | 2017-06-06 | cif/ Adding structures of 1546246, 1546247, 1546248, 1546249, 1546250 via cif-deposit CGI script. |
1546246.cif |
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Users of the data should acknowledge the original authors of the
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