Crystallography Open Database

Information card for entry 1546713

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Structure parameters

Chemical name	1,1'-(Diphosphene-1,2-diyl)bis(2,2,6,6-tetramethylpiperidine)
Formula	C18 H36 N2 P2
Calculated formula	C18 H36 N2 P2
SMILES	C1(CCCC(C)(C)N1/P=P/N1C(CCCC1(C)C)(C)C)(C)C
Title of publication	1,1'-(Diphosphene-1,2-diyl)bis(2,2,6,6-tetramethylpiperidine)
Authors of publication	Höhne, Martha; Spannenberg, Anke; Müller, Bernd H.; Rosenthal, Uwe
Journal of publication	IUCrData
Year of publication	2017
Journal volume	2
Journal issue	6
Pages of publication	x170903
a	11.3277 ± 0.0003 Å
b	12.3257 ± 0.0003 Å
c	15.5274 ± 0.0004 Å
α	112.59 ± 0.0006°
β	90.7806 ± 0.0007°
γ	92.9221 ± 0.0007°
Cell volume	1997.74 ± 0.09 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0481
Residual factor for significantly intense reflections	0.035
Weighted residual factors for significantly intense reflections	0.0874
Weighted residual factors for all reflections included in the refinement	0.0949
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

Version history

Revision	Date	Message	Files
199309 (current)	2017-07-25	cif/ hkl/ Adding structures of 1546713 via cif-deposit CGI script.	1546713.cif 1546713.hkl