#------------------------------------------------------------------------------ #$Date: 2017-07-25 13:42:26 +0300 (Tue, 25 Jul 2017) $ #$Revision: 199314 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/67/1546718.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1546718 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.6744 _cell_length_b 6.9475 _cell_length_c 11.9880 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.8202 _cod_data_source_file hb4139Isup2.hkl _cod_data_source_block I _shelx_title ' shelxt_a.res in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 214.01 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 7900.46 7475.66 65.99 o 6 0 0 317.56 286.50 4.21 o 8 0 0 1003.23 1027.83 9.28 o 10 0 0 51.39 39.36 3.07 o 12 0 0 4950.87 5003.75 37.52 o 14 0 0 540.84 556.03 13.75 o 16 0 0 6.68 6.32 1.76 o 18 0 0 6.02 4.76 1.91 o 2 1 0 273.68 262.14 1.72 o 4 1 0 364.33 376.29 3.95 o 6 1 0 982.74 989.91 5.38 o 8 1 0 3.12 5.44 0.52 o 10 1 0 332.60 343.47 5.82 o 12 1 0 65.25 66.56 3.67 o 14 1 0 143.30 151.85 5.11 o 16 1 0 1.52 0.75 0.87 o 18 1 0 5.52 6.53 1.45 o 0 2 0 45798.23 47822.38 79.78 o 2 2 0 4785.29 4715.06 9.44 o 4 2 0 565.48 569.70 2.97 o 6 2 0 10.82 10.67 0.56 o 8 2 0 31.61 36.72 1.09 o 10 2 0 86.05 79.35 2.08 o 12 2 0 3168.41 3197.62 17.36 o 14 2 0 547.96 586.48 8.15 o 16 2 0 6.47 6.55 1.42 o 18 2 0 14.22 17.47 2.82 o 2 3 0 23.77 25.36 0.69 o 4 3 0 101.03 97.52 1.21 o 6 3 0 27.38 30.81 0.89 o 8 3 0 725.22 745.35 6.63 o 10 3 0 7.99 6.05 0.62 o 12 3 0 701.06 732.80 10.85 o 14 3 0 251.83 249.65 6.27 o 16 3 0 52.03 57.85 3.47 o 0 4 0 11804.85 11724.73 126.70 o 2 4 0 2544.73 2690.59 9.29 o 4 4 0 114.84 110.25 2.05 o 6 4 0 177.10 169.84 2.39 o 8 4 0 25.93 32.40 1.34 o 10 4 0 0.38 1.27 0.42 o 12 4 0 1962.56 2029.09 43.50 o 14 4 0 575.34 614.41 11.30 o 16 4 0 3.91 5.17 1.29 o 2 5 0 33.68 34.34 0.99 o 4 5 0 15.60 15.94 0.74 o 6 5 0 31.27 24.50 1.47 o 8 5 0 12.01 10.64 1.96 o 10 5 0 70.12 67.58 2.51 o 12 5 0 80.02 88.49 4.23 o 14 5 0 42.27 40.58 3.11 o 0 6 0 8427.27 8086.43 106.73 o 2 6 0 820.09 807.89 5.94 o 4 6 0 288.39 291.27 4.22 o 6 6 0 19.66 18.34 1.38 o 8 6 0 124.35 111.03 3.51 o 10 6 0 23.12 27.53 2.36 o 12 6 0 1561.95 1611.76 18.87 o 2 7 0 41.54 41.89 2.86 o 4 7 0 10.08 8.10 1.02 o 6 7 0 85.93 91.32 3.13 o 8 7 0 0.97 1.64 0.66 o 10 7 0 33.50 32.75 2.54 o 0 8 0 2142.36 1990.11 29.84 o 2 8 0 309.67 264.37 10.15 o 4 8 0 0.01 -2.15 2.15 o 6 8 0 3.77 2.54 1.41 o 3 0 1 0.24 0.37 0.39 o 4 0 1 305.26 348.32 3.48 o 5 0 1 2628.13 2473.99 9.46 o 6 0 1 1383.25 1281.15 7.96 o 7 0 1 0.05 0.06 0.37 o 8 0 1 587.81 632.80 5.99 o 9 0 1 75.78 90.84 2.45 o 10 0 1 196.30 193.47 4.73 o 11 0 1 769.06 739.37 7.76 o 12 0 1 152.64 147.46 4.63 o 13 0 1 1154.94 1142.76 13.31 o 14 0 1 519.63 514.93 9.40 o 15 0 1 4.00 7.44 1.51 o 16 0 1 74.77 72.04 3.83 o 17 0 1 25.32 29.63 2.64 o 18 0 1 9.43 10.39 1.67 o 19 0 1 16.85 15.89 2.18 o 0 1 1 10457.75 9362.05 633.80 o 1 1 1 67.97 67.24 2.08 o 2 1 1 2024.58 1890.10 8.64 o 3 1 1 1006.44 970.85 3.24 o 4 1 1 3685.49 3495.30 7.35 o 5 1 1 52.11 53.31 0.85 o 6 1 1 1.42 4.01 0.27 o 7 1 1 97.92 98.18 1.28 o 8 1 1 692.99 669.85 3.78 o 9 1 1 0.01 -0.31 0.36 o 10 1 1 69.89 72.78 2.72 o 11 1 1 9.70 11.70 0.89 o 12 1 1 84.43 83.63 2.17 o 13 1 1 1.42 3.15 0.68 o 14 1 1 73.24 79.70 2.61 o 15 1 1 14.76 14.87 1.27 o 16 1 1 19.47 20.06 1.51 o 17 1 1 18.95 17.94 1.50 o 18 1 1 11.32 11.79 1.26 o 1 2 1 13098.44 12835.76 77.59 o 2 2 1 888.45 926.40 2.34 o 3 2 1 693.29 662.12 1.93 o 4 2 1 101.11 85.32 0.78 o 5 2 1 76.80 81.13 0.92 o 6 2 1 4.16 4.69 0.28 o 7 2 1 19.85 27.18 0.67 o 8 2 1 11.68 6.89 0.42 o 9 2 1 517.14 517.04 4.09 o 10 2 1 7.69 5.24 0.47 o 11 2 1 431.93 423.42 4.25 o 12 2 1 628.38 632.04 5.97 o 13 2 1 1300.07 1314.49 9.03 o 14 2 1 765.52 773.56 7.24 o 15 2 1 26.77 25.26 1.46 o 16 2 1 1.84 0.85 0.57 o 17 2 1 16.50 17.84 1.46 o 18 2 1 25.27 26.90 2.51 o 0 3 1 4.78 1.71 0.26 o 1 3 1 29.13 29.50 0.38 o 2 3 1 807.80 847.02 2.53 o 3 3 1 0.72 0.87 0.15 o 4 3 1 308.56 316.32 1.72 o 5 3 1 8.40 8.94 0.30 o 6 3 1 157.07 168.17 1.28 o 7 3 1 36.17 39.30 0.79 o 8 3 1 43.69 41.52 0.97 o 9 3 1 53.53 57.54 1.16 o 10 3 1 7.95 7.88 0.54 o 11 3 1 41.36 41.59 1.21 o 12 3 1 1.22 1.32 0.63 o 13 3 1 49.01 52.40 1.71 o 14 3 1 154.32 172.23 3.46 o 15 3 1 4.68 3.70 0.70 o 16 3 1 8.70 8.73 0.89 o 17 3 1 0.07 0.82 0.73 o 1 4 1 2880.49 3040.94 4.52 o 2 4 1 983.89 1047.18 3.41 o 3 4 1 111.19 117.84 1.05 o 4 4 1 52.18 51.82 0.71 o 5 4 1 1.82 2.54 0.20 o 6 4 1 45.04 52.79 0.93 o 7 4 1 87.38 94.06 1.23 o 8 4 1 31.96 36.56 0.94 o 9 4 1 195.08 197.11 2.26 o 10 4 1 1.93 2.20 0.33 o 11 4 1 422.37 411.39 4.94 o 12 4 1 502.36 523.01 6.87 o 13 4 1 871.98 935.44 8.03 o 14 4 1 441.45 455.03 6.89 o 15 4 1 9.40 8.41 1.40 o 16 4 1 0.00 0.89 1.22 o 0 5 1 776.30 731.96 2.98 o 1 5 1 40.18 44.80 0.65 o 2 5 1 237.46 240.41 1.67 o 3 5 1 165.07 169.49 1.60 o 4 5 1 170.44 149.00 1.62 o 5 5 1 0.71 0.31 0.27 o 6 5 1 56.41 61.44 1.48 o 7 5 1 36.29 42.88 0.86 o 8 5 1 83.60 79.30 1.43 o 9 5 1 0.74 0.45 0.39 o 10 5 1 1.93 -0.25 0.45 o 11 5 1 0.27 0.00 0.56 o 12 5 1 49.92 55.24 2.38 o 13 5 1 0.64 1.83 0.79 o 14 5 1 77.43 82.00 3.07 o 15 5 1 3.06 2.79 1.19 o 1 6 1 606.91 602.28 3.96 o 2 6 1 18.50 20.99 1.17 o 3 6 1 1.35 1.47 0.30 o 4 6 1 5.84 4.80 0.39 o 5 6 1 56.23 58.25 1.43 o 6 6 1 21.45 22.33 1.04 o 7 6 1 9.44 7.09 0.65 o 8 6 1 39.64 39.34 1.33 o 9 6 1 21.80 18.60 0.97 o 10 6 1 19.52 19.43 1.18 o 11 6 1 237.45 229.08 3.90 o 12 6 1 81.55 78.91 2.65 o 13 6 1 424.33 428.71 6.16 o 0 7 1 377.04 369.48 6.29 o 1 7 1 0.23 0.66 0.47 o 2 7 1 64.03 63.19 1.65 o 3 7 1 10.82 10.02 0.70 o 4 7 1 95.61 96.57 2.44 o 5 7 1 3.58 3.92 0.54 o 6 7 1 0.94 -0.08 0.51 o 7 7 1 1.62 1.22 0.47 o 8 7 1 47.52 45.31 1.68 o 9 7 1 0.21 0.19 0.46 o 10 7 1 25.88 30.06 1.47 o 1 8 1 578.05 540.82 7.73 o 2 8 1 18.78 14.54 1.86 o 3 8 1 2.98 2.51 1.67 o 4 8 1 0.10 -0.16 1.06 o 5 8 1 4.76 4.15 1.52 o 6 8 1 0.16 -0.42 0.90 o 0 0 2 15.68 18.32 1.02 o 1 0 2 1165.17 1057.68 7.93 o 2 0 2 58.75 46.64 1.39 o 3 0 2 1225.92 1159.95 6.76 o 4 0 2 501.38 449.34 3.82 o 5 0 2 2652.20 2671.65 10.16 o 6 0 2 268.75 284.33 3.57 o 7 0 2 1191.60 1344.65 6.42 o 8 0 2 72.08 55.90 1.58 o 9 0 2 74.61 71.09 2.18 o 10 0 2 397.95 399.32 5.42 o 11 0 2 67.47 56.35 2.55 o 12 0 2 34.87 30.93 1.72 o 13 0 2 557.32 551.39 7.37 o 14 0 2 87.75 96.11 3.27 o 15 0 2 57.22 56.71 3.39 o 16 0 2 0.25 1.41 1.05 o 17 0 2 42.56 46.46 3.28 o 18 0 2 0.22 1.31 1.08 o 1 1 2 1784.01 1663.41 6.81 o 2 1 2 2339.74 2260.94 6.67 o 3 1 2 48.35 45.61 0.63 o 4 1 2 74.78 89.44 0.93 o 5 1 2 3.95 5.42 0.30 o 6 1 2 234.41 276.40 2.01 o 7 1 2 579.23 618.16 3.23 o 8 1 2 1.96 -0.24 0.25 o 9 1 2 15.33 16.88 1.07 o 10 1 2 143.61 150.16 3.29 o 11 1 2 32.88 30.98 1.30 o 12 1 2 103.23 103.96 2.44 o 13 1 2 4.03 3.07 0.90 o 14 1 2 22.74 23.30 1.33 o 15 1 2 30.08 31.47 1.56 o 16 1 2 52.25 50.32 2.05 o 17 1 2 0.17 0.42 0.67 o 18 1 2 105.14 131.66 3.99 o 0 2 2 51.88 55.91 0.70 o 1 2 2 1646.03 1618.05 6.67 o 2 2 2 429.36 423.66 1.76 o 3 2 2 4.89 8.02 0.28 o 4 2 2 0.05 0.29 0.17 o 5 2 2 935.57 1010.72 3.68 o 6 2 2 250.46 252.64 2.24 o 7 2 2 1361.30 1522.27 5.51 o 8 2 2 74.34 89.87 2.42 o 9 2 2 115.51 114.92 2.69 o 10 2 2 14.66 11.81 0.79 o 11 2 2 82.55 88.86 2.15 o 12 2 2 183.42 185.98 3.28 o 13 2 2 121.08 113.77 2.73 o 14 2 2 2.14 1.41 0.68 o 15 2 2 50.70 52.40 2.02 o 16 2 2 13.37 14.84 1.21 o 17 2 2 0.65 1.23 0.77 o 18 2 2 19.41 26.52 2.45 o 1 3 2 130.09 118.90 0.71 o 2 3 2 1121.84 1169.29 3.33 o 3 3 2 702.79 688.37 2.55 o 4 3 2 18.73 16.07 0.34 o 5 3 2 572.38 541.18 3.64 o 6 3 2 1800.94 1886.35 5.41 o 7 3 2 787.25 780.94 4.77 o 8 3 2 31.94 24.20 1.00 o 9 3 2 336.99 331.71 3.57 o 10 3 2 14.46 17.55 1.08 o 11 3 2 0.93 1.25 0.56 o 12 3 2 202.63 212.79 4.33 o 13 3 2 43.89 36.32 1.95 o 14 3 2 41.48 45.13 1.80 o 15 3 2 18.03 15.59 1.15 o 16 3 2 6.66 6.11 1.02 o 17 3 2 0.66 0.10 0.92 o 0 4 2 343.33 357.88 2.40 o 1 4 2 139.42 140.19 0.94 o 2 4 2 115.82 115.38 0.95 o 3 4 2 46.00 47.33 0.77 o 4 4 2 114.30 121.33 1.20 o 5 4 2 331.19 360.24 2.14 o 6 4 2 148.90 157.57 1.61 o 7 4 2 460.39 457.61 5.43 o 8 4 2 64.71 73.85 1.22 o 9 4 2 67.98 82.94 1.51 o 10 4 2 28.80 28.29 1.01 o 11 4 2 54.96 51.77 1.67 o 12 4 2 93.02 88.00 2.68 o 13 4 2 99.01 97.65 3.70 o 14 4 2 5.02 6.34 1.18 o 15 4 2 55.42 58.90 3.05 o 16 4 2 1.01 -0.04 1.19 o 1 5 2 112.11 98.73 0.99 o 2 5 2 47.34 46.57 0.67 o 3 5 2 0.92 0.99 0.19 o 4 5 2 18.66 19.59 0.48 o 5 5 2 5.42 3.56 0.26 o 6 5 2 88.92 93.30 1.17 o 7 5 2 186.69 180.96 2.03 o 8 5 2 19.32 18.66 0.74 o 9 5 2 4.71 9.23 0.66 o 10 5 2 22.69 19.39 1.05 o 11 5 2 0.48 1.21 0.83 o 12 5 2 109.39 119.55 3.33 o 13 5 2 1.12 -0.44 0.94 o 14 5 2 12.79 10.43 1.41 o 15 5 2 2.68 2.32 1.19 o 0 6 2 1.08 1.19 0.33 o 1 6 2 81.07 79.04 1.11 o 2 6 2 3.33 3.17 0.27 o 3 6 2 10.25 12.10 0.44 o 4 6 2 5.33 3.21 0.43 o 5 6 2 272.57 274.59 3.05 o 6 6 2 2.13 2.22 0.47 o 7 6 2 191.98 176.71 2.93 o 8 6 2 0.59 0.68 0.44 o 9 6 2 0.45 0.42 0.43 o 10 6 2 31.31 35.57 1.37 o 11 6 2 11.84 8.91 1.08 o 12 6 2 25.46 24.97 1.69 o 13 6 2 149.99 153.90 4.93 o 1 7 2 9.26 12.16 0.91 o 2 7 2 32.78 32.37 1.40 o 3 7 2 0.18 -0.39 0.39 o 4 7 2 6.50 6.62 0.60 o 5 7 2 5.09 6.03 0.66 o 6 7 2 34.62 32.75 1.47 o 7 7 2 37.37 33.95 1.55 o 8 7 2 12.11 14.00 1.06 o 9 7 2 16.86 17.87 1.11 o 10 7 2 13.89 13.11 1.03 o 0 8 2 3.13 2.79 1.52 o 1 8 2 67.87 66.91 2.79 o 2 8 2 2.62 5.16 1.37 o 3 8 2 5.65 2.50 1.57 o 4 8 2 0.03 -1.74 2.42 o 5 8 2 123.67 106.18 4.97 o 1 0 3 201.20 179.29 2.67 o 2 0 3 10214.45 10212.05 74.89 o 3 0 3 1166.45 1121.74 4.53 o 4 0 3 0.10 0.10 0.22 o 5 0 3 460.89 467.94 5.22 o 6 0 3 5132.31 5498.55 20.60 o 7 0 3 68.09 67.22 1.95 o 8 0 3 571.04 588.18 5.26 o 9 0 3 2.32 0.81 0.47 o 10 0 3 162.95 173.84 3.67 o 11 0 3 19.59 23.62 1.47 o 12 0 3 0.09 0.19 0.77 o 13 0 3 18.09 21.61 1.54 o 14 0 3 16.37 11.34 1.26 o 15 0 3 39.89 45.92 2.38 o 16 0 3 4.58 3.16 1.20 o 17 0 3 22.44 23.51 2.40 o 18 0 3 19.22 26.03 2.68 o 0 1 3 1525.85 1453.46 8.29 o 1 1 3 231.50 217.93 1.55 o 2 1 3 1.18 1.28 0.17 o 3 1 3 641.63 637.13 3.55 o 4 1 3 84.00 71.01 1.11 o 5 1 3 3936.31 4227.24 9.34 o 6 1 3 66.35 71.78 1.08 o 7 1 3 2644.95 2925.91 7.13 o 8 1 3 58.22 61.54 1.23 o 9 1 3 102.01 92.58 2.06 o 10 1 3 6.61 7.08 0.73 o 11 1 3 9.87 6.13 0.60 o 12 1 3 31.74 33.39 1.29 o 13 1 3 49.04 47.43 1.59 o 14 1 3 0.31 -0.60 0.60 o 15 1 3 11.64 14.77 1.10 o 16 1 3 17.31 19.49 1.35 o 17 1 3 36.40 45.55 2.07 o 18 1 3 4.03 1.66 0.72 o 1 2 3 80.89 68.97 0.71 o 2 2 3 33.15 39.35 0.62 o 3 2 3 11.46 9.70 0.33 o 4 2 3 128.52 151.32 1.11 o 5 2 3 62.37 75.53 0.85 o 6 2 3 349.68 395.53 2.17 o 7 2 3 125.19 137.59 1.52 o 8 2 3 353.10 356.59 3.44 o 9 2 3 4.67 3.86 0.48 o 10 2 3 6.73 5.31 0.56 o 11 2 3 43.87 44.47 1.58 o 12 2 3 0.96 0.87 0.54 o 13 2 3 2.48 3.02 0.81 o 14 2 3 23.34 21.02 1.26 o 15 2 3 0.01 -0.60 0.60 o 16 2 3 0.92 0.36 0.54 o 17 2 3 13.48 17.15 1.34 o 18 2 3 43.30 55.24 3.62 o 0 3 3 259.81 258.28 1.83 o 1 3 3 666.26 701.69 2.35 o 2 3 3 161.61 159.57 1.33 o 3 3 3 92.02 120.22 1.22 o 4 3 3 0.76 0.30 0.18 o 5 3 3 595.77 607.86 2.36 o 6 3 3 295.95 290.32 2.21 o 7 3 3 697.19 773.79 4.76 o 8 3 3 0.46 -0.41 0.41 o 9 3 3 20.03 25.29 1.13 o 10 3 3 326.86 321.93 5.07 o 11 3 3 32.54 26.47 1.33 o 12 3 3 0.92 -0.61 0.98 o 13 3 3 138.71 133.15 2.94 o 14 3 3 121.61 124.26 2.99 o 15 3 3 5.40 6.98 0.97 o 16 3 3 24.54 21.63 1.41 o 17 3 3 4.40 7.80 1.94 o 1 4 3 54.61 51.85 0.73 o 2 4 3 0.98 1.03 0.17 o 3 4 3 4.02 3.83 0.33 o 4 4 3 0.34 0.69 0.22 o 5 4 3 18.82 16.33 0.60 o 6 4 3 122.84 127.89 1.23 o 7 4 3 137.87 128.12 1.69 o 8 4 3 493.98 496.76 6.37 o 9 4 3 1.44 1.54 0.36 o 10 4 3 0.85 0.99 0.38 o 11 4 3 52.45 49.33 2.26 o 12 4 3 26.15 25.84 2.03 o 13 4 3 6.35 4.87 1.46 o 14 4 3 17.54 17.70 1.37 o 15 4 3 2.11 1.73 0.92 o 0 5 3 9.19 14.31 0.55 o 1 5 3 32.18 31.19 0.79 o 2 5 3 8.35 12.41 0.53 o 3 5 3 11.99 7.41 0.40 o 4 5 3 15.56 16.80 0.61 o 5 5 3 469.05 475.40 2.91 o 6 5 3 3.67 2.55 0.36 o 7 5 3 647.15 686.94 5.09 o 8 5 3 2.24 2.54 0.47 o 9 5 3 0.26 0.10 0.51 o 10 5 3 0.00 -0.36 0.51 o 11 5 3 0.31 0.39 0.70 o 12 5 3 21.87 23.39 1.34 o 13 5 3 32.27 33.52 1.93 o 14 5 3 0.16 -0.63 0.89 o 1 6 3 4.45 4.12 0.43 o 2 6 3 387.58 398.49 3.72 o 3 6 3 49.72 44.93 1.20 o 4 6 3 12.83 11.50 0.65 o 5 6 3 44.76 40.09 1.22 o 6 6 3 463.44 462.67 4.51 o 7 6 3 0.15 1.51 0.58 o 8 6 3 142.33 142.25 3.07 o 9 6 3 1.13 -0.04 0.54 o 10 6 3 35.59 38.58 1.70 o 11 6 3 0.40 0.01 0.88 o 12 6 3 1.45 1.25 0.83 o 0 7 3 124.47 119.24 3.79 o 1 7 3 2.02 2.02 0.59 o 2 7 3 2.53 1.58 0.49 o 3 7 3 7.54 5.74 0.80 o 4 7 3 10.63 11.83 0.91 o 5 7 3 324.50 316.84 4.30 o 6 7 3 2.73 2.54 0.57 o 7 7 3 303.73 312.94 6.31 o 8 7 3 4.34 4.32 0.80 o 9 7 3 7.35 8.02 1.35 o 10 7 3 0.37 -0.16 0.88 o 1 8 3 0.02 1.29 0.65 o 2 8 3 6.19 3.29 0.85 o 3 8 3 7.90 4.12 0.80 o 4 8 3 35.62 29.03 2.51 o 0 0 4 181.17 171.05 3.03 o 1 0 4 3651.39 3622.48 13.77 o 2 0 4 296.73 277.64 2.32 o 3 0 4 2266.24 2183.02 6.76 o 4 0 4 651.25 638.61 4.99 o 5 0 4 179.26 161.76 2.19 o 6 0 4 133.33 117.38 1.95 o 7 0 4 101.40 82.25 1.97 o 8 0 4 68.98 61.99 2.52 o 9 0 4 14.87 8.84 1.04 o 10 0 4 7.15 8.45 1.19 o 11 0 4 113.75 138.03 3.48 o 12 0 4 4.14 3.64 0.81 o 13 0 4 42.47 46.61 2.26 o 14 0 4 5.04 3.59 1.40 o 15 0 4 20.05 18.64 1.61 o 16 0 4 2.57 1.88 0.78 o 17 0 4 24.97 26.97 2.08 o 18 0 4 0.03 -0.84 0.94 o 1 1 4 171.28 162.49 1.66 o 2 1 4 300.38 273.78 1.92 o 3 1 4 164.48 152.80 1.40 o 4 1 4 163.16 142.40 1.41 o 5 1 4 17.10 19.91 0.69 o 6 1 4 2619.04 2771.95 7.84 o 7 1 4 41.34 54.56 1.17 o 8 1 4 4.18 11.62 0.73 o 9 1 4 23.69 28.73 1.21 o 10 1 4 0.00 -0.34 0.34 o 11 1 4 99.01 98.90 2.10 o 12 1 4 24.24 21.67 1.08 o 13 1 4 26.03 20.52 1.10 o 14 1 4 141.44 119.71 2.61 o 15 1 4 0.17 0.04 0.62 o 16 1 4 2.17 3.69 0.69 o 17 1 4 0.42 0.49 0.59 o 18 1 4 99.80 118.77 4.32 o 0 2 4 75.85 67.21 1.29 o 1 2 4 23.34 28.72 0.57 o 2 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9.65 0.98 o 14 1 9 7.48 4.36 0.87 o 1 2 9 18.37 10.56 0.53 o 2 2 9 0.91 1.38 0.41 o 3 2 9 2.91 -0.56 1.14 o 4 2 9 379.05 378.37 3.95 o 5 2 9 185.33 172.52 2.71 o 6 2 9 2253.39 2388.12 12.85 o 7 2 9 7.67 10.68 1.06 o 8 2 9 359.32 350.93 4.48 o 9 2 9 0.05 -0.23 0.57 o 10 2 9 10.89 12.80 0.96 o 11 2 9 0.01 -0.40 0.52 o 12 2 9 13.15 12.24 1.24 o 13 2 9 0.01 -0.15 0.62 o 14 2 9 33.13 45.40 3.20 o 0 3 9 197.41 226.00 3.16 o 1 3 9 0.62 0.74 0.23 o 2 3 9 27.51 27.20 0.91 o 3 3 9 33.76 32.73 1.09 o 4 3 9 379.51 406.60 3.94 o 5 3 9 177.41 170.51 3.33 o 6 3 9 199.32 209.38 3.73 o 7 3 9 194.22 207.27 3.77 o 8 3 9 30.61 38.00 1.74 o 9 3 9 22.33 19.30 1.14 o 10 3 9 12.96 13.85 1.00 o 11 3 9 73.95 72.23 2.24 o 12 3 9 8.77 10.40 1.04 o 13 3 9 33.90 25.46 2.50 o 1 4 9 8.43 11.46 0.76 o 2 4 9 24.84 25.51 1.11 o 3 4 9 0.16 0.34 0.86 o 4 4 9 185.23 177.03 3.23 o 5 4 9 142.49 154.37 3.37 o 6 4 9 1756.75 1852.14 11.66 o 7 4 9 10.80 13.63 1.28 o 8 4 9 341.33 359.07 5.40 o 9 4 9 3.71 5.50 0.85 o 10 4 9 11.37 11.93 1.08 o 11 4 9 0.35 -0.46 0.63 o 12 4 9 11.29 13.20 1.88 o 0 5 9 12.81 13.52 1.27 o 1 5 9 5.86 8.49 0.79 o 2 5 9 0.29 -0.73 0.79 o 3 5 9 2.18 -0.23 0.66 o 4 5 9 10.65 7.68 0.80 o 5 5 9 82.56 76.71 2.31 o 6 5 9 9.91 15.43 1.33 o 7 5 9 109.02 104.37 2.96 o 8 5 9 5.95 7.88 0.89 o 9 5 9 1.79 2.82 0.81 o 1 6 9 9.28 7.42 1.38 o 2 6 9 30.08 21.26 1.72 o 3 6 9 21.59 19.28 1.34 o 4 6 9 103.37 99.78 3.05 o 5 6 9 56.92 60.55 2.51 o 6 6 9 1028.79 1078.58 10.77 o 0 0 10 199.43 222.08 7.66 o 1 0 10 4.89 5.91 0.72 o 2 0 10 39.72 40.53 1.62 o 3 0 10 0.50 0.05 0.36 o 4 0 10 4.01 6.96 0.73 o 5 0 10 56.51 70.65 2.82 o 6 0 10 71.63 61.79 2.55 o 7 0 10 72.23 72.21 2.48 o 8 0 10 156.13 158.37 4.25 o 9 0 10 2.34 6.60 1.06 o 10 0 10 3.71 5.90 1.02 o 11 0 10 0.39 0.50 0.90 o 12 0 10 69.34 86.84 4.47 o 13 0 10 87.05 125.38 5.50 o 1 1 10 100.15 91.64 2.13 o 2 1 10 51.14 56.47 1.38 o 3 1 10 0.08 -0.48 0.48 o 4 1 10 10.06 10.82 0.80 o 5 1 10 0.02 -0.01 0.40 o 6 1 10 113.22 110.13 2.23 o 7 1 10 0.16 0.06 0.48 o 8 1 10 30.00 24.76 1.15 o 9 1 10 14.87 14.89 1.06 o 10 1 10 0.16 -0.34 0.51 o 11 1 10 39.24 37.52 2.07 o 12 1 10 13.19 8.38 1.12 o 13 1 10 0.19 1.43 0.86 o 0 2 10 0.97 0.99 0.55 o 1 2 10 96.39 83.77 1.45 o 2 2 10 14.54 11.65 0.81 o 3 2 10 173.67 168.45 2.72 o 4 2 10 89.06 100.28 1.96 o 5 2 10 174.73 180.00 2.67 o 6 2 10 122.26 129.44 2.46 o 7 2 10 271.15 272.12 4.17 o 8 2 10 11.83 10.22 0.89 o 9 2 10 3.57 4.00 0.68 o 10 2 10 0.19 -0.01 0.56 o 11 2 10 3.63 4.83 0.75 o 12 2 10 5.78 6.04 0.83 o 13 2 10 58.56 75.91 4.10 o 1 3 10 185.58 188.42 2.81 o 2 3 10 52.13 58.92 2.10 o 3 3 10 5.02 2.37 0.88 o 4 3 10 9.98 7.54 0.71 o 5 3 10 85.30 91.91 2.56 o 6 3 10 52.38 48.43 1.92 o 7 3 10 36.31 37.96 1.72 o 8 3 10 11.38 16.45 1.27 o 9 3 10 24.91 26.38 1.53 o 10 3 10 12.70 17.82 1.19 o 11 3 10 1.49 1.60 0.55 o 12 3 10 0.52 -0.81 1.45 o 0 4 10 15.14 11.52 1.69 o 1 4 10 63.81 59.93 2.12 o 2 4 10 15.86 15.87 1.13 o 3 4 10 72.11 66.46 2.01 o 4 4 10 41.02 40.48 1.46 o 5 4 10 183.18 180.04 3.43 o 6 4 10 52.85 57.93 2.20 o 7 4 10 137.93 137.03 3.35 o 8 4 10 7.46 7.89 0.95 o 9 4 10 13.06 16.02 1.28 o 10 4 10 3.58 1.86 1.00 o 1 5 10 16.12 17.84 1.09 o 2 5 10 39.76 26.98 1.49 o 3 5 10 5.67 2.40 0.69 o 4 5 10 3.25 2.72 1.25 o 5 5 10 1.24 0.87 0.57 o 6 5 10 28.50 33.66 1.62 o 7 5 10 0.01 1.07 0.64 o 8 5 10 13.57 17.95 1.48 o 0 6 10 46.25 53.37 5.05 o 1 6 10 2.50 -0.10 3.37 o 2 6 10 12.05 11.13 1.91 o 3 6 10 2.61 2.93 1.38 o 1 0 11 248.21 173.32 3.62 o 2 0 11 220.88 196.49 3.70 o 3 0 11 0.84 -0.05 0.49 o 4 0 11 15.15 15.76 2.08 o 5 0 11 5.54 7.09 1.14 o 6 0 11 34.18 38.47 2.15 o 7 0 11 45.33 46.29 2.08 o 8 0 11 0.76 -0.06 0.62 o 9 0 11 7.83 8.96 1.01 o 10 0 11 150.27 167.59 4.78 o 11 0 11 95.92 103.34 4.93 o 12 0 11 15.23 28.13 3.85 o 0 1 11 23.05 19.46 1.49 o 1 1 11 11.32 12.58 0.72 o 2 1 11 0.40 -0.28 0.46 o 3 1 11 15.11 17.48 1.00 o 4 1 11 20.19 20.70 1.06 o 5 1 11 61.98 55.98 1.60 o 6 1 11 6.50 7.25 0.76 o 7 1 11 75.10 71.63 1.81 o 8 1 11 12.59 12.80 0.91 o 9 1 11 8.24 6.31 0.71 o 10 1 11 10.97 10.57 1.21 o 11 1 11 1.26 3.09 0.71 o 12 1 11 19.85 22.13 3.42 o 1 2 11 493.86 453.47 4.58 o 2 2 11 7.94 3.08 0.54 o 3 2 11 0.17 -0.19 0.56 o 4 2 11 0.50 0.01 0.40 o 5 2 11 53.51 56.93 1.59 o 6 2 11 5.02 7.36 0.65 o 7 2 11 6.03 7.42 1.06 o 8 2 11 33.12 38.06 1.86 o 9 2 11 34.99 34.34 1.61 o 10 2 11 57.91 60.45 2.14 o 11 2 11 21.10 24.91 1.75 o 0 3 11 41.44 37.28 1.91 o 1 3 11 107.06 106.74 2.61 o 2 3 11 7.83 5.57 0.69 o 3 3 11 7.92 5.37 0.82 o 4 3 11 11.33 14.45 0.95 o 5 3 11 4.20 4.31 0.64 o 6 3 11 7.16 7.20 0.77 o 7 3 11 16.33 20.47 1.36 o 8 3 11 34.93 36.58 1.87 o 9 3 11 0.48 1.07 0.67 o 10 3 11 4.39 3.00 0.92 o 1 4 11 247.44 259.28 4.52 o 2 4 11 9.10 11.17 1.02 o 3 4 11 2.06 0.90 0.65 o 4 4 11 0.57 -0.16 0.72 o 5 4 11 9.62 14.08 1.12 o 6 4 11 4.79 3.01 0.76 o 7 4 11 5.47 9.22 1.02 o 8 4 11 9.74 10.87 2.01 o 0 5 11 2.70 6.68 1.47 o 1 5 11 6.94 6.91 0.89 o 2 5 11 0.02 -0.65 0.65 o 3 5 11 14.89 19.83 1.54 o 4 5 11 17.70 11.21 1.32 o 5 5 11 18.19 19.11 1.56 o 0 0 12 451.69 393.25 16.77 o 1 0 12 55.06 52.97 3.03 o 2 0 12 26.07 21.68 2.93 o 3 0 12 26.27 25.45 2.17 o 4 0 12 40.83 38.51 2.62 o 5 0 12 8.02 6.48 1.25 o 6 0 12 20.86 18.52 1.88 o 7 0 12 12.54 15.18 1.32 o 8 0 12 0.47 -0.61 0.61 o 9 0 12 12.99 9.92 1.09 o 10 0 12 17.78 12.45 1.41 o 1 1 12 131.06 105.81 2.27 o 2 1 12 9.22 6.34 0.79 o 3 1 12 7.23 8.07 0.89 o 4 1 12 12.52 13.48 1.15 o 5 1 12 2.19 0.37 0.74 o 6 1 12 0.06 -0.17 0.48 o 7 1 12 14.32 17.00 1.06 o 8 1 12 0.88 2.72 0.55 o 9 1 12 5.75 5.31 0.69 o 10 1 12 18.85 21.63 1.82 o 0 2 12 146.67 138.48 3.84 o 1 2 12 41.10 40.35 1.46 o 2 2 12 2.62 0.78 0.48 o 3 2 12 47.69 51.10 1.78 o 4 2 12 0.25 -0.58 0.76 o 5 2 12 28.74 26.59 1.65 o 6 2 12 9.74 11.91 1.07 o 7 2 12 0.04 0.28 0.58 o 8 2 12 0.01 0.31 0.67 o 9 2 12 0.04 -0.04 0.79 o 1 3 12 61.20 57.90 2.41 o 2 3 12 66.51 75.41 2.73 o 3 3 12 0.24 1.37 0.56 o 4 3 12 39.85 45.12 1.74 o 5 3 12 0.36 0.35 0.50 o 6 3 12 74.82 79.85 2.63 o 7 3 12 11.83 11.24 1.11 o 8 3 12 6.75 7.44 1.30 o 0 4 12 197.83 182.92 9.98 o 1 4 12 28.23 32.76 1.73 o 2 4 12 6.55 6.13 0.81 o 3 4 12 38.45 44.35 2.00 o 4 4 12 8.54 7.01 0.99 o 5 4 12 18.58 16.80 1.50 o 6 4 12 0.67 -0.63 0.85 o 1 0 13 0.02 -0.46 0.83 o 2 0 13 5.50 5.78 1.24 o 3 0 13 4.58 4.28 1.18 o 4 0 13 0.70 2.71 1.08 o 5 0 13 103.46 104.33 4.55 o 6 0 13 1.08 0.99 1.69 o 7 0 13 61.40 66.80 3.13 o 8 0 13 26.99 32.51 3.02 o 0 1 13 39.34 44.58 2.98 o 1 1 13 0.60 1.04 0.47 o 2 1 13 0.49 0.47 0.90 o 3 1 13 0.50 0.89 0.59 o 4 1 13 0.41 0.98 0.59 o 5 1 13 3.76 4.21 0.91 o 6 1 13 14.45 15.16 1.18 o 7 1 13 5.27 8.14 0.94 o 8 1 13 7.22 7.89 1.22 o 1 2 13 55.06 47.64 2.16 o 2 2 13 11.70 12.94 1.20 o 3 2 13 2.17 0.19 0.68 o 4 2 13 0.33 0.11 0.65 o 5 2 13 7.36 10.32 1.19 o 6 2 13 16.09 25.14 1.73 o 7 2 13 70.28 85.48 4.31 o 0 3 13 35.94 29.36 4.36 o 1 3 13 22.86 25.46 1.68 o 2 3 13 0.15 1.29 0.81 o 3 3 13 37.96 47.61 2.38 o 4 3 13 0.65 0.56 0.77 o 5 3 13 2.30 4.72 1.36 o 0 0 14 29.12 16.13 2.79 o 1 0 14 4.10 1.64 0.92 o 2 0 14 18.85 22.68 2.24 o 3 0 14 7.33 6.87 1.48 o 4 0 14 0.01 0.14 0.87 o 5 0 14 54.30 64.73 3.78 o 1 1 14 18.91 19.76 1.49 o 2 1 14 0.82 0.66 0.65 o 3 1 14 9.51 12.20 1.18 o 4 1 14 45.36 60.21 3.04 o 5 1 14 7.66 7.68 1.33 o 0 2 14 3.27 6.85 2.19 o 1 2 14 33.26 40.13 3.26 o 2 2 14 31.98 32.97 2.99 o 3 2 14 78.05 93.97 4.88 o