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Information card for entry 1547104
Preview
| Coordinates | 1547104.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C19 H26 Cl O3.5 |
|---|---|
| Calculated formula | C19 H26 Cl O3.5 |
| Title of publication | Construction of Distant Stereocenters by Enantioselective Desymmetrizing Carbonyl-Ene Reaction. |
| Authors of publication | Luo, Weiwei; Lin, Lili; Zhang, Yu; Liu, Xiaohua; Feng, Xiaoming |
| Journal of publication | Organic letters |
| Year of publication | 2017 |
| Journal volume | 19 |
| Journal issue | 13 |
| Pages of publication | 3374 - 3377 |
| a | 18.6435 ± 0.0007 Å |
| b | 6.1999 ± 0.0002 Å |
| c | 15.8122 ± 0.0006 Å |
| α | 90° |
| β | 90.137 ± 0.003° |
| γ | 90° |
| Cell volume | 1827.69 ± 0.11 Å3 |
| Cell temperature | 290.64 ± 0.1 K |
| Ambient diffraction temperature | 290.64 ± 0.1 K |
| Number of distinct elements | 4 |
| Space group number | 5 |
| Hermann-Mauguin space group symbol | C 1 2 1 |
| Hall space group symbol | C 2y |
| Residual factor for all reflections | 0.06 |
| Residual factor for significantly intense reflections | 0.0572 |
| Weighted residual factors for significantly intense reflections | 0.1533 |
| Weighted residual factors for all reflections included in the refinement | 0.1587 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.074 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 200623 (current) | 2017-09-12 | cif/ Adding structures of 1547104 via cif-deposit CGI script. |
1547104.cif |
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Users of the data should acknowledge the original authors of the
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