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Information card for entry 1547159
Preview
Coordinates | 1547159.cif |
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Original paper (by DOI) | HTML |
Formula | C39 H40 N4 O10 |
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Calculated formula | C39 H40 N4 O10 |
Title of publication | Gelsekoumidines A and B: Two Pairs of Atropisomeric Bisindole Alkaloids from the Roots of Gelsemium elegans. |
Authors of publication | Zhang, Wei; Xu, Wei; Wang, Gui-Yang; Gong, Xue-Ying; Li, Ni-Ping; Wang, Lei; Ye, Wen-Cai |
Journal of publication | Organic letters |
Year of publication | 2017 |
Journal volume | 19 |
Journal issue | 19 |
Pages of publication | 5194 - 5197 |
a | 12.6396 ± 0.0003 Å |
b | 20.1301 ± 0.0004 Å |
c | 14.184 ± 0.0003 Å |
α | 90° |
β | 91.5813 ± 0.0017° |
γ | 90° |
Cell volume | 3607.55 ± 0.14 Å3 |
Cell temperature | 100 ± 0.1 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0821 |
Residual factor for significantly intense reflections | 0.0759 |
Weighted residual factors for significantly intense reflections | 0.2056 |
Weighted residual factors for all reflections included in the refinement | 0.2176 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
202776 (current) | 2017-11-07 | cif/ Updating files of 1547159 Original log message: Adding full bibliography for 1547159.cif. |
1547159.cif |
200852 | 2017-09-14 | cif/ Adding structures of 1547159 via cif-deposit CGI script. |
1547159.cif |
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