Crystallography Open Database

Information card for entry 1547846

Preview

Coordinates	1547846.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C238 H196 Ag18 Cl F18 P6 Sb3
Calculated formula	C238 H196 Ag18 Cl F18 P6 Sb3
Title of publication	Novel chloride-centered Ag <sub>18</sub> clusters featuring a cuboctahedral Ag <sub>12</sub> skeleton
Authors of publication	Shen, Hui; Kubo, Kazuyuki; Kume, Shoko; Zhang, Limin; Mizuta, Tsutomu
Journal of publication	Dalton Transactions
Year of publication	2017
Journal volume	46
Journal issue	46
Pages of publication	16199 - 16204
a	18.465 ± 0.002 Å
b	19.82 ± 0.002 Å
c	20.121 ± 0.003 Å
α	117.453 ± 0.001°
β	116.671 ± 0.001°
γ	92.003 ± 0.002°
Cell volume	5561 ± 1.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0999
Residual factor for significantly intense reflections	0.0524
Weighted residual factors for significantly intense reflections	0.121
Weighted residual factors for all reflections included in the refinement	0.1549
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKa
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
282777 (current)	2023-04-20	cod/ (saulius@starta) Updating COD bibliographies for 271 COD entries identified by R.M.	1547846.cif
202462	2017-11-01	cif/ Adding structures of 1547845, 1547846 via cif-deposit CGI script.	1547846.cif