#------------------------------------------------------------------------------ #$Date: 2018-04-30 20:08:23 +0300 (Mon, 30 Apr 2018) $ #$Revision: 207587 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/93/1549356.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1549356 _cell_angle_alpha 90.000 _cell_angle_beta 97.849 _cell_angle_gamma 90.000 _cell_length_a 9.6505 _cell_length_b 19.3780 _cell_length_c 15.1026 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.6985 _cod_data_source_file wm4070Isup2.hkl _cod_data_source_block I _shelx_title ' SMB_AsPh4ZrCl6_0m_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 290.78 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 108.04 145.65 14.08 o 2 0 0 21.15 11.78 12.96 o 3 0 0 22783.76 22272.94 388.62 o 4 0 0 368.62 458.13 46.50 o 5 0 0 42.85 87.50 24.79 o 6 0 0 9359.84 9119.65 217.74 o 7 0 0 862.92 760.35 91.94 o 8 0 0 100.34 142.15 55.12 o 9 0 0 12082.11 12084.87 368.46 o 10 0 0 317.26 436.95 124.04 o 11 0 0 32.55 162.12 101.12 o 12 0 0 878.74 679.38 198.92 o 13 0 0 355.97 329.24 150.63 o 1 1 0 18754.56 19319.22 259.67 o 2 1 0 279.49 274.79 16.34 o 3 1 0 1846.70 2033.16 46.50 o 4 1 0 2481.61 2651.55 82.63 o 5 1 0 12824.18 12695.96 187.41 o 6 1 0 382.97 477.56 34.18 o 7 1 0 151.45 107.72 28.51 o 8 1 0 3684.06 3699.33 99.75 o 9 1 0 87.32 53.64 37.45 o 10 1 0 3020.16 3163.39 147.96 o 11 1 0 1207.30 1121.30 122.20 o 12 1 0 106.73 162.33 81.43 o 13 1 0 755.11 704.73 235.82 o 0 2 0 132.49 82.55 12.42 o 1 2 0 16149.08 17055.92 216.86 o 2 2 0 947.11 902.41 25.80 o 3 2 0 5264.77 5339.98 86.72 o 4 2 0 6230.42 6108.83 103.77 o 5 2 0 817.67 703.38 36.35 o 6 2 0 2152.79 2066.97 70.44 o 7 2 0 4856.38 4906.64 109.67 o 8 2 0 3700.61 3556.31 124.06 o 9 2 0 427.67 446.82 67.10 o 10 2 0 2449.87 2501.94 165.93 o 11 2 0 3.36 -24.44 59.36 o 12 2 0 905.68 751.98 115.74 o 13 2 0 1209.99 1166.15 151.91 o 1 3 0 2369.24 2387.28 46.00 o 2 3 0 19035.31 19574.69 258.85 o 3 3 0 5427.65 5360.17 87.75 o 4 3 0 4753.44 4656.11 86.66 o 5 3 0 774.02 736.17 37.50 o 6 3 0 535.68 494.43 43.24 o 7 3 0 2295.80 2388.57 70.77 o 8 3 0 566.70 507.80 51.04 o 9 3 0 5.07 -6.84 42.37 o 10 3 0 39.89 35.70 50.22 o 11 3 0 1837.60 2222.04 156.63 o 12 3 0 217.72 176.88 85.04 o 13 3 0 89.55 137.74 88.91 o 0 4 0 424.44 421.80 33.35 o 1 4 0 13276.24 13509.21 170.43 o 2 4 0 163.51 207.48 21.71 o 3 4 0 2538.51 2588.65 54.06 o 4 4 0 244.55 230.06 21.32 o 5 4 0 5633.81 5793.44 107.63 o 6 4 0 6117.55 6237.39 120.30 o 7 4 0 5067.43 5176.40 113.45 o 8 4 0 5093.95 5110.44 149.71 o 9 4 0 9493.93 9288.70 225.49 o 10 4 0 3101.03 3126.76 150.38 o 11 4 0 515.42 387.93 79.31 o 12 4 0 1.10 -14.33 64.61 o 13 4 0 26.37 24.10 78.97 o 1 5 0 5973.09 5985.78 90.29 o 2 5 0 7919.45 7909.00 127.07 o 3 5 0 952.93 1093.93 42.40 o 4 5 0 2106.92 2304.43 66.18 o 5 5 0 1918.54 1962.64 56.43 o 6 5 0 2559.13 2445.31 76.37 o 7 5 0 229.90 241.43 37.22 o 8 5 0 581.69 492.33 58.12 o 9 5 0 599.43 573.94 65.81 o 10 5 0 1.29 -44.33 44.33 o 11 5 0 419.12 332.35 111.99 o 12 5 0 443.53 349.15 96.80 o 13 5 0 598.80 454.66 145.90 o 0 6 0 23099.47 23354.11 408.23 o 1 6 0 111.75 108.11 14.63 o 2 6 0 561.97 702.56 40.10 o 3 6 0 6245.71 5832.86 111.39 o 4 6 0 25.56 10.62 17.91 o 5 6 0 139.15 131.40 25.88 o 6 6 0 8882.18 8557.41 148.96 o 7 6 0 80.17 26.65 26.45 o 8 6 0 1708.97 1642.94 86.49 o 9 6 0 2926.86 2817.13 120.70 o 10 6 0 9.39 -47.58 47.58 o 11 6 0 120.06 130.59 67.14 o 12 6 0 715.89 806.37 110.09 o 13 6 0 2.62 34.43 114.27 o 1 7 0 5118.37 5090.97 91.30 o 2 7 0 2457.98 2352.22 53.29 o 3 7 0 196.65 180.64 24.15 o 4 7 0 4212.03 4156.57 97.02 o 5 7 0 71.12 34.22 22.91 o 6 7 0 7090.88 6894.37 148.16 o 7 7 0 5496.77 5583.98 137.57 o 8 7 0 5565.20 5686.64 154.92 o 9 7 0 63.76 15.09 39.34 o 10 7 0 263.41 82.66 64.09 o 11 7 0 1744.09 1857.83 142.30 o 12 7 0 53.04 22.53 74.80 o 13 7 0 3.71 12.30 122.57 o 0 8 0 472.95 389.47 39.77 o 1 8 0 25225.11 24865.80 314.54 o 2 8 0 20115.66 20445.38 267.57 o 3 8 0 2322.91 2264.71 66.45 o 4 8 0 3215.59 3137.23 84.52 o 5 8 0 1060.07 1016.34 54.65 o 6 8 0 2927.58 2622.75 87.11 o 7 8 0 7438.09 7306.30 171.14 o 8 8 0 6192.88 6050.62 186.91 o 9 8 0 1034.29 957.70 85.05 o 10 8 0 2244.14 2101.46 165.33 o 11 8 0 5.50 -60.25 60.25 o 12 8 0 165.91 184.26 89.24 o 13 8 0 1264.63 1028.97 174.64 o 1 9 0 3521.57 3392.24 72.56 o 2 9 0 3585.93 3232.80 70.32 o 3 9 0 7677.32 7921.02 146.36 o 4 9 0 14551.09 14188.92 232.60 o 5 9 0 10528.28 10596.93 194.61 o 6 9 0 226.82 266.02 40.74 o 7 9 0 1605.65 1812.88 90.77 o 8 9 0 1752.91 1857.23 99.50 o 9 9 0 225.43 178.36 49.60 o 10 9 0 860.46 817.91 120.40 o 11 9 0 2793.45 2718.67 163.86 o 12 9 0 164.22 85.35 80.79 o 0 10 0 27785.48 27307.71 497.29 o 1 10 0 722.33 691.71 34.83 o 2 10 0 1814.54 1621.59 49.25 o 3 10 0 10480.17 10261.93 161.00 o 4 10 0 3469.19 3150.73 90.20 o 5 10 0 277.05 302.38 38.26 o 6 10 0 9345.26 9339.51 188.77 o 7 10 0 498.25 507.72 59.18 o 8 10 0 835.99 737.14 85.24 o 9 10 0 5157.53 5380.78 227.64 o 10 10 0 354.51 411.85 94.63 o 11 10 0 567.15 579.28 113.03 o 12 10 0 856.77 972.92 141.10 o 1 11 0 79.10 45.60 17.69 o 2 11 0 5939.76 5600.22 105.86 o 3 11 0 2686.41 2525.53 66.03 o 4 11 0 534.89 554.54 53.47 o 5 11 0 2808.49 2916.80 93.24 o 6 11 0 407.05 332.75 46.68 o 7 11 0 147.59 141.79 52.39 o 8 11 0 1649.99 1596.13 124.80 o 9 11 0 27.76 -41.66 48.02 o 10 11 0 1869.07 1657.75 133.22 o 11 11 0 53.88 -10.94 70.96 o 12 11 0 71.91 -7.14 78.44 o 0 12 0 5876.37 5593.50 155.69 o 1 12 0 6672.51 6964.32 126.88 o 2 12 0 6557.20 6595.03 122.08 o 3 12 0 459.04 438.65 39.67 o 4 12 0 495.50 495.94 53.94 o 5 12 0 362.45 308.47 48.16 o 6 12 0 410.77 328.15 51.68 o 7 12 0 9751.20 9754.39 267.03 o 8 12 0 3908.71 3869.84 205.03 o 9 12 0 63.68 34.91 54.71 o 10 12 0 819.34 705.70 99.80 o 11 12 0 914.62 668.76 124.34 o 12 12 0 11.14 -72.24 72.24 o 1 13 0 13.06 -3.38 18.08 o 2 13 0 13.83 -7.84 21.87 o 3 13 0 272.90 289.09 45.26 o 4 13 0 969.19 1181.19 77.12 o 5 13 0 1.82 0.53 33.37 o 6 13 0 466.13 411.05 56.89 o 7 13 0 133.22 100.25 56.10 o 8 13 0 148.11 164.03 63.29 o 9 13 0 118.36 64.29 59.48 o 10 13 0 154.57 189.08 74.01 o 11 13 0 76.60 84.85 80.01 o 12 13 0 56.39 3.76 87.75 o 0 14 0 1887.70 1965.13 93.14 o 1 14 0 2386.32 2317.32 81.41 o 2 14 0 2930.36 3018.10 94.50 o 3 14 0 495.22 457.82 53.97 o 4 14 0 1092.08 1116.91 78.48 o 5 14 0 164.67 145.97 44.08 o 6 14 0 547.11 471.73 61.74 o 7 14 0 5528.61 5563.28 202.87 o 8 14 0 2415.90 2596.08 134.93 o 9 14 0 29.20 22.10 60.49 o 10 14 0 1795.21 1664.37 145.79 o 11 14 0 747.02 586.88 119.77 o 1 15 0 1998.61 1893.87 77.79 o 2 15 0 1750.10 1715.64 76.29 o 3 15 0 379.27 400.53 54.08 o 4 15 0 78.59 56.80 38.08 o 5 15 0 2576.41 2510.60 113.83 o 6 15 0 175.40 238.12 54.54 o 7 15 0 24.38 58.65 56.72 o 8 15 0 678.05 829.12 94.23 o 9 15 0 866.15 766.09 105.78 o 10 15 0 958.90 885.80 119.50 o 11 15 0 151.00 108.25 89.64 o 0 16 0 4891.99 4601.35 201.29 o 1 16 0 1247.86 1276.49 72.26 o 2 16 0 607.43 606.64 62.84 o 3 16 0 10237.56 10198.29 234.21 o 4 16 0 895.19 827.41 75.88 o 5 16 0 399.51 444.70 65.21 o 6 16 0 2849.45 3196.66 155.24 o 7 16 0 110.61 18.60 55.14 o 8 16 0 244.16 204.21 73.06 o 9 16 0 951.78 838.02 112.78 o 10 16 0 300.06 163.45 77.02 o 11 16 0 2.44 64.95 91.11 o 1 17 0 38.64 38.61 37.79 o 2 17 0 7348.54 7388.61 199.40 o 3 17 0 160.20 87.87 44.14 o 4 17 0 1682.38 1694.12 115.90 o 5 17 0 1357.79 1463.04 102.91 o 6 17 0 33.34 26.48 51.76 o 7 17 0 1687.09 1807.27 135.91 o 8 17 0 1723.68 1960.05 151.86 o 9 17 0 441.21 406.82 94.99 o 10 17 0 16.33 -60.70 67.78 o 0 18 0 168.35 286.34 78.45 o 1 18 0 8912.74 9279.12 225.47 o 2 18 0 5504.01 5473.36 192.79 o 3 18 0 320.26 187.83 61.04 o 4 18 0 1171.59 1117.14 91.56 o 5 18 0 1619.58 1456.07 104.96 o 6 18 0 243.42 194.72 68.39 o 7 18 0 4161.96 4314.99 176.15 o 8 18 0 679.08 668.15 102.40 o 9 18 0 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0 1350.02 1186.79 147.07 o 6 22 0 154.41 96.91 86.83 o 7 22 0 655.52 765.94 132.78 o 8 22 0 1715.26 1457.15 173.40 o 1 23 0 1.97 44.89 76.52 o 2 23 0 449.41 262.84 100.14 o 3 23 0 24.91 23.48 66.72 o 4 23 0 1340.91 1132.87 122.87 o 5 23 0 0.74 21.41 84.33 o 6 23 0 39.47 -42.70 76.50 o 7 23 0 170.86 187.17 97.74 o 0 24 0 839.65 837.48 183.42 o 1 24 0 2937.72 3182.90 205.93 o 2 24 0 362.59 350.07 89.48 o 3 24 0 23.53 -62.24 62.24 o 4 24 0 673.77 865.44 120.15 o 5 24 0 1319.27 1488.73 168.01 o 6 24 0 312.44 245.07 107.50 o 1 25 0 1426.87 1329.74 159.44 o 2 25 0 105.62 165.68 96.88 o 3 25 0 172.96 116.88 92.42 o 4 25 0 361.96 405.72 99.09 o 5 25 0 742.54 902.31 148.06 o 0 26 0 6068.96 6067.94 414.72 o 1 26 0 604.48 509.50 121.57 o 2 26 0 2.50 -78.41 78.41 o 3 26 0 1770.45 1648.98 168.17 o 4 26 0 5.63 79.67 110.63 o 1 27 0 756.02 836.42 145.90 o 2 27 0 1762.78 1649.64 181.37 o 3 27 0 224.56 370.50 115.58 o -13 1 1 747.37 565.81 111.90 o -12 1 1 546.96 591.14 136.89 o -11 1 1 9.76 -61.30 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219.83 25.00 o -4 2 1 8815.57 8743.34 134.69 o -3 2 1 2512.27 2601.29 54.56 o -2 2 1 128.96 119.91 12.87 o -1 2 1 14367.18 14631.93 206.00 o 0 2 1 2671.93 2768.71 45.92 o 1 2 1 1125.81 1150.87 32.65 o 2 2 1 3550.31 3905.68 60.52 o 3 2 1 9716.72 9668.30 129.93 o 4 2 1 8107.88 8244.41 128.46 o 5 2 1 555.36 528.61 31.97 o 6 2 1 2444.51 2495.85 69.76 o 7 2 1 29.77 3.58 19.98 o 8 2 1 2836.25 2782.60 95.61 o 9 2 1 208.56 182.39 54.10 o 10 2 1 578.90 648.04 83.31 o 11 2 1 1025.66 1139.76 128.42 o 12 2 1 11.57 27.01 71.95 o 13 2 1 28.91 -7.91 77.62 o -13 3 1 5.07 -60.32 72.72 o -12 3 1 663.13 812.32 183.99 o -11 3 1 35.86 -23.85 53.60 o -10 3 1 14.09 -3.44 47.41 o -9 3 1 6689.76 6691.73 182.23 o -8 3 1 689.85 707.09 52.17 o -7 3 1 1679.28 1712.93 63.81 o -6 3 1 33753.11 34754.38 445.47 o -5 3 1 163.92 101.00 20.14 o -4 3 1 412.55 480.47 33.01 o -3 3 1 42.27 43.63 13.21 o -2 3 1 11485.91 12190.42 171.97 o -1 3 1 7408.02 7570.40 122.06 o 0 3 1 39797.95 40318.92 460.10 o 1 3 1 1672.58 1605.33 34.25 o 2 3 1 2213.40 2471.03 48.45 o 3 3 1 4716.44 4133.97 73.66 o 4 3 1 637.38 799.06 43.81 o 5 3 1 2036.13 2010.30 56.75 o 6 3 1 3238.30 2926.70 83.63 o 7 3 1 1035.98 1002.41 50.86 o 8 3 1 6039.78 5984.56 145.46 o 9 3 1 13676.96 13988.75 328.57 o 10 3 1 589.70 548.69 79.68 o 11 3 1 548.89 551.54 91.64 o 12 3 1 876.81 988.34 132.10 o 13 3 1 299.72 111.00 89.65 o -13 4 1 557.74 589.18 122.35 o -12 4 1 7.67 -2.77 71.07 o -11 4 1 260.54 281.06 71.66 o -10 4 1 3070.86 3024.48 147.83 o -9 4 1 542.07 619.30 72.45 o -8 4 1 3417.76 3518.92 138.65 o -7 4 1 10005.74 10370.65 178.72 o -6 4 1 3.99 -17.33 17.33 o -5 4 1 2529.75 2488.66 64.21 o -4 4 1 3245.99 3146.73 84.55 o -3 4 1 992.31 979.55 38.75 o -2 4 1 18697.06 18420.06 249.27 o -1 4 1 7209.88 7238.25 110.68 o 0 4 1 12025.86 12193.20 155.62 o 1 4 1 20043.27 20540.81 265.66 o 2 4 1 13090.25 12864.05 169.44 o 3 4 1 6253.32 6864.14 113.84 o 4 4 1 242.95 218.59 22.06 o 5 4 1 1345.73 1170.14 42.48 o 6 4 1 3083.77 2975.60 77.05 o 7 4 1 43.61 15.42 26.27 o 8 4 1 7186.89 7535.81 280.28 o 9 4 1 1553.36 1477.97 121.26 o 10 4 1 515.05 385.30 101.00 o 11 4 1 1617.39 1785.29 132.21 o 12 4 1 206.89 335.68 101.51 o 13 4 1 7.88 44.64 85.04 o -13 5 1 1926.56 1864.20 234.66 o -12 5 1 806.86 861.60 137.10 o -11 5 1 1293.61 1250.10 115.82 o -10 5 1 1958.38 2193.15 129.56 o -9 5 1 362.20 307.88 52.01 o -8 5 1 13186.84 13024.03 289.37 o -7 5 1 9951.24 9692.03 190.53 o -6 5 1 33.49 29.59 19.17 o -5 5 1 11288.38 11231.11 172.54 o -4 5 1 90.40 38.71 18.93 o -3 5 1 15844.78 16182.24 234.65 o -2 5 1 18303.23 18985.48 259.64 o -1 5 1 2107.40 2160.47 51.57 o 0 5 1 462.69 480.03 28.28 o 1 5 1 84555.27 86532.22 978.69 o 2 5 1 8102.06 8390.51 122.53 o 3 5 1 3001.56 3084.50 63.31 o 4 5 1 15609.58 14994.86 209.28 o 5 5 1 73.78 44.54 17.39 o 6 5 1 2128.93 2252.91 66.54 o 7 5 1 15906.04 15617.04 271.51 o 8 5 1 2651.21 2651.83 109.75 o 9 5 1 2716.67 2760.86 136.73 o 10 5 1 4210.81 4324.28 212.92 o 11 5 1 83.17 19.90 66.23 o 12 5 1 42.55 27.24 73.51 o 13 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