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Information card for entry 1549488
Preview
| Coordinates | 1549488.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C15 H20 Cl2 O6 Pd |
|---|---|
| Calculated formula | C15 H20 Cl2 O6 Pd |
| Title of publication | Ten-fold boost of catalytic performance in thiol‒yne click reaction enabled by a palladium diketonate complex with a hexafluoroacetylacetonate ligand |
| Authors of publication | Eremin, Dmitry B.; Boiko, Daniil A.; Borkovskaya, Eugenia V.; Khrustalev, Victor N.; Chernyshev, Victor M.; Ananikov, Valentine P. |
| Journal of publication | Catalysis Science & Technology |
| Year of publication | 2018 |
| Journal volume | 8 |
| Journal issue | 12 |
| Pages of publication | 3073 |
| a | 11.6869 ± 0.0005 Å |
| b | 8.8935 ± 0.0004 Å |
| c | 8.551 ± 0.0004 Å |
| α | 90° |
| β | 90.223 ± 0.001° |
| γ | 90° |
| Cell volume | 888.76 ± 0.07 Å3 |
| Cell temperature | 120 ± 2 K |
| Ambient diffraction temperature | 120 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 12 |
| Hermann-Mauguin space group symbol | C 1 2/m 1 |
| Hall space group symbol | -C 2y |
| Residual factor for all reflections | 0.0217 |
| Residual factor for significantly intense reflections | 0.0217 |
| Weighted residual factors for significantly intense reflections | 0.0555 |
| Weighted residual factors for all reflections included in the refinement | 0.0555 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.069 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 227977 (current) | 2019-11-17 | cif/ Updating files of 1549488, 1549489 Original log message: Adding full bibliography for 1549488--1549489.cif. |
1549488.cif |
| 208027 | 2018-05-30 | cif/ Adding structures of 1549488, 1549489 via cif-deposit CGI script. |
1549488.cif |
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Users of the data should acknowledge the original authors of the
structural data.