Crystallography Open Database

Information card for entry 1549673

Preview

Coordinates	1549673.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C108.67 H59 N O24 Rh4
Calculated formula	C108.667 H59 N O24 Rh4
Title of publication	Switchable gate-opening effect in metal-organic polyhedra assemblies through solution processing.
Authors of publication	Craig, Gavin A.; Larpent, Patrick; Kusaka, Shinpei; Matsuda, Ryotaro; Kitagawa, Susumu; Furukawa, Shuhei
Journal of publication	Chemical science
Year of publication	2018
Journal volume	9
Journal issue	31
Pages of publication	6463 - 6469
a	17.9146 ± 0.0002 Å
b	18.0902 ± 0.0003 Å
c	27.6891 ± 0.0003 Å
α	77.345 ± 0.001°
β	83.125 ± 0.001°
γ	61.947 ± 0.001°
Cell volume	7725.35 ± 0.19 Å³
Cell temperature	92 K
Ambient diffraction temperature	92 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0687
Residual factor for significantly intense reflections	0.0568
Weighted residual factors for significantly intense reflections	0.1585
Weighted residual factors for all reflections included in the refinement	0.1693
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
228810 (current)	2019-11-17	cif/ Updating files of 1549671, 1549672, 1549673 Original log message: Adding full bibliography for 1549671--1549673.cif.	1549673.cif
208957	2018-07-11	cif/ Adding structures of 1549671, 1549672, 1549673 via cif-deposit CGI script.	1549673.cif