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Information card for entry 1549956
Preview
| Coordinates | 1549956.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C169 H142 Au13 B Cl6 Sb8 |
|---|---|
| Calculated formula | C169 H142 Au13 B Cl6 Sb8 |
| SMILES | [Au]123([Au]456([Au]789([Au]%10%11%12([Au]%13%14%15([Au]%16%17%18([Au]%19%20%21([Au]%221([Au]4%13%16([Au]1369%12%15%18%21%22([Au]%10%17%19([Au]27%201Cl)Cl)[Au]58%11%14Cl)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)Cl)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1.ClCCl.c1(ccccc1)[B-](c1ccccc1)(c1ccccc1)c1ccccc1 |
| Title of publication | Stibine-protected Au<sub>13</sub> nanoclusters: syntheses, properties and facile conversion to GSH-protected Au<sub>25</sub> nanocluster. |
| Authors of publication | Li, Ying-Zhou; Ganguly, Rakesh; Hong, Kar Yiu; Li, Yongxin; Tessensohn, Malcolm Eugene; Webster, Richard; Leong, Weng Kee |
| Journal of publication | Chemical science |
| Year of publication | 2018 |
| Journal volume | 9 |
| Journal issue | 46 |
| Pages of publication | 8723 - 8730 |
| a | 16.7528 ± 0.0008 Å |
| b | 46.762 ± 0.002 Å |
| c | 22.2312 ± 0.0011 Å |
| α | 90° |
| β | 96.6202 ± 0.0016° |
| γ | 90° |
| Cell volume | 17299.7 ± 1.4 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0955 |
| Residual factor for significantly intense reflections | 0.0741 |
| Weighted residual factors for significantly intense reflections | 0.1752 |
| Weighted residual factors for all reflections included in the refinement | 0.1914 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.068 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 228752 (current) | 2019-11-17 | cif/ Updating files of 1549953, 1549954, 1549955, 1549956, 1549957 Original log message: Adding full bibliography for 1549953--1549957.cif. |
1549956.cif |
| 211030 | 2018-09-18 | cif/ Adding structures of 1549953, 1549954, 1549955, 1549956, 1549957 via cif-deposit CGI script. |
1549956.cif |
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Users of the data should acknowledge the original authors of the
structural data.