Crystallography Open Database

Information card for entry 1550008

Preview

Coordinates	1550008.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C73 H32 Al Cs F46 O7
Calculated formula	C73 H32 Al Cs F46 O7
Title of publication	Al(OCArF3)<sub>3</sub> - a thermally stable Lewis superacid.
Authors of publication	Kögel, Julius F; Timoshkin, Alexey Y.; Schröder, Artem; Lork, Enno; Beckmann, Jens
Journal of publication	Chemical science
Year of publication	2018
Journal volume	9
Journal issue	43
Pages of publication	8178 - 8183
a	13.4499 ± 0.0005 Å
b	13.5054 ± 0.0005 Å
c	44.2327 ± 0.0016 Å
α	98.198 ± 0.001°
β	92.575 ± 0.001°
γ	90.287 ± 0.001°
Cell volume	7944 ± 0.5 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0756
Residual factor for significantly intense reflections	0.055
Weighted residual factors for significantly intense reflections	0.1068
Weighted residual factors for all reflections included in the refinement	0.114
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
228686 (current)	2019-11-17	cif/ Updating files of 1550001, 1550002, 1550003, 1550004, 1550005, 1550006, 1550007, 1550008, 1550009, 1550010, 1550011, 1550012, 1550013, 1550014 Original log message: Adding full bibliography for 1550001--1550014.cif.	1550008.cif
211285	2018-10-03	cif/ Adding structures of 1550001, 1550002, 1550003, 1550004, 1550005, 1550006, 1550007, 1550008, 1550009, 1550010, 1550011, 1550012, 1550013, 1550014 via cif-deposit CGI script.	1550008.cif