#------------------------------------------------------------------------------ #$Date: 2019-01-16 05:40:06 +0200 (Wed, 16 Jan 2019) $ #$Revision: 213120 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/55/04/1550482.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1550482 _cell_angle_alpha 88.061 _cell_angle_beta 72.058 _cell_angle_gamma 77.104 _cell_length_a 12.2257 _cell_length_b 19.3422 _cell_length_c 19.5199 _exptl_crystal_F_000 1806.00 _reflns_d_resolution_high 0.7857 _cod_data_source_file pk4022Isup2.hkl _cod_data_source_block I _shelx_title ' jfli47_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 383.79 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 160.17 180.54 7.58 o 3 0 0 7559.67 7235.09 88.12 o 4 0 0 328.58 356.82 11.00 o 5 0 0 232.41 221.75 13.47 o 6 0 0 35.33 47.61 13.08 o 7 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82.00 o -9 11 4 1399.62 1479.84 75.91 o -8 11 4 242.79 260.00 44.75 o -7 11 4 1009.61 1014.25 31.55 o -6 11 4 24.02 77.38 28.62 o -5 11 4 405.43 453.66 23.72 o -4 11 4 2842.36 2769.18 46.83 o -3 11 4 5643.34 5738.22 74.82 o -2 11 4 887.18 1009.68 28.19 o -1 11 4 358.25 309.43 19.89 o 0 11 4 4372.12 4270.99 55.26 o 1 11 4 143.28 110.86 20.46 o 2 11 4 2803.54 2676.54 47.19 o 3 11 4 16.06 34.32 15.76 o 4 11 4 597.27 612.79 19.16 o 5 11 4 3802.90 3784.91 44.22 o 6 11 4 1786.58 1912.75 30.71 o 7 11 4 23.53 18.00 12.19 o 8 11 4 161.91 164.63 15.50 o 9 11 4 163.36 180.18 15.68 o 10 11 4 275.53 295.26 24.35 o 11 11 4 441.39 367.75 33.55 o 12 11 4 786.68 799.29 49.63 o 13 11 4 1521.90 1409.22 65.69 o 14 11 4 1043.33 1249.59 61.30 o -10 12 4 60.81 26.17 57.98 o -9 12 4 38.54 53.90 63.66 o -8 12 4 70.83 85.40 42.21 o -7 12 4 4233.21 4266.24 78.77 o -6 12 4 1445.48 1437.41 42.30 o -5 12 4 109.40 60.54 19.77 o -4 12 4 7.04 9.71 19.25 o -3 12 4 904.40 817.83 27.66 o -2 12 4 1026.98 1095.84 30.57 o 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